Effect of sintering procedures on optical properties, chemical composition, and grain size of monolithic zirconia ceramic at different thicknesses after hydrothermal aging: An in vitro study

• Published in: The journal of Indian Prosthodontic Society Vol. 23; no. 1; pp. 57 - 64
• Main Authors: Albayrak, Haydar, Eraslan, Ravza, Aydinlioglu, Ömer
• Format: Journal Article
• Language: English
• Published: India Wolters Kluwer India Pvt. Ltd 01.01.2023; Medknow Publications and Media Pvt. Ltd; Medknow Publications & Media Pvt. Ltd; Wolters Kluwer - Medknow; Wolters Kluwer Medknow Publications
• Subjects: 3 mol% yttria-stabilized tetragonal zirconia polycrystal; Aging; Aluminum oxide; Ceramics - chemistry; Chemical composition; Corticosteroids; Dental Materials - chemistry; Fluorescence; fluorescence parameter; Fluorescence spectroscopy; Grain size; Materials Testing; Optical properties; Scanning electron microscopy; Sintering; sintering procedure; Statistical analysis; Surface Properties; Variance analysis; Zirconia; Zirconium oxide; Florida; grain size; sintering procedure; 3 Mol% yttria-stabilized tetragonal zirconia polycrystal; fluorescence parameter
• ISSN: 0972-4052; 1998-4057
• DOI: 10.4103/jips.jips_345_22

Aim: The purpose of the present study was to examine the optical properties, chemical composition, and grain size (GS) of monolithic zirconia (MZ) ceramic at different thicknesses sintered using different procedures after hydrothermal aging. Settings and Design: An in vitro study. Materials and Methods: Forty MZ discs (0.5-mm thickness [Group-0.5] and 1-mm thickness [Group-1]; 12 mm diameter) were milled and divided according to standard (Group-ST) and speed (Group-SP) sintering procedures. All specimens were hydrothermally aged at 134°C after sintering. Translucency (TP), opalescence (OP), and fluorescence (ΔEabFNx01-FL) parameters were calculated using the color coordinates (LFNx01, aFNx01, bFNx01, respectively) of the discs. The chemical composition and the GS of the specimens were characterized using X-ray fluorescence spectroscopy and a scanning electron microscopy, respectively. Statistical Analysis Used: TPs and ΔEabFNx01-FLs were analyzed using independent samples t-tests and Mann-Whitney U-tests while a two-way analysis of variance (ANOVA) was used for OPs. Results: Group-1 showed significantly lower TP than Group-0.5 (P < 0.001) but a significantly higher OP (P = 0.014). Group-SP showed significantly higher OP (P = 0.00003) and ΔEabFNx01-FL (P = 0.0026) values than Group-ST without considering the thickness. Group-SP (0.29 ± 0.119 μm) had a smaller GS than Group-ST (0.306 ± 0.142 μm). Compared to Group-ST, Group-SP had a lower percentage of Y2O3 and a higher percentage of Al2O3. Conclusion: The effect of the sintering procedure on TP and OP of MZ was not perceived by the naked eye. The speed sintering procedure may increase Δ EFNx01ab-FL of MZ to higher values than natural teeth when compared with standard sintering. The speed sintering may cause minor changes in GS and the chemical composition of MZ.