Sealed rotors for in situ high temperature high pressure MAS NMR

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO 4 -5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biol...

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Published inChemical communications (Cambridge, England) Vol. 51; no. 70; pp. 13458 - 13461
Main Authors Hu, Jian Zhi, Hu, Mary Y., Zhao, Zhenchao, Xu, Suochang, Vjunov, Aleksei, Shi, Hui, Camaioni, Donald M., Peden, Charles H. F., Lercher, Johannes A.
Format Journal Article
LanguageEnglish
Published England Royal Society of Chemistry 01.01.2015
Subjects
Biological
chemical compounds
chemical reactions
Chemistry Techniques, Analytical - instrumentation
Crystallization
Dehydration
ENGINEERING
Environmental Molecular Sciences Laboratory
Hot Temperature
Magnetic Resonance Spectroscopy - instrumentation
MATERIALS SCIENCE
metabolomics
Molecular sieves
NMR spectroscopy
nuclear magnetic resonance spectroscopy
Pressure
Reusable
Rotors
temperature
Zirconium - chemistry
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Summary:Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO 4 -5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.
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AC05-76RL01830; AC06-76RL01830; NIEHS R01ES022176
PNNL-SA-110035
USDOE Office of Science (SC), Basic Energy Sciences (BES)
ISSN:1359-7345
1364-548X
1364-548X
DOI:10.1039/C5CC03910J