Reductive coupling of aromatic dialkyl acetals using the combination of zinc and chlorotrimethylsilane in the presence of potassium carbonate

The treatment of aromatic acetals with zinc and chlorosilane in the presence of potassium carbonate in toluene brought about facile and effective reductive coupling to give the corresponding coupling products.

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Bibliographic Details
Published inChemistry letters Vol. 36; no. 12; pp. 1418 - 1419
Main Authors Hatano, Bunpei, Nagahashi, Keita, Habaue, Shigeki
Format Journal Article
LanguageEnglish
Published TOKYO Chemical Soc Japan 05.12.2007
Subjects
Chemistry
Chemistry, Multidisciplinary
Physical Sciences
Science & Technology
REAGENT
ARYL ALDEHYDES
CHLOROSILANE
ONE-POT SYNTHESIS
CATALYTIC-SYSTEM
PINACOL
METAL
ALIPHATIC-ALDEHYDES
TITANIUM
CP2TIPH
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Summary:The treatment of aromatic acetals with zinc and chlorosilane in the presence of potassium carbonate in toluene brought about facile and effective reductive coupling to give the corresponding coupling products.
ISSN:0366-7022
1348-0715
DOI:10.1246/cl.2007.1418