First enantioseparation and circular dichroism spectra of Au38 clusters protected by achiral ligands
Bestowing chirality to metals is central in fields such as heterogeneous catalysis and modern optics. Although the bulk phase of metals is symmetric, their surfaces can become chiral through adsorption of molecules. Interestingly, even achiral molecules can lead to locally chiral, though globally ra...
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| Published in | Nature communications Vol. 3; no. 1; p. 798 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
24.04.2012
Nature Publishing Group Nature Pub. Group |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Bestowing chirality to metals is central in fields such as heterogeneous catalysis and modern optics. Although the bulk phase of metals is symmetric, their surfaces can become chiral through adsorption of molecules. Interestingly, even achiral molecules can lead to locally chiral, though globally racemic, surfaces. A similar situation can be obtained for metal particles or clusters. Here we report the first separation of the enantiomers of a gold cluster protected by achiral thiolates, Au
38
(SCH
2
CH
2
Ph)
24
, achieved by chiral high-performance liquid chromatography. The chirality of the nanocluster arises from the chiral arrangement of the thiolates on its surface, forming 'staple motifs'. The enantiomers show mirror-image circular dichroism responses and large anisotropy factors of up to 4×10
−3
. Comparison with reported circular dichroism spectra of other Au
38
clusters reveals that the influence of the ligand on the chiroptical properties is minor.
Clusters of gold atoms protected with achiral thiolates can display chirality, and such chiral nanoparticles could open new possibilities in catalysis and sensing. Here, the first separation of the enantiomers of a gold cluster, protected by achiral thiolates, Au
38
(SCH
2
CH
2
Ph)
24
, is achieved. |
|---|---|
| AbstractList | Bestowing chirality to metals is central in fields such as heterogeneous catalysis and modern optics. Although the bulk phase of metals is symmetric, their surfaces can become chiral through adsorption of molecules. Interestingly, even achiral molecules can lead to locally chiral, though globally racemic, surfaces. A similar situation can be obtained for metal particles or clusters. Here we report the first separation of the enantiomers of a gold cluster protected by achiral thiolates, Au(38)(SCH(2)CH(2)Ph)(24), achieved by chiral high-performance liquid chromatography. The chirality of the nanocluster arises from the chiral arrangement of the thiolates on its surface, forming 'staple motifs'. The enantiomers show mirror-image circular dichroism responses and large anisotropy factors of up to 4×10(-3). Comparison with reported circular dichroism spectra of other Au(38) clusters reveals that the influence of the ligand on the chiroptical properties is minor.Bestowing chirality to metals is central in fields such as heterogeneous catalysis and modern optics. Although the bulk phase of metals is symmetric, their surfaces can become chiral through adsorption of molecules. Interestingly, even achiral molecules can lead to locally chiral, though globally racemic, surfaces. A similar situation can be obtained for metal particles or clusters. Here we report the first separation of the enantiomers of a gold cluster protected by achiral thiolates, Au(38)(SCH(2)CH(2)Ph)(24), achieved by chiral high-performance liquid chromatography. The chirality of the nanocluster arises from the chiral arrangement of the thiolates on its surface, forming 'staple motifs'. The enantiomers show mirror-image circular dichroism responses and large anisotropy factors of up to 4×10(-3). Comparison with reported circular dichroism spectra of other Au(38) clusters reveals that the influence of the ligand on the chiroptical properties is minor. Bestowing chirality to metals is central in fields such as heterogeneous catalysis and modern optics. Although the bulk phase of metals is symmetric, their surfaces can become chiral through adsorption of molecules. Interestingly, even achiral molecules can lead to locally chiral, though globally racemic, surfaces. A similar situation can be obtained for metal particles or clusters. Here we report the first separation of the enantiomers of a gold cluster protected by achiral thiolates, Au 38 (SCH 2 CH 2 Ph) 24 , achieved by chiral high-performance liquid chromatography. The chirality of the nanocluster arises from the chiral arrangement of the thiolates on its surface, forming 'staple motifs'. The enantiomers show mirror-image circular dichroism responses and large anisotropy factors of up to 4×10 −3 . Comparison with reported circular dichroism spectra of other Au 38 clusters reveals that the influence of the ligand on the chiroptical properties is minor. Clusters of gold atoms protected with achiral thiolates can display chirality, and such chiral nanoparticles could open new possibilities in catalysis and sensing. Here, the first separation of the enantiomers of a gold cluster, protected by achiral thiolates, Au 38 (SCH 2 CH 2 Ph) 24 , is achieved. Bestowing chirality to metals is central in fields such as heterogeneous catalysis and modern optics. Although the bulk phase of metals is symmetric, their surfaces can become chiral through adsorption of molecules. Interestingly, even achiral molecules can lead to locally chiral, though globally racemic, surfaces. A similar situation can be obtained for metal particles or clusters. Here we report the first separation of the enantiomers of a gold cluster protected by achiral thiolates, Au(38)(SCH(2)CH(2)Ph)(24), achieved by chiral high-performance liquid chromatography. The chirality of the nanocluster arises from the chiral arrangement of the thiolates on its surface, forming 'staple motifs'. The enantiomers show mirror-image circular dichroism responses and large anisotropy factors of up to 4×10(-3). Comparison with reported circular dichroism spectra of other Au(38) clusters reveals that the influence of the ligand on the chiroptical properties is minor. Bestowing chirality to metals is central in fields such as heterogeneous catalysis and modern optics. Although the bulk phase of metals is symmetric, their surfaces can become chiral through adsorption of molecules. Interestingly, even achiral molecules can lead to locally chiral, though globally racemic, surfaces. A similar situation can be obtained for metal particles or clusters. Here we report the first separation of the enantiomers of a gold cluster protected by achiral thiolates, Au38 (SCH2 CH2 Ph)24 , achieved by chiral high-performance liquid chromatography. The chirality of the nanocluster arises from the chiral arrangement of the thiolates on its surface, forming 'staple motifs'. The enantiomers show mirror-image circular dichroism responses and large anisotropy factors of up to 4×10-3 . Comparison with reported circular dichroism spectra of other Au38 clusters reveals that the influence of the ligand on the chiroptical properties is minor. |
| ArticleNumber | 798 |
| Author | Knoppe, Stefan Bürgi, Thomas Dolamic, Igor Dass, Amala |
| Author_xml | – sequence: 1 givenname: Igor surname: Dolamic fullname: Dolamic, Igor organization: Département de Chimie Physique, Université de Genève – sequence: 2 givenname: Stefan surname: Knoppe fullname: Knoppe, Stefan organization: Département de Chimie Physique, Université de Genève – sequence: 3 givenname: Amala surname: Dass fullname: Dass, Amala organization: Department of Chemistry and Biochemistry, University of Mississippi – sequence: 4 givenname: Thomas surname: Bürgi fullname: Bürgi, Thomas email: Thomas.Buergi@unige.ch organization: Département de Chimie Physique, Université de Genève |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/22531183$$D View this record in MEDLINE/PubMed |
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| Title | First enantioseparation and circular dichroism spectra of Au38 clusters protected by achiral ligands |
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