Microstructure of Spark Plasma-Sintered Silicon Nitride Ceramics

The microstructure and phase composition of the high-content Al 2 O 3 -Y 2 O 3 -doped spark plasma-sintered silicon nitride were investigated. Fully dense silicon nitride ceramics with a typical α-Si 3 N 4 equiaxed structure with average grain size from 200 to 530 nm, high elastic modulus of 288 GPa...

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Published inNanoscale research letters Vol. 12; no. 1; p. 293
Main Authors Lukianova, O. A., Novikov, V. Yu, Parkhomenko, A. A., Sirota, V. V., Krasilnikov, V. V.
Format Journal Article
LanguageEnglish
Published New York Springer US 24.04.2017
Springer Nature B.V
SpringerOpen
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Summary:The microstructure and phase composition of the high-content Al 2 O 3 -Y 2 O 3 -doped spark plasma-sintered silicon nitride were investigated. Fully dense silicon nitride ceramics with a typical α-Si 3 N 4 equiaxed structure with average grain size from 200 to 530 nm, high elastic modulus of 288 GPa, and high hardness of 2038 HV were spark plasma sintered (SPSed) at 1550 °C. Silicon nitride with elongated β-Si 3 N 4 grains, higher hardness of 1800 HV, density of 3.25 g/cm 3 , and Young’s modulus 300 GPa SPSed at 1650 °C was also reviewed.
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ISSN:1931-7573
1556-276X
DOI:10.1186/s11671-017-2067-z