Palladium‐Loaded Cucurbit[7]uril‐Modified Iron Oxide Nanoparticles for C−C Cross‐Coupling Reactions

Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano‐catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki–Miyaura, Sonogashira, and Mizoroki–Heck cross‐coupling reactions. Reactions were run in environmentally benign 1:1 ethanol/water...

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Published inChemistry : a European journal Vol. 24; no. 10; pp. 2349 - 2353
Main Authors Benyettou, Farah, Motte, Laurence, Traboulsi, Hassan, Mazher, Javed, Pasricha, Renu, Olsen, John‐Carl, Trabolsi, Ali, Guenin, Erwan
Format Journal Article
LanguageEnglish
Published Germany Wiley Subscription Services, Inc 16.02.2018
Wiley-VCH Verlag
Subjects
Aerobic conditions
Catalysis
Catalysts
Chemical and Process Engineering
Chemical reactions
Chemistry
Coupling
Cross coupling
cross-coupling reactions
cucurbituril
Engineering Sciences
Environmental Engineering
Environmental Sciences
Ethanol
Iron oxides
macrocyclic chemistry
magnetic nano-catalyst
Nanoparticles
Palladium
palladium
magnetic nano-catalyst
cucurbituril
cross-coupling reactions
macrocyclic chemistry
Online AccessGet full text
ISSN0947-6539
1521-3765
DOI10.1002/chem.201705082

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Abstract Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano‐catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki–Miyaura, Sonogashira, and Mizoroki–Heck cross‐coupling reactions. Reactions were run in environmentally benign 1:1 ethanol/water solvent under convenient aerobic conditions. In a preliminary screening, conversions and yields were uniformly high with turn over frequencies (TOF) ranging from 64 to 7360 h−1. The nano‐catalysts could be recovered with a magnet and reused several times (6 times for Suzuki–Miayura reaction) without loss of activity. Cucurbit[7]uril modified iron‐oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano‐catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki–Miyaura, Sonogashira, and Mizoroki–Heck cross‐coupling reactions.
AbstractList Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano-catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki-Miyaura, Sonogashira, and Mizoroki-Heck cross-coupling reactions. Reactions were run in environmentally benign 1:1 ethanol/water solvent under convenient aerobic conditions. In a preliminary screening, conversions and yields were uniformly high with turn over frequencies (TOF) ranging from 64 to 7360 h . The nano-catalysts could be recovered with a magnet and reused several times (6 times for Suzuki-Miayura reaction) without loss of activity.
Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano-catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki-Miyaura, Sonogashira, and Mizoroki-Heck cross-coupling reactions. Reactions were run in environmentally benign 1:1 ethanol/water solvent under convenient aerobic conditions. In a preliminary screening, conversions and yields were uniformly high with turn over frequencies (TOF) ranging from 64 to 7360h-1. The nano-catalysts could be recovered with a magnet and reused several times (6times for Suzuki-Miayura reaction) without loss of activity.
Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano‐catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki–Miyaura, Sonogashira, and Mizoroki–Heck cross‐coupling reactions. Reactions were run in environmentally benign 1:1 ethanol/water solvent under convenient aerobic conditions. In a preliminary screening, conversions and yields were uniformly high with turn over frequencies (TOF) ranging from 64 to 7360 h−1. The nano‐catalysts could be recovered with a magnet and reused several times (6 times for Suzuki–Miayura reaction) without loss of activity. Cucurbit[7]uril modified iron‐oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano‐catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki–Miyaura, Sonogashira, and Mizoroki–Heck cross‐coupling reactions.
Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano‐catalysts (Pd@CB[7]NPs) that, with microwave heating, catalysed Suzuki–Miyaura, Sonogashira, and Mizoroki–Heck cross‐coupling reactions. Reactions were run in environmentally benign 1:1 ethanol/water solvent under convenient aerobic conditions. In a preliminary screening, conversions and yields were uniformly high with turn over frequencies (TOF) ranging from 64 to 7360 h −1 . The nano‐catalysts could be recovered with a magnet and reused several times (6 times for Suzuki–Miayura reaction) without loss of activity.
Author Mazher, Javed
Pasricha, Renu
Motte, Laurence
Guenin, Erwan
Trabolsi, Ali
Olsen, John‐Carl
Traboulsi, Hassan
Benyettou, Farah
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  email: erwann.guenin@utc.fr
  organization: Université Paris 13, Sorbonne Paris Cité
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Copyright 2018 Wiley‐VCH Verlag GmbH & Co. KGaA, Weinheim
2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim.
2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim
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Keywords palladium
magnetic nano-catalyst
cucurbituril
cross-coupling reactions
macrocyclic chemistry
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Snippet Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano‐catalysts (Pd@CB[7]NPs) that, with microwave heating,...
Cucurbit[7]uril modified iron oxide nanoparticles (CB[7]NPs) were loaded with palladium to form nano-catalysts (Pd@CB[7]NPs) that, with microwave heating,...
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StartPage 2349
SubjectTerms Aerobic conditions
Catalysis
Catalysts
Chemical and Process Engineering
Chemical reactions
Chemistry
Coupling
Cross coupling
cross-coupling reactions
cucurbituril
Engineering Sciences
Environmental Engineering
Environmental Sciences
Ethanol
Iron oxides
macrocyclic chemistry
magnetic nano-catalyst
Nanoparticles
Palladium
Title Palladium‐Loaded Cucurbit[7]uril‐Modified Iron Oxide Nanoparticles for C−C Cross‐Coupling Reactions
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fchem.201705082
https://www.ncbi.nlm.nih.gov/pubmed/29297954
https://www.proquest.com/docview/2002458886
https://hal.science/hal-02148522
Volume 24
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