Crystal Structure of 4-Hydroxy-3-methoxybenzaldehyde-4-methylthiosemicarbazone

The structure of 4-hydroxy-3-methoxybenzaldehyde-4-methylthiosemicarbazone (VAMTSC) was determined by X-ray crystallography. The molecular structure matches the asymmetric unit, and the compound crystallizes in a monoclinic system. It was characterized thus: P21/c, a = 8.4960(3), b = 8.5040(2), c =...

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Published inX-ray Structure Analysis Online Vol. 31; pp. 5 - 6
Main Authors OLIVEIRA, Adriano Bof de, BECK, Johannes, DANIELS, Jörg, FEITOSA, Bárbara Regina Santos
Format Journal Article
LanguageEnglish
Published Tokyo The Japan Society for Analytical Chemistry 2015
Japan Science and Technology Agency
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Summary:The structure of 4-hydroxy-3-methoxybenzaldehyde-4-methylthiosemicarbazone (VAMTSC) was determined by X-ray crystallography. The molecular structure matches the asymmetric unit, and the compound crystallizes in a monoclinic system. It was characterized thus: P21/c, a = 8.4960(3), b = 8.5040(2), c = 17.2236(6)Å, β = 111.513(2)°, Z = 4, V = 1157.71(6)Å3. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R1 = 0.0403 and wR2 = 0.078.
ISSN:1883-3578
1883-3578
DOI:10.2116/xraystruct.31.5