Single drop microextraction—Development, applications and future trends
Single drop microextraction (SDME) has emerged over the last 10–15 years as one of the simplest and most easily implemented forms of micro-scale sample cleanup and preconcentration. In the most common arrangement, an ordinary chromatography syringe is used to suspend microliter quantities of extract...
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Published in | Journal of Chromatography A Vol. 1217; no. 16; pp. 2326 - 2336 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
Netherlands
Elsevier B.V
16.04.2010
Amsterdam; New York: Elsevier |
Subjects | |
Online Access | Get full text |
ISSN | 0021-9673 1873-3778 |
DOI | 10.1016/j.chroma.2009.10.089 |
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Abstract | Single drop microextraction (SDME) has emerged over the last 10–15 years as one of the simplest and most easily implemented forms of micro-scale sample cleanup and preconcentration. In the most common arrangement, an ordinary chromatography syringe is used to suspend microliter quantities of extracting solvent either directly immersed in the sample, or in the headspace above the sample. The same syringe is then used to introduce the solvent and extracted analytes into the chromatography system for identification and/or quantitation. This review article summarizes the historical development and various modes of the technique, some theoretical and practical aspects, recent trends and selected applications. |
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AbstractList | Single drop microextraction (SDME) has emerged over the last 10-15 years as one of the simplest and most easily implemented forms of micro-scale sample cleanup and preconcentration. In the most common arrangement, an ordinary chromatography syringe is used to suspend microliter quantities of extracting solvent either directly immersed in the sample, or in the headspace above the sample. The same syringe is then used to introduce the solvent and extracted analytes into the chromatography system for identification and/or quantitation. This review article summarizes the historical development and various modes of the technique, some theoretical and practical aspects, recent trends and selected applications. |
Author | Kokosa, John M. Jeannot, Michael A. Przyjazny, Andrzej |
Author_xml | – sequence: 1 givenname: Michael A. surname: Jeannot fullname: Jeannot, Michael A. email: mjeannot@stcloudstate.edu organization: Department of Chemistry, St. Cloud State University, 366 Wick Science Building, 720 4th Ave. S., St. Cloud, MN 56301-4498, USA – sequence: 2 givenname: Andrzej surname: Przyjazny fullname: Przyjazny, Andrzej email: aprzyjaz@kettering.edu organization: Department of Chemistry & Biochemistry, Kettering University, Flint, MI 48504 USA – sequence: 3 givenname: John M. surname: Kokosa fullname: Kokosa, John M. email: jmkokosa@yahoo.com organization: MDRC Consulting/Mott Community College, Flint, MI 48503 USA |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/19932482$$D View this record in MEDLINE/PubMed |
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Keywords | Solvent microextraction Single drop microextraction Liquid-phase microextraction |
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PublicationTitle | Journal of Chromatography A |
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Snippet | Single drop microextraction (SDME) has emerged over the last 10–15 years as one of the simplest and most easily implemented forms of micro-scale sample cleanup... Single drop microextraction (SDME) has emerged over the last 10-15 years as one of the simplest and most easily implemented forms of micro-scale sample cleanup... |
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SubjectTerms | Chemical Fractionation - instrumentation Chemical Fractionation - methods chromatography Forecasting headspace analysis Liquid-phase microextraction microextraction Osmolar Concentration Single drop microextraction Solvent microextraction solvents Solvents - chemistry Temperature |
Title | Single drop microextraction—Development, applications and future trends |
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