Crystal Structure of a Methanesulfonate Salt of 3-(N-Methyl)quinolinium Boronic Acid

A methanesulfonate salt of 3-(N-methyl)quinolinium boronic acid, [3-(N-Me)QnB(OH)2]CH3SO3, was structurally determined by X-ray analysis. The boronic acid salt was crystalized as: P21/c, a = 8.57927(17), b = 6.99494(16), c = 21.0760(4)Å, β = 99.4787(19)°, Z = 4, V = 1247.53(4)Å3. In the single cryst...

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Published inX-ray Structure Analysis Online Vol. 33; pp. 9 - 10
Main Authors TAKEYAMA, Tomoyuki, NAKAJIMA, Yuki, KATAGIRI, Kosuke, IWATSUKI, Satoshi
Format Journal Article
LanguageEnglish
Published Tokyo The Japan Society for Analytical Chemistry 2017
Japan Science and Technology Agency
Subjects
Crystal structure
Crystals
Hydrogen bonding
Single crystals
X ray analysis
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Summary:A methanesulfonate salt of 3-(N-methyl)quinolinium boronic acid, [3-(N-Me)QnB(OH)2]CH3SO3, was structurally determined by X-ray analysis. The boronic acid salt was crystalized as: P21/c, a = 8.57927(17), b = 6.99494(16), c = 21.0760(4)Å, β = 99.4787(19)°, Z = 4, V = 1247.53(4)Å3. In the single crystal, hydrogen-bonded 1D-array structures of asymmetric cation-anion units were observed.
ISSN:1883-3578
1883-3578
DOI:10.2116/xraystruct.33.9