Superior adsorption of phosphate by ferrihydrite-coated and lanthanum-decorated magnetite
[Display omitted] Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its synthesis, natural magnetite (Mag), Fe3O4, was subjected to partial dissolution in HCl solution and the obtained suspension was...
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| Published in | Journal of colloid and interface science Vol. 530; pp. 704 - 713 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier Inc
15.11.2018
|
| Subjects | |
| Online Access | Get full text |
| ISSN | 0021-9797 1095-7103 1095-7103 |
| DOI | 10.1016/j.jcis.2018.07.025 |
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| Abstract | [Display omitted]
Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its synthesis, natural magnetite (Mag), Fe3O4, was subjected to partial dissolution in HCl solution and the obtained suspension was mixed with an alkaline solution for in-situ synthesis of ferrihydrite (Fh)-coated Mag (Mag@Fh). Mag@Fh was then decorated with La (hydr)oxides followed by calcination to produce Fh-coated and La-decorated Mag (Mag@Fh-La). Obtained Mag@Fh-La represented high phosphate adsorption capacity (44.8 mg P/g at 15.7% La in its structure) and La usage efficiency. Moreover, Mag@Fh-La retained its high adsorption capacity (>35.0 mg P/g) over a wide range of equilibrium solution pH (3.2–10.7). The combination of FTIR, XPS analysis and adsorption experiments revealed that ligand exchange and electrostatic attraction were the main mechanisms that jointly facilitated the adsorption of phosphate. Adsorption-desorption cycle studies confirmed the well-retained adsorption efficiency of regenerated Mag@Fh-La for repeated applications. Final experiments with real domestic wastewater (initial phosphate concentration of 1.7 mg/L) revealed that 0.2 g/L Mag@Fh-La efficiently reduced the phosphate concentration to below 0.02 mg/L. Overall, this work clearly highlights that the synthesized novel adsorbent has promising applications in phosphate removal from real wastewater. |
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| AbstractList | Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its synthesis, natural magnetite (Mag), Fe₃O₄, was subjected to partial dissolution in HCl solution and the obtained suspension was mixed with an alkaline solution for in-situ synthesis of ferrihydrite (Fh)-coated Mag (Mag@Fh). Mag@Fh was then decorated with La (hydr)oxides followed by calcination to produce Fh-coated and La-decorated Mag (Mag@Fh-La). Obtained Mag@Fh-La represented high phosphate adsorption capacity (44.8 mg P/g at 15.7% La in its structure) and La usage efficiency. Moreover, Mag@Fh-La retained its high adsorption capacity (>35.0 mg P/g) over a wide range of equilibrium solution pH (3.2–10.7). The combination of FTIR, XPS analysis and adsorption experiments revealed that ligand exchange and electrostatic attraction were the main mechanisms that jointly facilitated the adsorption of phosphate. Adsorption-desorption cycle studies confirmed the well-retained adsorption efficiency of regenerated Mag@Fh-La for repeated applications. Final experiments with real domestic wastewater (initial phosphate concentration of 1.7 mg/L) revealed that 0.2 g/L Mag@Fh-La efficiently reduced the phosphate concentration to below 0.02 mg/L. Overall, this work clearly highlights that the synthesized novel adsorbent has promising applications in phosphate removal from real wastewater. Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its synthesis, natural magnetite (Mag), Fe O , was subjected to partial dissolution in HCl solution and the obtained suspension was mixed with an alkaline solution for in-situ synthesis of ferrihydrite (Fh)-coated Mag (Mag@Fh). Mag@Fh was then decorated with La (hydr)oxides followed by calcination to produce Fh-coated and La-decorated Mag (Mag@Fh-La). Obtained Mag@Fh-La represented high phosphate adsorption capacity (44.8 mg P/g at 15.7% La in its structure) and La usage efficiency. Moreover, Mag@Fh-La retained its high adsorption capacity (>35.0 mg P/g) over a wide range of equilibrium solution pH (3.2-10.7). The combination of FTIR, XPS analysis and adsorption experiments revealed that ligand exchange and electrostatic attraction were the main mechanisms that jointly facilitated the adsorption of phosphate. Adsorption-desorption cycle studies confirmed the well-retained adsorption efficiency of regenerated Mag@Fh-La for repeated applications. Final experiments with real domestic wastewater (initial phosphate concentration of 1.7 mg/L) revealed that 0.2 g/L Mag@Fh-La efficiently reduced the phosphate concentration to below 0.02 mg/L. Overall, this work clearly highlights that the synthesized novel adsorbent has promising applications in phosphate removal from real wastewater. Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its synthesis, natural magnetite (Mag), Fe3O4, was subjected to partial dissolution in HCl solution and the obtained suspension was mixed with an alkaline solution for in-situ synthesis of ferrihydrite (Fh)-coated Mag (Mag@Fh). Mag@Fh was then decorated with La (hydr)oxides followed by calcination to produce Fh-coated and La-decorated Mag (Mag@Fh-La). Obtained Mag@Fh-La represented high phosphate adsorption capacity (44.8 mg P/g at 15.7% La in its structure) and La usage efficiency. Moreover, Mag@Fh-La retained its high adsorption capacity (>35.0 mg P/g) over a wide range of equilibrium solution pH (3.2-10.7). The combination of FTIR, XPS analysis and adsorption experiments revealed that ligand exchange and electrostatic attraction were the main mechanisms that jointly facilitated the adsorption of phosphate. Adsorption-desorption cycle studies confirmed the well-retained adsorption efficiency of regenerated Mag@Fh-La for repeated applications. Final experiments with real domestic wastewater (initial phosphate concentration of 1.7 mg/L) revealed that 0.2 g/L Mag@Fh-La efficiently reduced the phosphate concentration to below 0.02 mg/L. Overall, this work clearly highlights that the synthesized novel adsorbent has promising applications in phosphate removal from real wastewater.Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its synthesis, natural magnetite (Mag), Fe3O4, was subjected to partial dissolution in HCl solution and the obtained suspension was mixed with an alkaline solution for in-situ synthesis of ferrihydrite (Fh)-coated Mag (Mag@Fh). Mag@Fh was then decorated with La (hydr)oxides followed by calcination to produce Fh-coated and La-decorated Mag (Mag@Fh-La). Obtained Mag@Fh-La represented high phosphate adsorption capacity (44.8 mg P/g at 15.7% La in its structure) and La usage efficiency. Moreover, Mag@Fh-La retained its high adsorption capacity (>35.0 mg P/g) over a wide range of equilibrium solution pH (3.2-10.7). The combination of FTIR, XPS analysis and adsorption experiments revealed that ligand exchange and electrostatic attraction were the main mechanisms that jointly facilitated the adsorption of phosphate. Adsorption-desorption cycle studies confirmed the well-retained adsorption efficiency of regenerated Mag@Fh-La for repeated applications. Final experiments with real domestic wastewater (initial phosphate concentration of 1.7 mg/L) revealed that 0.2 g/L Mag@Fh-La efficiently reduced the phosphate concentration to below 0.02 mg/L. Overall, this work clearly highlights that the synthesized novel adsorbent has promising applications in phosphate removal from real wastewater. [Display omitted] Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its synthesis, natural magnetite (Mag), Fe3O4, was subjected to partial dissolution in HCl solution and the obtained suspension was mixed with an alkaline solution for in-situ synthesis of ferrihydrite (Fh)-coated Mag (Mag@Fh). Mag@Fh was then decorated with La (hydr)oxides followed by calcination to produce Fh-coated and La-decorated Mag (Mag@Fh-La). Obtained Mag@Fh-La represented high phosphate adsorption capacity (44.8 mg P/g at 15.7% La in its structure) and La usage efficiency. Moreover, Mag@Fh-La retained its high adsorption capacity (>35.0 mg P/g) over a wide range of equilibrium solution pH (3.2–10.7). The combination of FTIR, XPS analysis and adsorption experiments revealed that ligand exchange and electrostatic attraction were the main mechanisms that jointly facilitated the adsorption of phosphate. Adsorption-desorption cycle studies confirmed the well-retained adsorption efficiency of regenerated Mag@Fh-La for repeated applications. Final experiments with real domestic wastewater (initial phosphate concentration of 1.7 mg/L) revealed that 0.2 g/L Mag@Fh-La efficiently reduced the phosphate concentration to below 0.02 mg/L. Overall, this work clearly highlights that the synthesized novel adsorbent has promising applications in phosphate removal from real wastewater. |
| Author | Yang, Yixuan Liu, Jing He, Hongping Fu, Haoyang Usman, Muhammad Chen, Qingze Zhu, Runliang |
| Author_xml | – sequence: 1 givenname: Haoyang surname: Fu fullname: Fu, Haoyang organization: CAS Key Laboratory of Mineralogy and Metallogeny/Guangdong Provincial Key Laboratory of Mineral Physics and Material, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China – sequence: 2 givenname: Yixuan surname: Yang fullname: Yang, Yixuan organization: CAS Key Laboratory of Mineralogy and Metallogeny/Guangdong Provincial Key Laboratory of Mineral Physics and Material, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China – sequence: 3 givenname: Runliang surname: Zhu fullname: Zhu, Runliang email: zhurl@gig.ac.cn organization: CAS Key Laboratory of Mineralogy and Metallogeny/Guangdong Provincial Key Laboratory of Mineral Physics and Material, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China – sequence: 4 givenname: Jing surname: Liu fullname: Liu, Jing organization: CAS Key Laboratory of Mineralogy and Metallogeny/Guangdong Provincial Key Laboratory of Mineral Physics and Material, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China – sequence: 5 givenname: Muhammad surname: Usman fullname: Usman, Muhammad organization: Environmental Mineralogy, Center for Applied Geosciences, University of Tübingen, 72074 Tübingen, Germany – sequence: 6 givenname: Qingze surname: Chen fullname: Chen, Qingze organization: CAS Key Laboratory of Mineralogy and Metallogeny/Guangdong Provincial Key Laboratory of Mineral Physics and Material, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China – sequence: 7 givenname: Hongping orcidid: 0000-0002-7057-7687 surname: He fullname: He, Hongping organization: CAS Key Laboratory of Mineralogy and Metallogeny/Guangdong Provincial Key Laboratory of Mineral Physics and Material, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30015156$$D View this record in MEDLINE/PubMed |
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| Keywords | Ferrihydrite Natural magnetite Lanthanum Adsorption Phosphate |
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Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from... Present study reports the successful development of a novel lanthanum (La)-based magnetic adsorbent and its use for phosphate removal from water. For its... |
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| SubjectTerms | adsorbents Adsorption electrostatic interactions Ferrihydrite Fourier transform infrared spectroscopy hydrochloric acid Lanthanum ligands magnetism magnetite municipal wastewater Natural magnetite Phosphate phosphates X-ray photoelectron spectroscopy |
| Title | Superior adsorption of phosphate by ferrihydrite-coated and lanthanum-decorated magnetite |
| URI | https://dx.doi.org/10.1016/j.jcis.2018.07.025 https://www.ncbi.nlm.nih.gov/pubmed/30015156 https://www.proquest.com/docview/2071562812 https://www.proquest.com/docview/2116863410 |
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