石墨炉原子吸收分光光度法测定自制阳性猪肉中铅的不确定度评定

目的评估用石墨炉原子吸收分光光度法测定自制阳性猪肉中铅的不确定度,以找出影响不确定度的因素,为评价检验结果提供科学依据。方法建立猪肉中铅含量不确定度的数学模型,分析不确定度来源,并进行不确定度的评定。结果自制阳性猪肉中铅的含量为0.236 mg/kg,扩展不确定度为0.026 mg/kg（包含因子k=2）,影响不确定度的主要因素是标准曲线线性拟合和分析仪器。结论可通过控制标准曲线校准过程和加强对分析仪器的保养维护,来降低石墨炉原子吸收分光光度法测定猪肉中铅含量的不确定度。...

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Bibliographic Details
Published in食品安全质量检测学报 Vol. 7; no. 7; pp. 2963 - 2967
Main Author 陈晓 刘剑虹 张可冬 娄婧婧 张晓文
Format Journal Article
LanguageChinese
Published 广州市体育科学研究所,广州,510620 2016
Subjects
不确定度
原子吸收分光光度法
自制阳性猪肉
铅
原子吸收分光光度法
graphite furnace atomic absorption spectrometry
铅
不确定度
homemade positive pork
自制阳性猪肉
uncertainty
plumbum
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Summary:目的评估用石墨炉原子吸收分光光度法测定自制阳性猪肉中铅的不确定度,以找出影响不确定度的因素,为评价检验结果提供科学依据。方法建立猪肉中铅含量不确定度的数学模型,分析不确定度来源,并进行不确定度的评定。结果自制阳性猪肉中铅的含量为0.236 mg/kg,扩展不确定度为0.026 mg/kg（包含因子k=2）,影响不确定度的主要因素是标准曲线线性拟合和分析仪器。结论可通过控制标准曲线校准过程和加强对分析仪器的保养维护,来降低石墨炉原子吸收分光光度法测定猪肉中铅含量的不确定度。
Bibliography:graphite furnace atomic absorption spectrometry; homemade positive pork; plumbum; uncertainty
11-5956/TS
CHEN Xiao, LIU Jian-Hong, ZHANG Ke-Dong, LOU Jing-Jing, ZHANG Xiao-Wen （Guangzhou Institute of Sports Science, Guangzhou 510620, China）
Objective To analyze the uncertainty in the determination of plumbum in homemade positive pork by graphite furnace atomic absorption spectrometry to provide the evidence for the measurement evaluation. Methods Graphite furnace atomic absorption spectrometry was used to determine the content of plumbum in pork. The determination process was analyzed to identify the source of uncertainty and the combined uncertainty was calculated. Results The content of plumbum in homemade positive pork was 0.236 mg/kg, and the expanded uncertainty was 0.026 mg/kg （k=2）. The main factors of the uncertainty were standard curve linear fitting and analytical instruments. Conclusion The control of preparation of standard curve and the maintenance of analytical instruments can reduce the uncertaint
ISSN:2095-0381