An overview of sample preparation and extraction of synthetic pyrethroids from water, sediment and soil

• Published in: Journal of Chromatography A Vol. 1217; no. 35; pp. 5537 - 5554
• Main Authors: Albaseer, Saeed S., Nageswara Rao, R., Swamy, Y.V., Mukkanti, K.
• Format: Journal Article
• Language: English
• Published: Amsterdam Elsevier B.V 27.08.2010; Amsterdam; New York: Elsevier; Elsevier
• Subjects: Analysis methods; Analytical chemistry; Applied sciences; Chemical Fractionation - instrumentation; Chemical Fractionation - methods; Chemistry; Chromatographic methods and physical methods associated with chromatography; Exact sciences and technology; Extraction; Gas chromatographic methods; Geologic Sediments - analysis; Natural water pollution; Other chromatographic methods; Pesticides; Pesticides - analysis; Pesticides - chemical synthesis; Pesticides - isolation & purification; Pollution; Pyrethrins - analysis; Pyrethrins - chemical synthesis; Pyrethrins - isolation & purification; Sample preparation; Sediment and soil; Soil and sediments pollution; Soil Pollutants - analysis; Soil Pollutants - chemical synthesis; Soil Pollutants - isolation & purification; Synthetic pyrethroids; Water; Water Pollutants, Chemical - analysis; Water Pollutants, Chemical - chemical synthesis; Water Pollutants, Chemical - isolation & purification; Water treatment and pollution; Water; NPD; PLE; SD; SFC; Sample preparation; MDL; C8; HWE; Extraction; GC; FID; LOD; SWE; DOM; Synthetic pyrethroids; EI; DAD; PTFE; ECD; Pesticides; ESI-MS; C18; DCM; LOQ; RP-HPLC; Sediment and soil; DVB; PA; NCI-MS; PE; SIM; Kd; PDMS; Chemical analysis; Insecticide; HPLC chromatography; Pyrethroids; Review; Soil pollution; Sediments; Gas chromatography; Soils; Water pollution
• ISSN: 0021-9673; 1873-3778
• DOI: 10.1016/j.chroma.2010.06.058

The latest developments in sample preparation and extraction of synthetic pyrethroids from environmental matrices viz., water, sediment and soil were reviewed. Though the synthetic pyrethroids were launched in 1970s, to the best of authors’ knowledge there was no review on this subject until date. The present status and recent advances made during the last 10 years in sample preparation including conservation and extraction techniques used in determination of synthetic pyrethroids in water, sediment and soil were discussed. Pre- and post-extraction treatments, sample stability during extraction and its influence upon the whole process of analytical determination were covered. Relative merits and demerits including the green aspects of extraction were evaluated. The current trends and future prospects were also addressed.