The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source
The MYTHEN single‐photon‐counting silicon microstrip detector has been developed at the Swiss Light Source for time‐resolved powder diffraction experiments. An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns o...
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Published in | Journal of synchrotron radiation Vol. 17; no. 5; pp. 653 - 668 |
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Main Authors | , , , , , , , , , |
Format | Journal Article |
Language | English |
Published |
5 Abbey Square, Chester, Cheshire CH1 2HU, England
International Union of Crystallography
01.09.2010
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Subjects | |
Online Access | Get full text |
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Summary: | The MYTHEN single‐photon‐counting silicon microstrip detector has been developed at the Swiss Light Source for time‐resolved powder diffraction experiments. An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns over 120° in 2θ in fractions of seconds. Thanks to the outstanding performance of the detector and to the calibration procedures developed, the quality of the data obtained is now comparable with that of traditional high‐resolution point detectors in terms of FWHM resolution and peak profile shape, with the additional advantage of fast and simultaneous acquisition of the full diffraction pattern. MYTHEN is therefore optimal for time‐resolved or dose‐critical measurements. The characteristics of the MYTHEN detector together with the calibration procedures implemented for the optimization of the data are described in detail. The refinements of two known standard powders are discussed together with a remarkable application of MYTHEN to organic compounds in relation to the problem of radiation damage. |
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Bibliography: | ark:/67375/WNG-XM7S3FF6-H istex:60C797F135B0C59CF34B52D9DB2532D100F5F9AF ArticleID:JSYGF5028 ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 ObjectType-Article-2 ObjectType-Feature-1 |
ISSN: | 1600-5775 0909-0495 1600-5775 |
DOI: | 10.1107/S0909049510026051 |