Effects of milling method and artificial ageing on optical properties of high translucent zirconia for chairside restorations

• Published in: Dental materials Vol. 38; no. 1; pp. 108 - 120
• Main Authors: Mourouzis, Petros, Tolidis, Kosmas
• Format: Journal Article
• Language: English
• Published: England Elsevier Inc 01.01.2022; Elsevier BV
• Subjects: Aging; Aging (artificial); Aluminum oxide; CAD/CAM; Ceramics; Ceramics - chemistry; Computer-Aided Design; Computer-aided manufacturing; Dental Materials - chemistry; Digital dentistry; Distilled water; Materials Testing; Optical phenomena; Optical properties; Partial stabilization; Phase composition; Phase transitions; Surface Properties; Tetragonal zirconia; Variance analysis; X-ray diffraction; Y-TZP ceramic; Yttria-stabilized zirconia; Yttrium oxide; Zirconia; Zirconium - chemistry; Optical phenomena; Computer-aided design; Ceramics; Digital dentistry; Y-TZP ceramic; Computer-aided manufacturing
• ISSN: 0109-5641; 1879-0097; 1879-0097
• DOI: 10.1016/j.dental.2021.10.015

This study aimed to evaluate the optical properties of highly translucent 5 mol% yttria, partially stabilised monolithic zirconia, and 3 mol% yttria-stabilised tetragonal zirconia after their subjection to different milling methods and artificial ageing. Two types of pre-shaded zirconia materials were used: inCoris TZI C and Katana STML. A total of 120 specimens were categorised according to the milling method (dry or wet-milling) and the solution used for milling (fresh distilled water or impregnated water with residues of CAD/CAM ceramic materials). The translucency and contrast ratios of all specimens were calculated after they were subjected to sintering and accelerated ageing. The material phase composition was tested before and after ageing, using X-ray diffraction analysis to evaluate T-M phase transformation. Data were statistically analysed via a three-way analysis of variance between the subject factors, the material and milling method, and the within-subject factor, ageing. The analysis of covariance model was used to analyse the changes in translucency and contrast ratio between baseline and ageing, with statistical significance set at p < 0.05. Katana STML and inCoris TZI C showed the highest translucency when dry-milled (21.9 ± 1.4, and 11.8 ± 0.7, respectively), and the lowest when milled with used impregnated water (5.4 ± 1.2 and 10.7 ± 1.3, respectively). Wet-milling using impregnated water, should be avoided owing to the saturation of alumina particles. Accelerated ageing resulted in the same pattern for both materials. Significance Dry milling of highly translucent zirconia can result in higher translucency and lower contrast ratio values.