Kinetics of the self-assembly of nanocrystal superlattices measured by real-time in situ X-ray scattering
On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and final states can be readily characterized, little is known about the dynamic transformation from colloid to superlattice. Here, by using in situ grazing-i...
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| Published in | Nature materials Vol. 15; no. 7; pp. 775 - 781 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
01.07.2016
Nature Publishing Group |
| Subjects | |
| Online Access | Get full text |
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| Abstract | On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and final states can be readily characterized, little is known about the dynamic transformation from colloid to superlattice. Here, by using
in situ
grazing-incidence X-ray scattering, we tracked the self-assembly of lead sulfide nanocrystals in real time. Following the first appearance of an ordered arrangement, the superlattice underwent uniaxial contraction and collective rotation as it approached its final body-centred cubic structure. The nanocrystals became crystallographically aligned early in the overall self-assembly process, showing that nanocrystal ordering occurs on a faster timescale than superlattice densification. Our findings demonstrate that synchrotron X-ray scattering is a viable method for studying self-assembly in its native environment, with ample time resolution to extract kinetic rates and observe intermediate configurations. The method could be used for real-time direction of self-assembly processes and to better understand the forces governing self-organization of soft materials.
The self-assembly of lead sulfide nanocrystals into a body-centred cubic lattice can be tracked in real time by using
in situ
grazing-incidence X-ray scattering. |
|---|---|
| AbstractList | On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and final states can be readily characterized, little is known about the dynamic transformation from colloid to superlattice. Here, by using in situ grazing-incidence X-ray scattering, we tracked the self-assembly of lead sulfide nanocrystals in real time. Following the first appearance of an ordered arrangement, the superlattice underwent uniaxial contraction and collective rotation as it approached its final body-centred cubic structure. The nanocrystals became crystallographically aligned early in the overall self-assembly process, showing that nanocrystal ordering occurs on a faster timescale than superlattice densification. Our findings demonstrate that synchrotron X-ray scattering is a viable method for studying self-assembly in its native environment, with ample time resolution to extract kinetic rates and observe intermediate configurations. The method could be used for real-time direction of self-assembly processes and to better understand the forces governing self-organization of soft materials.On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and final states can be readily characterized, little is known about the dynamic transformation from colloid to superlattice. Here, by using in situ grazing-incidence X-ray scattering, we tracked the self-assembly of lead sulfide nanocrystals in real time. Following the first appearance of an ordered arrangement, the superlattice underwent uniaxial contraction and collective rotation as it approached its final body-centred cubic structure. The nanocrystals became crystallographically aligned early in the overall self-assembly process, showing that nanocrystal ordering occurs on a faster timescale than superlattice densification. Our findings demonstrate that synchrotron X-ray scattering is a viable method for studying self-assembly in its native environment, with ample time resolution to extract kinetic rates and observe intermediate configurations. The method could be used for real-time direction of self-assembly processes and to better understand the forces governing self-organization of soft materials. On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and final states can be readily characterized, little is known about the dynamic transformation from colloid to superlattice. Here, by using in situ grazing-incidence X-ray scattering, we tracked the self-assembly of lead sulfide nanocrystals in real time. Following the first appearance of an ordered arrangement, the superlattice underwent uniaxial contraction and collective rotation as it approached its final body-centred cubic structure. The nanocrystals became crystallographically aligned early in the overall self-assembly process, showing that nanocrystal ordering occurs on a faster timescale than superlattice densification. Our findings demonstrate that synchrotron X-ray scattering is a viable method for studying self-assembly in its native environment, with ample time resolution to extract kinetic rates and observe intermediate configurations. The method could be used for real-time direction of self-assembly processes and to better understand the forces governing self-organization of soft materials. On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and nal states can be readily characterized, little is known about the dynamic transformation from colloid to superlattice. Here, by using in situ grazing-incidence X-ray scattering, we tracked the self-assembly of lead sulde nanocrystals in real time. Following the rst appearance of an ordered arrangement, the superlattice underwent uniaxial contraction and collective rotation as it approached its nal body-centred cubic structure. The nanocrystals became crystallographically aligned early in the overall self-assembly process, showing that nanocrystal ordering occurs on a faster timescale than superlattice densication. Our ndings demonstrate that synchrotron X-ray scattering is a viable method for studying self-assembly in its native environment, with ample time resolution to extract kinetic rates and observe intermediate congurations. The method could be used for real-time direction of self-assembly processes and to better understand the forces governing self-organization of soft materials. On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and final states can be readily characterized, little is known about the dynamic transformation from colloid to superlattice. Here, by using in situ grazing-incidence X-ray scattering, we tracked the self-assembly of lead sulfide nanocrystals in real time. Following the first appearance of an ordered arrangement, the superlattice underwent uniaxial contraction and collective rotation as it approached its final body-centred cubic structure. The nanocrystals became crystallographically aligned early in the overall self-assembly process, showing that nanocrystal ordering occurs on a faster timescale than superlattice densification. Our findings demonstrate that synchrotron X-ray scattering is a viable method for studying self-assembly in its native environment, with ample time resolution to extract kinetic rates and observe intermediate configurations. The method could be used for real-time direction of self-assembly processes and to better understand the forces governing self-organization of soft materials. The self-assembly of lead sulfide nanocrystals into a body-centred cubic lattice can be tracked in real time by using in situ grazing-incidence X-ray scattering. |
| Author | Weidman, Mark C. Tisdale, William A. Smilgies, Detlef-M. |
| Author_xml | – sequence: 1 givenname: Mark C. surname: Weidman fullname: Weidman, Mark C. organization: Department of Chemical Engineering, Massachusetts Institute of Technology – sequence: 2 givenname: Detlef-M. surname: Smilgies fullname: Smilgies, Detlef-M. organization: Cornell High Energy Synchrotron Source (CHESS), Cornell University – sequence: 3 givenname: William A. orcidid: 0000-0002-6615-5342 surname: Tisdale fullname: Tisdale, William A. email: tisdale@mit.edu organization: Department of Chemical Engineering, Massachusetts Institute of Technology |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/26998914$$D View this record in MEDLINE/PubMed https://www.osti.gov/biblio/1371222$$D View this record in Osti.gov |
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| ContentType | Journal Article |
| Copyright | Springer Nature Limited 2016 Copyright Nature Publishing Group Jul 2016 |
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| DOI | 10.1038/nmat4600 |
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| Snippet | On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and final states... On solvent evaporation, non-interacting monodisperse colloidal particles self-assemble into a close-packed superlattice. Although the initial and nal states... |
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| SubjectTerms | 639/301/357/1017 639/301/357/341 639/925/357/1017 639/925/357/341 Biomaterials Colloids Condensed Matter Physics Evaporation Kinetics Materials Science Nanocrystals Nanotechnology Optical and Electronic Materials Order disorder Real time Scattering Self assembly solar (photovoltaic), solid state lighting, photosynthesis (natural and artificial), charge transport, optics, synthesis (novel materials), synthesis (self-assembly), synthesis (scalable processing) Solvents Superlattices X-rays |
| Title | Kinetics of the self-assembly of nanocrystal superlattices measured by real-time in situ X-ray scattering |
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