Tributyl Borate Mediated Biginelli Reaction: A Facile Microwave-Assisted Green Synthetic Strategy toward Dihydropyrimidinones

Exploitation of a new boron-based catalyst, tributyl borate, for the formation of dihydropyrimidinones under solvent-free microwave-assisted conditions is described. The method is a simple, easy, fast, cost effective, and potentially green protocol for the formation of multi-functionalized pharmacol...

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Bibliographic Details
Published inBulletin of the Chemical Society of Japan Vol. 83; no. 3; pp. 288 - 290
Main Authors Ranjith, Choorikkat, Srinivasan, G. V, Vijayan, K. K
Format Journal Article
LanguageEnglish
Published TOKYO The Chemical Society of Japan 15.03.2010
Chemical Soc Japan
Subjects
Borates
Catalysts
Chemistry
Chemistry, Multidisciplinary
Exploitation
Physical Sciences
Science & Technology
Strategy
IRRADIATION
SOLVENT-FREE CONDITIONS
ONE-POT SYNTHESIS
EFFICIENT SYNTHESIS
PROTOCOL
CONDENSATION
3,4-DIHYDROPYRIMIDIN-2(1H)-ONES
CATALYST
CALCIUM-CHANNEL BLOCKERS
ACID-ESTERS
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Summary:Exploitation of a new boron-based catalyst, tributyl borate, for the formation of dihydropyrimidinones under solvent-free microwave-assisted conditions is described. The method is a simple, easy, fast, cost effective, and potentially green protocol for the formation of multi-functionalized pharmacologically active dihydropyrimidinones.
Bibliography:ObjectType-Article-2
SourceType-Scholarly Journals-1
ObjectType-Feature-1
content type line 23
ISSN:0009-2673
1348-0634
1348-0634
DOI:10.1246/bcsj.20090275