The Microstructure Evolution Process and Flexural Behaviours of SiC Matrix Ceramic Infiltrated by Aluminium Base Alloy

• Published in: Materials Vol. 15; no. 16; p. 5746
• Main Authors: Wang, Wei, Jia, Jinsheng, Sun, Yong, Kong, Zhuang, Yang, Liangliang, Ma, Ruina, Li, Qiang
• Format: Journal Article
• Language: English
• Published: Basel MDPI AG 01.08.2022; MDPI
• Subjects: Alloys; Aluminum base alloys; Atoms & subatomic particles; Bend strength; Bending modulus; Ceramics; Cermets; Electrical conductivity; Evolution; flexural behaviours; Infiltration; Low temperature; Mechanical properties; Microstructure; Modulus of rupture in bending; Phase composition; Plasma sintering; Scanning electron microscopy; SiC; Silicon carbide; Spectrum analysis; Temperature; Ti3Si(Al)C2; Titanium carbide; Transition layers; China; Beijing China; United States > US
• ISSN: 1996-1944; 1996-1944
• DOI: 10.3390/ma15165746

In this paper, an infiltration approach was proposed to generate a Ti3Si(Al)C2 transition layer in SiC matrix composites to effectually strengthen SiC ceramics. The infiltration temperature played a significant role in the evolution of the microstructure, phase composition, and flexural behaviours. Molten aluminium base alloy fully penetrated SiC ceramic after infiltration at different experimental temperatures (800–1000 °C). The phases in the reaction layer on the surface of SiC ceramic samples varied with the infiltration temperature. When infiltrated at 800 °C, only SiC and Al phases can be found in SiC composites, whereas at 900 °C, a reaction layer containing Ti3Si(Al)C2 and SiC was produced. The Ti3Si(Al)C2 phase grew in situ on SiC. At 1000 °C, the Ti3Si(Al)C2 phase was unstable and decomposed into TiC and Ti5Si3. The cermet phase Ti3Si(Al)C2 was synthesized at a relatively low temperature. Consequently, the flexural modulus and three-point bending strength of samples infiltrated at 900 °C was enhanced by 1.4 and 2.4 times for the original SiC ceramic, respectively.