Hydrophobic eutectic solvents for surface water treatment with a focus on benzophenone type UV filters

Effective removal of organic UV filters from aquatic environmental compartments and swimming waters is very important because these substances are hazardous to humans and wildlife at low concentrations and act as endocrine disruptors. Therefore, the aim of the present article is to determine the ext...

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Published in	Ecotoxicology and environmental safety Vol. 280; p. 116528
Main Authors	Hrabáková, Kateřina, Hložek, Tomáš, Bosáková, Zuzana, Tůma, Petr
Format	Journal Article
Language	English
Published	Netherlands Elsevier Inc 15.07.2024 Elsevier
Subjects	Benzophenone Benzophenones - chemistry Caprylates - chemistry Deep Eutectic Solvents - chemistry Hydrophobic and Hydrophilic Interactions Hydrophobic deep eutectic solvent Liquid chromatography Mass spectrometry Menthol - chemistry Solvent reuse Sunscreening Agents - chemistry Sunscreening Agents - toxicity Water Pollutants, Chemical - analysis Water Pollutants, Chemical - chemistry Water purification Water Purification - methods EE C10 Solvent reuse C12 BP-8 HBA Liquid chromatography BP-3 HBD HDES BP-2 L BP-1 M BP Benzophenone Hydrophobic deep eutectic solvent DES MOBP T C8 Water purification Mass spectrometry
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Abstract	Effective removal of organic UV filters from aquatic environmental compartments and swimming waters is very important because these substances are hazardous to humans and wildlife at low concentrations and act as endocrine disruptors. Therefore, the aim of the present article is to determine the extraction efficiencies of hydrophobic deep eutectic solvents (HDES) for the selected UV filters based on benzophenone structure (benzophenone, 2,4-dihydroxybenzophenone, 2,2´,4,4´-tetrahydroxybenzophenone, 2-hydroxy-4-methoxybenzophenone, 2,2´-dihydroxy-4-methoxybenzophenone, 4-methacryloxy-2-hydroxybenzophenone) from aqueous matrices. For this purpose, six HDESs based on dl-menthol in combination with caprylic, decanoic and lauric acid are prepared and compared with referent terpene solvents such as terpineol and linalool. The effect of various parameters such as HDES composition, volume ratio, frequency and shaking time are studied. The highest extraction efficiency is shown by HDES of menthol:caprylic acid (1:1) composition at the aqueous:organic phase volume ratio of 1:1, shaking frequency of 1500 rpm and shaking time of 15 min. The achieved extraction efficiencies are higher than 99.6 % for all benzophenones studied in the purification of stagnant pond water, swimming pool water and river water samples. After a simple and fast sample treatment, the residual levels of benzophenones in the waters are controlled by a newly developed sensitive HPLC-MS/MS method with LOQs in the range of 0.7 – 5.0 ng/mL. [Display omitted] •effective removal of benzophenone UV filters from swimming, river and pond water.•sensitive HPLC-MS/MS method with precise identification of benzophenones.•highest extraction efficiency for menthol:caprylic acid (1:1) as hydrophobic DES.•extraction efficiencies higher than 99.6 % for all benzophenones using DESs.•DESs repeatedly used for five extraction cycles with recovery higher than 95 %.
AbstractList	Effective removal of organic UV filters from aquatic environmental compartments and swimming waters is very important because these substances are hazardous to humans and wildlife at low concentrations and act as endocrine disruptors. Therefore, the aim of the present article is to determine the extraction efficiencies of hydrophobic deep eutectic solvents (HDES) for the selected UV filters based on benzophenone structure (benzophenone, 2,4-dihydroxybenzophenone, 2,2´,4,4´-tetrahydroxybenzophenone, 2-hydroxy-4-methoxybenzophenone, 2,2´-dihydroxy-4-methoxybenzophenone, 4-methacryloxy-2-hydroxybenzophenone) from aqueous matrices. For this purpose, six HDESs based on dl-menthol in combination with caprylic, decanoic and lauric acid are prepared and compared with referent terpene solvents such as terpineol and linalool. The effect of various parameters such as HDES composition, volume ratio, frequency and shaking time are studied. The highest extraction efficiency is shown by HDES of menthol:caprylic acid (1:1) composition at the aqueous:organic phase volume ratio of 1:1, shaking frequency of 1500 rpm and shaking time of 15 min. The achieved extraction efficiencies are higher than 99.6 % for all benzophenones studied in the purification of stagnant pond water, swimming pool water and river water samples. After a simple and fast sample treatment, the residual levels of benzophenones in the waters are controlled by a newly developed sensitive HPLC-MS/MS method with LOQs in the range of 0.7 – 5.0 ng/mL. [Display omitted] •effective removal of benzophenone UV filters from swimming, river and pond water.•sensitive HPLC-MS/MS method with precise identification of benzophenones.•highest extraction efficiency for menthol:caprylic acid (1:1) as hydrophobic DES.•extraction efficiencies higher than 99.6 % for all benzophenones using DESs.•DESs repeatedly used for five extraction cycles with recovery higher than 95 %. Effective removal of organic UV filters from aquatic environmental compartments and swimming waters is very important because these substances are hazardous to humans and wildlife at low concentrations and act as endocrine disruptors. Therefore, the aim of the present article is to determine the extraction efficiencies of hydrophobic deep eutectic solvents (HDES) for the selected UV filters based on benzophenone structure (benzophenone, 2,4-dihydroxybenzophenone, 2,2´,4,4´-tetrahydroxybenzophenone, 2-hydroxy-4-methoxybenzophenone, 2,2´-dihydroxy-4-methoxybenzophenone, 4-methacryloxy-2-hydroxybenzophenone) from aqueous matrices. For this purpose, six HDESs based on dl-menthol in combination with caprylic, decanoic and lauric acid are prepared and compared with referent terpene solvents such as terpineol and linalool. The effect of various parameters such as HDES composition, volume ratio, frequency and shaking time are studied. The highest extraction efficiency is shown by HDES of menthol:caprylic acid (1:1) composition at the aqueous:organic phase volume ratio of 1:1, shaking frequency of 1500 rpm and shaking time of 15 min. The achieved extraction efficiencies are higher than 99.6 % for all benzophenones studied in the purification of stagnant pond water, swimming pool water and river water samples. After a simple and fast sample treatment, the residual levels of benzophenones in the waters are controlled by a newly developed sensitive HPLC-MS/MS method with LOQs in the range of 0.7 - 5.0 ng/mL.Effective removal of organic UV filters from aquatic environmental compartments and swimming waters is very important because these substances are hazardous to humans and wildlife at low concentrations and act as endocrine disruptors. Therefore, the aim of the present article is to determine the extraction efficiencies of hydrophobic deep eutectic solvents (HDES) for the selected UV filters based on benzophenone structure (benzophenone, 2,4-dihydroxybenzophenone, 2,2´,4,4´-tetrahydroxybenzophenone, 2-hydroxy-4-methoxybenzophenone, 2,2´-dihydroxy-4-methoxybenzophenone, 4-methacryloxy-2-hydroxybenzophenone) from aqueous matrices. For this purpose, six HDESs based on dl-menthol in combination with caprylic, decanoic and lauric acid are prepared and compared with referent terpene solvents such as terpineol and linalool. The effect of various parameters such as HDES composition, volume ratio, frequency and shaking time are studied. The highest extraction efficiency is shown by HDES of menthol:caprylic acid (1:1) composition at the aqueous:organic phase volume ratio of 1:1, shaking frequency of 1500 rpm and shaking time of 15 min. The achieved extraction efficiencies are higher than 99.6 % for all benzophenones studied in the purification of stagnant pond water, swimming pool water and river water samples. After a simple and fast sample treatment, the residual levels of benzophenones in the waters are controlled by a newly developed sensitive HPLC-MS/MS method with LOQs in the range of 0.7 - 5.0 ng/mL. Effective removal of organic UV filters from aquatic environmental compartments and swimming waters is very important because these substances are hazardous to humans and wildlife at low concentrations and act as endocrine disruptors. Therefore, the aim of the present article is to determine the extraction efficiencies of hydrophobic deep eutectic solvents (HDES) for the selected UV filters based on benzophenone structure (benzophenone, 2,4-dihydroxybenzophenone, 2,2´,4,4´-tetrahydroxybenzophenone, 2-hydroxy-4-methoxybenzophenone, 2,2´-dihydroxy-4-methoxybenzophenone, 4-methacryloxy-2-hydroxybenzophenone) from aqueous matrices. For this purpose, six HDESs based on dl-menthol in combination with caprylic, decanoic and lauric acid are prepared and compared with referent terpene solvents such as terpineol and linalool. The effect of various parameters such as HDES composition, volume ratio, frequency and shaking time are studied. The highest extraction efficiency is shown by HDES of menthol:caprylic acid (1:1) composition at the aqueous:organic phase volume ratio of 1:1, shaking frequency of 1500 rpm and shaking time of 15 min. The achieved extraction efficiencies are higher than 99.6 % for all benzophenones studied in the purification of stagnant pond water, swimming pool water and river water samples. After a simple and fast sample treatment, the residual levels of benzophenones in the waters are controlled by a newly developed sensitive HPLC-MS/MS method with LOQs in the range of 0.7 – 5.0 ng/mL.
ArticleNumber	116528
Author	Tůma, Petr Bosáková, Zuzana Hrabáková, Kateřina Hložek, Tomáš
Author_xml	– sequence: 1 givenname: Kateřina surname: Hrabáková fullname: Hrabáková, Kateřina organization: Charles University, Faculty of Science, Department of Analytical Chemistry, Albertov 6, Prague 2 128 43, Czech Republic – sequence: 2 givenname: Tomáš surname: Hložek fullname: Hložek, Tomáš organization: Charles University, Third Faculty of Medicine, Department of Hygiene, Ruská 87, Prague 10 100 00, Czech Republic – sequence: 3 givenname: Zuzana surname: Bosáková fullname: Bosáková, Zuzana email: zuzana.bosakova@natur.cuni.cz organization: Charles University, Faculty of Science, Department of Analytical Chemistry, Albertov 6, Prague 2 128 43, Czech Republic – sequence: 4 givenname: Petr surname: Tůma fullname: Tůma, Petr email: petr.tuma@lf3.cuni.cz organization: Charles University, Third Faculty of Medicine, Department of Hygiene, Ruská 87, Prague 10 100 00, Czech Republic
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SubjectTerms	Benzophenone Benzophenones - chemistry Caprylates - chemistry Deep Eutectic Solvents - chemistry Hydrophobic and Hydrophilic Interactions Hydrophobic deep eutectic solvent Liquid chromatography Mass spectrometry Menthol - chemistry Solvent reuse Sunscreening Agents - chemistry Sunscreening Agents - toxicity Water Pollutants, Chemical - analysis Water Pollutants, Chemical - chemistry Water purification Water Purification - methods
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Title	Hydrophobic eutectic solvents for surface water treatment with a focus on benzophenone type UV filters
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