Polymerization within Nanoporous Anodized Alumina Oxide Templates (AAO): A Critical Survey

In the last few years, the polymerization of monomers within the nanocavities of porous materials has been thoroughly studied and developed, allowing for the synthesis of polymers with tailored morphologies, chemical architectures and functionalities. This is thus a subject of paramount scientific a...

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Published inPolymers Vol. 15; no. 3; p. 525
Main Authors Mijangos, Carmen, Martin, Jaime
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 19.01.2023
MDPI
Subjects
Addition polymerization
Alumina
Aluminum oxide
Catalysis
Chemical properties
Chemical synthesis
Engineering research
Free radical polymerization
Free radicals
Laboratories
Membranes
Molecular weight
Monomers
Nanostructured materials
Nanotechnology
Polymer melts
Polymerization
Polymers
Pore size
Porous materials
Review
State-of-the-art reviews
Spain
modeling
AAO templates reaction kinetics
nanoconfinement
polymer nanostructures
nanoporous geometries
polymer properties
nanopolymerization
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ISSN2073-4360
2073-4360
DOI10.3390/polym15030525

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Abstract In the last few years, the polymerization of monomers within the nanocavities of porous materials has been thoroughly studied and developed, allowing for the synthesis of polymers with tailored morphologies, chemical architectures and functionalities. This is thus a subject of paramount scientific and technological relevance, which, however, has not previously been analyzed from a general perspective. The present overview reports the state of the art on polymerization reactions in spatial confinement within porous materials, focusing on the use of anodized aluminum oxide (AAO) templates. It includes the description of the AAO templates used as nanoreactors. The polymerization reactions are categorized based on the polymerization mechanism. Amongst others, this includes electrochemical polymerization, free radical polymerization, step polymerization and atom transfer radical polymerization (ATRP). For each polymerization mechanism, a further subdivision is made based on the nature of the monomer used. Other aspects of “in situ” polymerization reactions in restricted AAO geometries include: conversion monitoring, kinetic studies, modeling and polymer characterization. In addition to the description of the polymerization process itself, the use of polymer materials derived from polymerization in AAO templates in nanotechnology applications, is also highlighted. Finally, the review is concluded with a general discussion outlining the challenges that remain in the field.
AbstractList In the last few years, the polymerization of monomers within the nanocavities of porous materials has been thoroughly studied and developed, allowing for the synthesis of polymers with tailored morphologies, chemical architectures and functionalities. This is thus a subject of paramount scientific and technological relevance, which, however, has not previously been analyzed from a general perspective. The present overview reports the state of the art on polymerization reactions in spatial confinement within porous materials, focusing on the use of anodized aluminum oxide (AAO) templates. It includes the description of the AAO templates used as nanoreactors. The polymerization reactions are categorized based on the polymerization mechanism. Amongst others, this includes electrochemical polymerization, free radical polymerization, step polymerization and atom transfer radical polymerization (ATRP). For each polymerization mechanism, a further subdivision is made based on the nature of the monomer used. Other aspects of "in situ" polymerization reactions in restricted AAO geometries include: conversion monitoring, kinetic studies, modeling and polymer characterization. In addition to the description of the polymerization process itself, the use of polymer materials derived from polymerization in AAO templates in nanotechnology applications, is also highlighted. Finally, the review is concluded with a general discussion outlining the challenges that remain in the field.In the last few years, the polymerization of monomers within the nanocavities of porous materials has been thoroughly studied and developed, allowing for the synthesis of polymers with tailored morphologies, chemical architectures and functionalities. This is thus a subject of paramount scientific and technological relevance, which, however, has not previously been analyzed from a general perspective. The present overview reports the state of the art on polymerization reactions in spatial confinement within porous materials, focusing on the use of anodized aluminum oxide (AAO) templates. It includes the description of the AAO templates used as nanoreactors. The polymerization reactions are categorized based on the polymerization mechanism. Amongst others, this includes electrochemical polymerization, free radical polymerization, step polymerization and atom transfer radical polymerization (ATRP). For each polymerization mechanism, a further subdivision is made based on the nature of the monomer used. Other aspects of "in situ" polymerization reactions in restricted AAO geometries include: conversion monitoring, kinetic studies, modeling and polymer characterization. In addition to the description of the polymerization process itself, the use of polymer materials derived from polymerization in AAO templates in nanotechnology applications, is also highlighted. Finally, the review is concluded with a general discussion outlining the challenges that remain in the field.
In the last few years, the polymerization of monomers within the nanocavities of porous materials has been thoroughly studied and developed, allowing for the synthesis of polymers with tailored morphologies, chemical architectures and functionalities. This is thus a subject of paramount scientific and technological relevance, which, however, has not previously been analyzed from a general perspective. The present overview reports the state of the art on polymerization reactions in spatial confinement within porous materials, focusing on the use of anodized aluminum oxide (AAO) templates. It includes the description of the AAO templates used as nanoreactors. The polymerization reactions are categorized based on the polymerization mechanism. Amongst others, this includes electrochemical polymerization, free radical polymerization, step polymerization and atom transfer radical polymerization (ATRP). For each polymerization mechanism, a further subdivision is made based on the nature of the monomer used. Other aspects of “in situ” polymerization reactions in restricted AAO geometries include: conversion monitoring, kinetic studies, modeling and polymer characterization. In addition to the description of the polymerization process itself, the use of polymer materials derived from polymerization in AAO templates in nanotechnology applications, is also highlighted. Finally, the review is concluded with a general discussion outlining the challenges that remain in the field.
Audience Academic
Author Mijangos, Carmen
Martin, Jaime
AuthorAffiliation 1 Instituto de Ciencia y Tecnología de Polímeros, ICTP-CSIC, Juan de la Cierva 3, 28006 Madrid, Spain
3 POLYMAT, University of the Basque Country UPV/EHU, Avenida Tolosa 72, 20018 Donostia-San Sebastian, Spain
2 Donostia International Physics Center, DIPC, Paseo de Manuel Lardizabal 4, 20018 Donostia-San Sebastian, Spain
4 Grupo de Polímeros, Centro de Investigacións Tecnolóxicas (CIT), Universidade da Coruña, 15471 Ferrol, Spain
AuthorAffiliation_xml – name: 4 Grupo de Polímeros, Centro de Investigacións Tecnolóxicas (CIT), Universidade da Coruña, 15471 Ferrol, Spain
– name: 1 Instituto de Ciencia y Tecnología de Polímeros, ICTP-CSIC, Juan de la Cierva 3, 28006 Madrid, Spain
– name: 2 Donostia International Physics Center, DIPC, Paseo de Manuel Lardizabal 4, 20018 Donostia-San Sebastian, Spain
– name: 3 POLYMAT, University of the Basque Country UPV/EHU, Avenida Tolosa 72, 20018 Donostia-San Sebastian, Spain
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  surname: Mijangos
  fullname: Mijangos, Carmen
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/36771824$$D View this record in MEDLINE/PubMed
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Issue 3
Keywords modeling
AAO templates reaction kinetics
nanoconfinement
polymer nanostructures
nanoporous geometries
polymer properties
nanopolymerization
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Snippet In the last few years, the polymerization of monomers within the nanocavities of porous materials has been thoroughly studied and developed, allowing for the...
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Enrichment Source
StartPage 525
SubjectTerms Addition polymerization
Alumina
Aluminum oxide
Catalysis
Chemical properties
Chemical synthesis
Engineering research
Free radical polymerization
Free radicals
Laboratories
Membranes
Molecular weight
Monomers
Nanostructured materials
Nanotechnology
Polymer melts
Polymerization
Polymers
Pore size
Porous materials
Review
State-of-the-art reviews
Title Polymerization within Nanoporous Anodized Alumina Oxide Templates (AAO): A Critical Survey
URI https://www.ncbi.nlm.nih.gov/pubmed/36771824
https://www.proquest.com/docview/2774954926
https://www.proquest.com/docview/2775628556
https://pubmed.ncbi.nlm.nih.gov/PMC9919978
Volume 15
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