Ag9GaSe6: high-pressure-induced Ag migration causes thermoelectric performance irreproducibility and elimination of such instability
The argyrodite Ag 9 GaSe 6 is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are believed to cause poor stability and performance irreproducibility, which was evidenced even after the 1 st measurement run. Herein, we de...
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| Published in | Nature communications Vol. 13; no. 1; pp. 2966 - 10 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Nature Publishing Group UK
27.05.2022
Nature Publishing Group Nature Portfolio |
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| Abstract | The argyrodite Ag
9
GaSe
6
is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are believed to cause poor stability and performance irreproducibility, which was evidenced even after the 1
st
measurement run. Herein, we demonstrate the abovementioned instability and irreproducibility are caused by standard thermoelectric sample hot-pressing procedure, during which high pressure promotes the 3-fold-coordinated Ag atoms migrate to 4-fold-coordinated sites with higher-chemical potentials. Such instability can be eliminated by a simple annealing treatment, driving the metastable Ag atoms back to the original sites with lower-chemical potentials as revealed by the valence band X-ray photoelectron chemical potential spectra and single crystal X-ray diffraction data. Furthermore, the hot-pressed-annealed samples exhibit great stability and TE property repeatability. Such a stability and repeatability has never been reported before. This discovery will give liquid-like materials great application potential.
The Ag
9
GaSe
6
is a high-efficient thermoelectric material yet suffers instability. Here, the authors demonstrate the instability is caused by the pressure-induced liquid-like Ag migration, which can be eliminated by a simple annealing treatment. |
|---|---|
| AbstractList | The argyrodite Ag
9
GaSe
6
is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are believed to cause poor stability and performance irreproducibility, which was evidenced even after the 1
st
measurement run. Herein, we demonstrate the abovementioned instability and irreproducibility are caused by standard thermoelectric sample hot-pressing procedure, during which high pressure promotes the 3-fold-coordinated Ag atoms migrate to 4-fold-coordinated sites with higher-chemical potentials. Such instability can be eliminated by a simple annealing treatment, driving the metastable Ag atoms back to the original sites with lower-chemical potentials as revealed by the valence band X-ray photoelectron chemical potential spectra and single crystal X-ray diffraction data. Furthermore, the hot-pressed-annealed samples exhibit great stability and TE property repeatability. Such a stability and repeatability has never been reported before. This discovery will give liquid-like materials great application potential.
The Ag
9
GaSe
6
is a high-efficient thermoelectric material yet suffers instability. Here, the authors demonstrate the instability is caused by the pressure-induced liquid-like Ag migration, which can be eliminated by a simple annealing treatment. The argyrodite Ag 9 GaSe 6 is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are believed to cause poor stability and performance irreproducibility, which was evidenced even after the 1 st measurement run. Herein, we demonstrate the abovementioned instability and irreproducibility are caused by standard thermoelectric sample hot-pressing procedure, during which high pressure promotes the 3-fold-coordinated Ag atoms migrate to 4-fold-coordinated sites with higher-chemical potentials. Such instability can be eliminated by a simple annealing treatment, driving the metastable Ag atoms back to the original sites with lower-chemical potentials as revealed by the valence band X-ray photoelectron chemical potential spectra and single crystal X-ray diffraction data. Furthermore, the hot-pressed-annealed samples exhibit great stability and TE property repeatability. Such a stability and repeatability has never been reported before. This discovery will give liquid-like materials great application potential. The argyrodite Ag9GaSe6 is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are believed to cause poor stability and performance irreproducibility, which was evidenced even after the 1st measurement run. Herein, we demonstrate the abovementioned instability and irreproducibility are caused by standard thermoelectric sample hot-pressing procedure, during which high pressure promotes the 3-fold-coordinated Ag atoms migrate to 4-fold-coordinated sites with higher-chemical potentials. Such instability can be eliminated by a simple annealing treatment, driving the metastable Ag atoms back to the original sites with lower-chemical potentials as revealed by the valence band X-ray photoelectron chemical potential spectra and single crystal X-ray diffraction data. Furthermore, the hot-pressed-annealed samples exhibit great stability and TE property repeatability. Such a stability and repeatability has never been reported before. This discovery will give liquid-like materials great application potential.The argyrodite Ag9GaSe6 is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are believed to cause poor stability and performance irreproducibility, which was evidenced even after the 1st measurement run. Herein, we demonstrate the abovementioned instability and irreproducibility are caused by standard thermoelectric sample hot-pressing procedure, during which high pressure promotes the 3-fold-coordinated Ag atoms migrate to 4-fold-coordinated sites with higher-chemical potentials. Such instability can be eliminated by a simple annealing treatment, driving the metastable Ag atoms back to the original sites with lower-chemical potentials as revealed by the valence band X-ray photoelectron chemical potential spectra and single crystal X-ray diffraction data. Furthermore, the hot-pressed-annealed samples exhibit great stability and TE property repeatability. Such a stability and repeatability has never been reported before. This discovery will give liquid-like materials great application potential. The argyrodite Ag9GaSe6 is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are believed to cause poor stability and performance irreproducibility, which was evidenced even after the 1st measurement run. Herein, we demonstrate the abovementioned instability and irreproducibility are caused by standard thermoelectric sample hot-pressing procedure, during which high pressure promotes the 3-fold-coordinated Ag atoms migrate to 4-fold-coordinated sites with higher-chemical potentials. Such instability can be eliminated by a simple annealing treatment, driving the metastable Ag atoms back to the original sites with lower-chemical potentials as revealed by the valence band X-ray photoelectron chemical potential spectra and single crystal X-ray diffraction data. Furthermore, the hot-pressed-annealed samples exhibit great stability and TE property repeatability. Such a stability and repeatability has never been reported before. This discovery will give liquid-like materials great application potential.The Ag9GaSe6 is a high-efficient thermoelectric material yet suffers instability. Here, the authors demonstrate the instability is caused by the pressure-induced liquid-like Ag migration, which can be eliminated by a simple annealing treatment. The Ag9GaSe6 is a high-efficient thermoelectric material yet suffers instability. Here, the authors demonstrate the instability is caused by the pressure-induced liquid-like Ag migration, which can be eliminated by a simple annealing treatment. |
| ArticleNumber | 2966 |
| Author | Wu, Li-Ming Liu, Jing-Yuan Chen, Ling |
| Author_xml | – sequence: 1 givenname: Jing-Yuan orcidid: 0000-0001-8259-9456 surname: Liu fullname: Liu, Jing-Yuan organization: Beijing Key Laboratory of Energy Conversion and Storage Materials, College of Chemistry, Beijing Normal University – sequence: 2 givenname: Ling orcidid: 0000-0002-3693-4193 surname: Chen fullname: Chen, Ling email: chenl@bnu.edu.cn organization: Beijing Key Laboratory of Energy Conversion and Storage Materials, College of Chemistry, Beijing Normal University, Center for Advanced Materials Research, Advanced Institute of Natural Sciences, Beijing Normal University – sequence: 3 givenname: Li-Ming orcidid: 0000-0001-8390-2138 surname: Wu fullname: Wu, Li-Ming email: wlm@bnu.edu.cn organization: Beijing Key Laboratory of Energy Conversion and Storage Materials, College of Chemistry, Beijing Normal University, Center for Advanced Materials Research, Advanced Institute of Natural Sciences, Beijing Normal University |
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| Snippet | The argyrodite Ag
9
GaSe
6
is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms... The argyrodite Ag9GaSe6 is a newly recognized high-efficiency thermoelectric material with an ultralow thermal conductivity; however, liquid-like Ag atoms are... The Ag9GaSe6 is a high-efficient thermoelectric material yet suffers instability. Here, the authors demonstrate the instability is caused by the... |
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| SubjectTerms | 639/301 639/301/299/2736 Annealing Chemical potential Heat conductivity High pressure Humanities and Social Sciences Instability multidisciplinary Photoelectrons Pressure Reproducibility Science Science (multidisciplinary) Single crystals Stability Thermal conductivity Thermoelectric materials Thermoelectricity Valence band X-ray diffraction |
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| Title | Ag9GaSe6: high-pressure-induced Ag migration causes thermoelectric performance irreproducibility and elimination of such instability |
| URI | https://link.springer.com/article/10.1038/s41467-022-30716-7 https://www.proquest.com/docview/2670513886 https://www.proquest.com/docview/2671275952 https://pubmed.ncbi.nlm.nih.gov/PMC9142491 https://doaj.org/article/5ffe5ffdf6714624a8b213c4b38fefcc |
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