Transient Microstructure Evolutions and Local Properties of Dual-Phase 980 MPa Grade Steel Via Friction Stir Spot Processing

• Published in: Materials Vol. 13; no. 19; p. 4406
• Main Authors: Taniguchi, Koichi, Lim, Yong Chae, Flores-Betancourt, Alexis, Feng, Zhili
• Format: Journal Article
• Language: English
• Published: Basel MDPI AG 02.10.2020; MDPI
• Subjects: advanced high-strength steel; Cameras; Ceramic tools; characterization; Deformation; Diamond pyramid hardness; Dual phase steels; Experiments; Friction stir processing; Friction stir welding; Grain boundaries; Grain refinement; Grain size; High strength steels; MATERIALS SCIENCE; Mechanical properties; Microstructure; microstructures; Nanoindentation; Plastic deformation; Recrystallization; Scanning electron microscopy; Shear strength; Silicon nitride; Steel; Temperature; Tempered martensite; Tensile strength; Yield stress; United States > US
• ISSN: 1996-1944; 1996-1944
• DOI: 10.3390/ma13194406

Friction stir processing is a novel solid-state process to modify microstructures and their properties by intense, localized plastic deformation. However, little research has been reported for microstructure evolutions of advanced high-strength steels during the process. The present work focuses on the study of transient microstructure changes and local mechanical properties for friction stir spot processed dual-phase (DP) 980 MPa grade steel (DP980) under different peak temperatures. A pinless silicon nitride ceramic tool was used to produce relatively simple material deformation and flow near the tool. Friction stir spot processed steel samples were characterized by optical and electron microscopies. Furthermore, Vickers microhardness and nano-indentation measurements were used to study local mechanical properties for correlation with microstructures. A swallow layer of refined grains (<0.6 µm) was obtained with a low peak temperature (under 400 °C), whereas higher peak temperatures (>Ac1) led to a change in grain size with different microstructures (fine-grained DP or martensite). Electron back-scattered diffraction characterizations revealed a large deformation in the as-received microstructures (mixture of ferrite and tempered martensite) induced by friction stir spot processing, leading to recrystallization and grain refinement around the stirred zone. Also, nano-indentation measurements showed a higher hardness than the hardness of the as-received DP980. Friction stir processing with different process conditions effectively changed microstructures and local mechanical properties.