Mechanochemical solvent-free and catalyst-free one-pot synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones with quantitative yields

Solvent-free synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones by ball-milling and without any catalyst is described. This method provides several advantages such as being environmentally friendly, using a simple workup procedure, and affording high yields.

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Bibliographic Details
Published inMolecules (Basel, Switzerland) Vol. 14; no. 1; pp. 474 - 479
Main Authors Mashkouri, Sara, Naimi-Jamal, M Reza
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 19.01.2009
Molecular Diversity Preservation International
Subjects
Acids
Aldehydes
Aldehydes - chemistry
Ball-milling
Barbiturates - chemistry
Barbituric acid
Chemistry
Combinatorial Chemistry Techniques
Condensation
Heterocyclic compounds
Molecular Structure
Nitriles - chemistry
Pyrimidinediones
Pyrimidines - chemical synthesis
Pyrimidines - chemistry
Solvent-free reaction
Solvents
Stainless steel
Temperature
Iran
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Summary:Solvent-free synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones by ball-milling and without any catalyst is described. This method provides several advantages such as being environmentally friendly, using a simple workup procedure, and affording high yields.
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SourceType-Scholarly Journals-1
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ISSN:1420-3049
1420-3049
DOI:10.3390/molecules14010474