Crystal structure of (4-hy-droxy-piperidin-1-yl)[4-(tri-fluoro-meth-yl)phen-yl]methanone

The title compound, C13H14NO2F3, crystallises with two mol-ecules, A and B, in the asymmetric unit, with similar conformations. The dihedral angles between the piperidine and phenyl rings are 83.76 (2) and 75.23 (2)° in mol-ecules A and B, respectively. The bond-angle sums around the N atoms [359.1...

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Bibliographic Details
Published inActa crystallographica. Section E, Crystallographic communications Vol. 71; no. Pt 10; pp. o790 - o791
Main Authors Revathi, B K, Reuben Jonathan, D, Kalai Sevi, K, Dhanalakshmi, K, Usha, G
Format Journal Article
LanguageEnglish
Published England International Union of Crystallography 01.10.2015
Subjects
crystal structure
Data Reports
hydrogen bonding
piperdine derivative
crystal structure
hydrogen bonding
piperdine derivative
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Summary:The title compound, C13H14NO2F3, crystallises with two mol-ecules, A and B, in the asymmetric unit, with similar conformations. The dihedral angles between the piperidine and phenyl rings are 83.76 (2) and 75.23 (2)° in mol-ecules A and B, respectively. The bond-angle sums around the N atoms [359.1 and 359.7° for mol-ecules A and B, respectively] indicate sp (2) hybridization for these atoms. In the crystal, O-H⋯O hydrogen bonds link the mol-ecules into separate [100] chains of A and B mol-ecules. The chains are cross-linked by C-H⋯O inter-actions, generating alternating (001) sheets of A and B mol-ecules.
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ISSN:2056-9890
2056-9890
DOI:10.1107/S205698901501765X