Studies on Pilocereine and Related Compounds. VI. Synthesis of O-Methylisopilocereine. (3)

Base (Ib) was synthesized by the Ullmann condensation between VII and VIII, and the two racemic diastereomers were obtained in crystalline states. One of them was proved to be O-methylisopilocereine, while the other was identified with the diastereomer obtained by another synthetic method. Non-ident...

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Bibliographic Details
Published inChemical & pharmaceutical bulletin Vol. 11; no. 12; pp. 1500 - 1503
Main Author Bessho, Kiyoshi
Format Journal Article
LanguageEnglish
Published Japan The Pharmaceutical Society of Japan 1963
Subjects
Alkaloids
Chemistry, Pharmaceutical
Old Medline
Spectrum Analysis
CHEMISTRY, PHARMACEUTICAL
SPECTRUM ANALYSIS
EXPERIMENTAL LAB STUDY
ALKALOIDS
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Summary:Base (Ib) was synthesized by the Ullmann condensation between VII and VIII, and the two racemic diastereomers were obtained in crystalline states. One of them was proved to be O-methylisopilocereine, while the other was identified with the diastereomer obtained by another synthetic method. Non-identities of them with O-methylpilocereine, to which the formula (Ib) had been inadequately assigned, were also proved.
Bibliography:ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 23
ISSN:0009-2363
1347-5223
DOI:10.1248/cpb.11.1500