Extraction of methocarbamol from human plasma with a polypyrrole/multiwalled carbon nanotubes composite decorated with magnetic nanoparticles as an adsorbent followed by electrospray ionization ion mobility spectrometry detection
In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3O4 nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of...
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| Published in | Journal of separation science Vol. 37; no. 23; pp. 3518 - 3525 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Blackwell Publishing Ltd
01.12.2014
Wiley Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1615-9306 1615-9314 1615-9314 |
| DOI | 10.1002/jssc.201400614 |
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| Abstract | In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3O4 nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic‐modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X‐ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2–150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe3O4‐polypyrrole and Fe3O4‐multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples. |
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| AbstractList | In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe sub(3)O sub(4) nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic-modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X-ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2-150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe sub(3)O sub(4)-polypyrrole and Fe sub(3)O sub(4)-multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples. In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3 O4 nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic-modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X-ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2-150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe3 O4 -polypyrrole and Fe3 O4 -multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples. In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe₃O₄nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic‐modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X‐ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2–150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe₃O₄‐polypyrrole and Fe₃O₄‐multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples. In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3 O4 nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic-modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X-ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2-150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe3 O4 -polypyrrole and Fe3 O4 -multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples.In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3 O4 nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic-modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X-ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2-150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe3 O4 -polypyrrole and Fe3 O4 -multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples. In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3O4 nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic-modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X-ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2-150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe3O4-polypyrrole and Fe3O4-multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples. In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe 3 O 4 nanoparticles was chemically synthesized and applied as a novel adsorbent for the extraction of methocarbamol from human plasma. Electrospray ionization ion mobility spectrometry was used for the determination of the analyte. The properties of the magnetic‐modified adsorbent were characterized by scanning electron microscopy, transmission electron microscopy, Fourier transform IR spectroscopy, and X‐ray diffraction. The effects of experimental parameters on the extraction efficiency of the sorbent were investigated. Under the optimized conditions, the linear dynamic range was found to be 2–150 ng/mL with the detection limit of 0.9 ng/mL. The relative standard deviation was 5.3% for three replicate measurements of methocarbamol in plasma sample. The extraction efficiency of the sorbent for the determination of different drugs with various polarities was also compared to that of Fe 3 O 4 ‐polypyrrole and Fe 3 O 4 ‐multiwalled carbon nanotubes sorbents. Finally, the method was used for the determination of methocarbamol in blood samples. |
| Author | Khayamian, Taghi Hashemian, Zahra Saraji, Mohammad |
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| CitedBy_id | crossref_primary_10_1002_jssc_201600614 crossref_primary_10_1016_j_talanta_2021_122285 crossref_primary_10_1134_S106193482101010X crossref_primary_10_1093_chromsci_bmac091 crossref_primary_10_1016_j_microc_2021_107167 crossref_primary_10_1002_bio_3457 crossref_primary_10_1002_cnma_201700278 crossref_primary_10_1016_j_aca_2018_03_059 crossref_primary_10_1016_j_aca_2020_07_037 crossref_primary_10_1002_jssc_201501258 crossref_primary_10_1016_j_microc_2019_02_007 crossref_primary_10_1016_j_aca_2019_10_066 crossref_primary_10_1016_j_microc_2022_108368 crossref_primary_10_1016_j_chroma_2020_461030 crossref_primary_10_1016_j_chroma_2024_465615 crossref_primary_10_1002_jssc_201401014 crossref_primary_10_1016_j_aca_2016_11_062 crossref_primary_10_1002_bmc_4877 crossref_primary_10_1007_s10337_017_3292_4 crossref_primary_10_1016_j_chroma_2015_07_087 crossref_primary_10_1016_j_jpba_2015_01_021 crossref_primary_10_1016_j_chroma_2018_09_024 crossref_primary_10_1016_j_colsurfa_2019_123583 crossref_primary_10_1039_D0AY01332C |
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| Keywords | Solid phase extraction Biological fluid Fourier transformation Chemical analysis Ion mobility spectrometry Nanoparticle Carbon nanotubes Electrospray Blood Chemical enrichment Blood plasma Surface structure Characterization Multiwalled carbon nanotubes Sample preparation Methocarbamol Antispasmodic agent Adsorbent Polypyrrole Quantitative analysis Modified material Human Validation Iron II Iron III Oxides Healthy subject Muscle relaxant Magnetic nanoparticles X ray diffraction Conducting polymers Infrared spectrometry Magnetic particles Transmission electron microscopy Multiwalled nanotube Magnetic separation Morphology Preparation Pyrrole polymer |
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| Snippet | In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3O4 nanoparticles was chemically synthesized and applied as a novel... In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe 3 O 4 nanoparticles was chemically synthesized and applied as a novel... In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe3 O4 nanoparticles was chemically synthesized and applied as a novel... In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe sub(3)O sub(4) nanoparticles was chemically synthesized and applied as a... In this work, a polypyrrole/multiwalled carbon nanotubes composite decorated with Fe₃O₄nanoparticles was chemically synthesized and applied as a novel... |
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| SubjectTerms | Adsorbents Adsorption Analysis Biological and medical sciences blood Carbon carbon nanotubes Chemical synthesis detection limit drugs Extraction General pharmacology Humans infrared spectroscopy Ion mobility Ion mobility spectrometry Ionic mobility Ionization Ions Magnetic nanoparticles Magnetite Nanoparticles - chemistry Medical sciences Methocarbamol Methocarbamol - blood Methocarbamol - chemistry Methocarbamol - isolation & purification Microscopy Multiwalled carbon nanotubes nanocomposites Nanoparticles Nanotubes Nanotubes, Carbon - chemistry Pharmacology. Drug treatments Plasma - chemistry Polymers - chemistry Polypyrrole Polypyrroles Pyrroles - chemistry scanning electron microscopy Solid Phase Extraction - instrumentation Solid Phase Extraction - methods Sorbents Spectrometry, Mass, Electrospray Ionization Spectroscopy Spectrum analysis transmission electron microscopy X-ray diffraction |
| Title | Extraction of methocarbamol from human plasma with a polypyrrole/multiwalled carbon nanotubes composite decorated with magnetic nanoparticles as an adsorbent followed by electrospray ionization ion mobility spectrometry detection |
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