Microstructure, mechanical properties and low temperature degradation resistance of 2Y-TZP ceramic materials derived from nanopowders prepared by laser vaporization

Starting from commercially available powders of tetragonal zirconia polycrystals (TZP) doped with 3mol% yttria (Tosoh grade TZ-3YS-E) and yttria-free monoclinic zirconia (Tosoh grade TZ-0) powders with an overall Y2O3 content of 2mol% (2Y/TZP) were fabricated by CO2 laser vaporization (LAVA) and wet...

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Published inJournal of the European Ceramic Society Vol. 35; no. 9; pp. 2685 - 2691
Main Authors Smirnov, Anton, Kurland, Heinz-Dieter, Grabow, Janet, Müller, Frank A., Bartolomé, José F.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.09.2015
Subjects
Aging
Laser vaporization
Low temperature degradation
Mechanical properties
Phase transformation
Low temperature degradation
Aging
Mechanical properties
Laser vaporization
Phase transformation
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Abstract Starting from commercially available powders of tetragonal zirconia polycrystals (TZP) doped with 3mol% yttria (Tosoh grade TZ-3YS-E) and yttria-free monoclinic zirconia (Tosoh grade TZ-0) powders with an overall Y2O3 content of 2mol% (2Y/TZP) were fabricated by CO2 laser vaporization (LAVA) and wet mixing, respectively. The obtained powders were compacted by spark plasma sintering. The influence of the Y3+ distribution on the mechanical properties and on the low temperature degradation (LTD) of the obtained ceramics was investigated. 2Y/TZP ceramics sintered from LAVA nanoparticles showed significantly enhanced mechanical properties and improved LTD resistance due to the homogeneous yttria and grain size distributions in the ceramic structure. For the first time, the present research has demonstrated the effectiveness and reproducibility of the LAVA process for the preparation of tailored zirconia nanopowders enabling microstructural homogeneity and therefore optimized mechanical properties and degradation resistance of Y-TZP ceramics.
AbstractList Starting from commercially available powders of tetragonal zirconia polycrystals (TZP) doped with 3mol% yttria (Tosoh grade TZ-3YS-E) and yttria-free monoclinic zirconia (Tosoh grade TZ-0) powders with an overall Y2O3 content of 2mol% (2Y/TZP) were fabricated by CO2 laser vaporization (LAVA) and wet mixing, respectively. The obtained powders were compacted by spark plasma sintering. The influence of the Y3+ distribution on the mechanical properties and on the low temperature degradation (LTD) of the obtained ceramics was investigated. 2Y/TZP ceramics sintered from LAVA nanoparticles showed significantly enhanced mechanical properties and improved LTD resistance due to the homogeneous yttria and grain size distributions in the ceramic structure. For the first time, the present research has demonstrated the effectiveness and reproducibility of the LAVA process for the preparation of tailored zirconia nanopowders enabling microstructural homogeneity and therefore optimized mechanical properties and degradation resistance of Y-TZP ceramics.
Author Smirnov, Anton
Grabow, Janet
Bartolomé, José F.
Müller, Frank A.
Kurland, Heinz-Dieter
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  surname: Bartolomé
  fullname: Bartolomé, José F.
  email: jbartolo@icmm.csic.es
  organization: Instituto de Ciencia de Materiales de Madrid (ICMM), Consejo Superior de Investigaciones Científicas (CSIC), C/ Sor Juana Inés de la Cruz 3, 28049 Madrid, Spain
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Aging
Mechanical properties
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Phase transformation
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Snippet Starting from commercially available powders of tetragonal zirconia polycrystals (TZP) doped with 3mol% yttria (Tosoh grade TZ-3YS-E) and yttria-free...
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SubjectTerms Aging
Laser vaporization
Low temperature degradation
Mechanical properties
Phase transformation
Title Microstructure, mechanical properties and low temperature degradation resistance of 2Y-TZP ceramic materials derived from nanopowders prepared by laser vaporization
URI https://dx.doi.org/10.1016/j.jeurceramsoc.2015.03.006
Volume 35
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