Ultra-stable sub-meV monochromator for hard X-rays

A high‐resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in 151Eu. The first‐of‐its‐kind, fully cryogenic design achieves an energy‐alignment stability of 0.017 m...

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Published inJournal of synchrotron radiation Vol. 22; no. 5; pp. 1155 - 1162
Main Authors Toellner, T. S., Collins, J., Goetze, K., Hu, M. Y., Preissner, C., Trakhtenberg, E., Yan, L.
Format Journal Article
LanguageEnglish
Published 5 Abbey Square, Chester, Cheshire CH1 2HU, England International Union of Crystallography 01.09.2015
John Wiley & Sons, Inc
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Summary:A high‐resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in 151Eu. The first‐of‐its‐kind, fully cryogenic design achieves an energy‐alignment stability of 0.017 meV r.m.s. per day, or a 100‐fold improvement over other meV‐monochromators, and can tolerate higher X‐ray power loads than room‐temperature designs of comparable resolution. This offers the potential for significantly more accurate measurements of lattice excitation energies using nuclear resonant vibrational spectroscopy if combined with accurate energy calibration using, for example, high‐speed Doppler shifting. The design of the monochromator along with its performance and impact on transmitted beam properties are presented.
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AC02-06CH11357; FC52-06NA27684
USDOE Office of Science (SC), Basic Energy Sciences (BES)
USDOE National Nuclear Security Administration (NNSA)
ISSN:1600-5775
0909-0495
1600-5775
DOI:10.1107/S1600577515012230