A high-temperature and high-pressure cell for in situ visualization of reaction processes by neutron imaging
This study developed a high-temperature and high-pressure (HTHP) cell for in situ neutron imaging of hydrothermal reactions. The cell’s maximum temperature and pressure were 500 °C and 50 MPa, respectively, and its vessel for observing reactions comprised SUS316 stainless steel. Neutron transmission...
Saved in:
| Published in | Review of Scientific Instruments Vol. 94; no. 8 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
AIP Publishing
01.08.2023
American Institute of Physics |
| Subjects | |
| Online Access | Get full text |
Cover
Loading…
| Abstract | This study developed a high-temperature and high-pressure (HTHP) cell for in situ neutron imaging of hydrothermal reactions. The cell’s maximum temperature and pressure were 500 °C and 50 MPa, respectively, and its vessel for observing reactions comprised SUS316 stainless steel. Neutron transmission images were obtained to observe the behavior of sub- and supercritical water and the decomposition of two plastics (polypropylene and polyethylene) at HTHP. The images showed that water’s density and phase changed with temperature and pressure, affecting neutron transmission (and thus image brightness). The plastics began to melt and change shape at 150–200 °C, and they decomposed at 500 °C and 20 MPa. This study provides a basis for future research using the HTHP cell to examine various reactions such as the decomposition of biomass samples, the reforming of heavy oil, and the synthesis of nano-materials using sub- and supercritical water. |
|---|---|
| AbstractList | This study developed a high-temperature and high-pressure (HTHP) cell for in situ neutron imaging of hydrothermal reactions. The cell’s maximum temperature and pressure were 500 °C and 50 MPa, respectively, and its vessel for observing reactions comprised SUS316 stainless steel. Neutron transmission images were obtained to observe the behavior of sub- and supercritical water and the decomposition of two plastics (polypropylene and polyethylene) at HTHP. The images showed that water’s density and phase changed with temperature and pressure, affecting neutron transmission (and thus image brightness). The plastics began to melt and change shape at 150–200 °C, and they decomposed at 500 °C and 20 MPa. This study provides a basis for future research using the HTHP cell to examine various reactions such as the decomposition of biomass samples, the reforming of heavy oil, and the synthesis of nano-materials using sub- and supercritical water. This study developed a high-temperature and high-pressure (HTHP) cell for in situ neutron imaging of hydrothermal reactions. The cell's maximum temperature and pressure were 500 °C and 50 MPa, respectively, and its vessel for observing reactions comprised SUS316 stainless steel. Neutron transmission images were obtained to observe the behavior of sub- and supercritical water and the decomposition of two plastics (polypropylene and polyethylene) at HTHP. The images showed that water's density and phase changed with temperature and pressure, affecting neutron transmission (and thus image brightness). The plastics began to melt and change shape at 150-200 °C, and they decomposed at 500 °C and 20 MPa. This study provides a basis for future research using the HTHP cell to examine various reactions such as the decomposition of biomass samples, the reforming of heavy oil, and the synthesis of nano-materials using sub- and supercritical water.This study developed a high-temperature and high-pressure (HTHP) cell for in situ neutron imaging of hydrothermal reactions. The cell's maximum temperature and pressure were 500 °C and 50 MPa, respectively, and its vessel for observing reactions comprised SUS316 stainless steel. Neutron transmission images were obtained to observe the behavior of sub- and supercritical water and the decomposition of two plastics (polypropylene and polyethylene) at HTHP. The images showed that water's density and phase changed with temperature and pressure, affecting neutron transmission (and thus image brightness). The plastics began to melt and change shape at 150-200 °C, and they decomposed at 500 °C and 20 MPa. This study provides a basis for future research using the HTHP cell to examine various reactions such as the decomposition of biomass samples, the reforming of heavy oil, and the synthesis of nano-materials using sub- and supercritical water. |
| Author | Tsukasa Miyazaki Yoshihiro Matsumoto Takashi Noma Jun Abe |
| Author_xml | – sequence: 1 givenname: Jun surname: Abe fullname: Abe, Jun organization: Neutron Science and Technology Center, Comprehensive Research Organization for Science and Society (CROSS), Tokai, Ibaraki 319-1106, Japan – sequence: 2 givenname: Yoshihiro surname: Matsumoto fullname: Matsumoto, Yoshihiro organization: Neutron Science and Technology Center, Comprehensive Research Organization for Science and Society (CROSS), Tokai, Ibaraki 319-1106, Japan – sequence: 3 givenname: Tsukasa surname: Miyazaki fullname: Miyazaki, Tsukasa organization: Neutron Science and Technology Center, Comprehensive Research Organization for Science and Society (CROSS), Tokai, Ibaraki 319-1106, Japan – sequence: 4 givenname: Takashi surname: Noma fullname: Noma, Takashi organization: Neutron Science and Technology Center, Comprehensive Research Organization for Science and Society (CROSS), Tokai, Ibaraki 319-1106, Japan |
| BackLink | https://cir.nii.ac.jp/crid/1873961342663738368$$DView record in CiNii https://www.ncbi.nlm.nih.gov/pubmed/38065167$$D View this record in MEDLINE/PubMed |
| BookMark | eNp9kU1r3DAQhkVJaDZpDv0DRdAe0oKT0aflYwjpBwRyac9CtsYbFa-8lexA-uujjXcvofSiES_PvLwzc0qO4hiRkPcMLhlocaUugalGG_WGrBiYpqo1F0dkBSBkpWtpTsh5zqEFrrlmDNRbciIMaMV0vSLDNX0I64dqws0Wk5vmhNRFv4jbhDnvlA6HgfZjoiHSHKaZPoY8uyH8dVMYIx17mtB1L_9tGrvShZm2TzTiPKUiho1bh7h-R457N2Q839cz8uvr7c-b79Xd_bcfN9d3VSelmCrO0HPpDArvG6E7BK56QIlOt0w50Tjoauf7tte-a72UAAZc7R36hmvg4oxcLL4lzJ8Z82Q3Ie9mcBHHOVveAG9qEEYU9OMr9Pc4p1jSWW6UqjnnqinUhz01txv0dpvKROnJHvZYgKsF6NKYc8LedmF6Wc6UXBgsA7s7llV2f6zS8flVx8H0X-yXhc0H1__CnxY4hlBS7F5matFoJiTXWtRlbG3EM8tCq3I |
| CODEN | RSINAK |
| CitedBy_id | crossref_primary_10_1016_j_jaap_2024_106805 |
| Cites_doi | 10.1016/S1369-7021(11)70139-0 10.1038/nmeth.2089 10.1063/1.5136034 10.1016/j.supflu.2011.11.010 10.1016/j.supflu.2007.08.003 10.1038/s41467-019-12117-5 10.1016/j.supflu.2008.11.019 10.1021/acssuschemeng.8b03841 10.1016/j.nima.2008.11.019 |
| ContentType | Journal Article |
| Copyright | Author(s) 2023 Author(s). Published under an exclusive license by AIP Publishing. |
| Copyright_xml | – notice: Author(s) – notice: 2023 Author(s). Published under an exclusive license by AIP Publishing. |
| DBID | RYH AAYXX CITATION NPM 8FD H8D L7M 7X8 |
| DOI | 10.1063/5.0159685 |
| DatabaseName | CiNii Complete CrossRef PubMed Technology Research Database Aerospace Database Advanced Technologies Database with Aerospace MEDLINE - Academic |
| DatabaseTitle | CrossRef PubMed Technology Research Database Aerospace Database Advanced Technologies Database with Aerospace MEDLINE - Academic |
| DatabaseTitleList | PubMed CrossRef MEDLINE - Academic Technology Research Database |
| Database_xml | – sequence: 1 dbid: NPM name: PubMed url: https://proxy.k.utb.cz/login?url=http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed sourceTypes: Index Database |
| DeliveryMethod | fulltext_linktorsrc |
| Discipline | Sciences (General) |
| EISSN | 1089-7623 |
| ExternalDocumentID | 38065167 10_1063_5_0159685 rsi |
| Genre | Journal Article |
| GroupedDBID | --- -DZ -~X .DC 123 1UP 2-P 29P 4.4 53G 5RE 5VS 85S A9. AAAAW AABDS AAGWI AAPUP AAYIH ABFTF ABJGX ABJNI ACBEA ACBRY ACGFO ACGFS ACLYJ ACNCT ACZLF ADCTM ADMLS AEGXH AEJMO AENEX AFATG AFHCQ AGKCL AGLKD AGMXG AGTJO AHSDT AIAGR AJJCW AJQPL ALEPV ALMA_UNASSIGNED_HOLDINGS AQWKA ATXIE AWQPM BDMKI BPZLN CS3 DU5 EBS F5P FDOHQ FFFMQ HAM L7B M43 M6X M71 M73 N9A NPSNA O-B P2P RIP RNS RQS RYH TAE TN5 WH7 XSW YNT YZZ ~02 AAEUA ESX VQA AAYXX CITATION NPM VXZ 8FD H8D L7M 7X8 |
| ID | FETCH-LOGICAL-c443t-21ed24a8e3dd936ce025f0e4ea6b15a39a0c7adfbf6dcbd440080a7daed926023 |
| ISSN | 0034-6748 1089-7623 |
| IngestDate | Thu Jul 10 23:26:19 EDT 2025 Mon Jun 30 06:39:04 EDT 2025 Wed Feb 19 02:08:09 EST 2025 Thu Apr 24 23:11:55 EDT 2025 Tue Jul 01 02:58:14 EDT 2025 Fri Jun 21 00:15:23 EDT 2024 Thu Jun 26 23:14:24 EDT 2025 |
| IsPeerReviewed | true |
| IsScholarly | true |
| Issue | 8 |
| Language | English |
| License | Published under an exclusive license by AIP Publishing. 2023 Author(s). Published under an exclusive license by AIP Publishing. |
| LinkModel | OpenURL |
| MergedId | FETCHMERGED-LOGICAL-c443t-21ed24a8e3dd936ce025f0e4ea6b15a39a0c7adfbf6dcbd440080a7daed926023 |
| Notes | ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 content type line 23 |
| ORCID | 0000-0001-9414-4619 0009-0003-4403-6435 0009-0000-7110-0314 |
| PMID | 38065167 |
| PQID | 2855722259 |
| PQPubID | 2050675 |
| PageCount | 6 |
| ParticipantIDs | crossref_citationtrail_10_1063_5_0159685 nii_cinii_1873961342663738368 pubmed_primary_38065167 proquest_journals_2855722259 proquest_miscellaneous_2902970383 crossref_primary_10_1063_5_0159685 scitation_primary_10_1063_5_0159685 |
| ProviderPackageCode | CITATION AAYXX |
| PublicationCentury | 2000 |
| PublicationDate | 2023-08-01 20230801 2023-Aug-01 |
| PublicationDateYYYYMMDD | 2023-08-01 |
| PublicationDate_xml | – month: 08 year: 2023 text: 2023-08-01 day: 01 |
| PublicationDecade | 2020 |
| PublicationPlace | United States |
| PublicationPlace_xml | – name: United States – name: Melville |
| PublicationTitle | Review of Scientific Instruments |
| PublicationTitleAlternate | Rev Sci Instrum |
| PublicationYear | 2023 |
| Publisher | AIP Publishing American Institute of Physics |
| Publisher_xml | – name: AIP Publishing – name: American Institute of Physics |
| References | Chen, Jin, Linda Wang (c10) 2019; 7 Peterson, Vontobel, Vogel, Tester (c3) 2009; 49 Schneider, Rasband, Eliceiri (c9) 2012; 9 Peterson, Vontobel, Vogel, Tester (c2) 2008; 43 Takami, Sugioka, Tsukada, Adschiri, Sugimoto, Takenaka, Saito (c5) 2012; 63 Shinohara, Kai, Oikawa, Nakatani, Segawa, Hiroi, Su, Ooi, Harada, Iikura, Hayashida, Parker, Matsumoto, Kamiyama, Sato, Kiyanagi (c7) 2020; 91 Kardjilov, Manke, Hilger, Strobl, Banhart (c1) 2011; 14 Maxim, Contescu, Boillat, Niceno, Karalis, Testino, Ludwig (c4) 2019; 10 Ikeda (c8) 2009; 600 (2023082312443790900_c1) 2011; 14 (2023082312443790900_c2) 2008; 43 (2023082312443790900_c5) 2012; 63 2023082312443790900_c6 (2023082312443790900_c7) 2020; 91 (2023082312443790900_c9) 2012; 9 (2023082312443790900_c3) 2009; 49 (2023082312443790900_c4) 2019; 10 (2023082312443790900_c8) 2009; 600 (2023082312443790900_c10) 2019; 7 |
| References_xml | – volume: 43 start-page: 490 year: 2008 ident: c2 article-title: visualization of the performance of a supercritical-water salt separator using neutron radiography publication-title: J. Supercrit. Fluids – volume: 63 start-page: 46 year: 2012 ident: c5 article-title: Neutron radiography on tubular flow reactor for hydrothermal synthesis: In situ monitoring of mixing behavior of supercritical water and room-temperature water publication-title: J. Supercrit. Fluids – volume: 600 start-page: 1 year: 2009 ident: c8 article-title: J-PARC status update publication-title: Nucl. Instrum. Methods Phys. Res., Sect. A – volume: 14 start-page: 248 year: 2011 ident: c1 article-title: Neutron imaging in materials science publication-title: Mater. Today – volume: 10 start-page: 4114 year: 2019 ident: c4 article-title: Visualization of supercritical water -boiling at Widom line crossover publication-title: Nat. Commun. – volume: 91 start-page: 043302 year: 2020 ident: c7 article-title: The energy-resolved neutron imaging system, RADEN publication-title: Rev. Sci. Instrum. – volume: 49 start-page: 71 year: 2009 ident: c3 article-title: Normal-phase dynamic imaging of supercritical-water salt precipitation using neutron radiography publication-title: J. Supercrit. Fluids – volume: 7 start-page: 3749 year: 2019 ident: c10 article-title: Use of supercritical water for the liquefaction of polypropylene into oil publication-title: ACS Sustainable Chem. Eng. – volume: 9 start-page: 671 year: 2012 ident: c9 article-title: NIH image to ImageJ: 25 years of image analysis publication-title: Nat. Methods – volume: 14 start-page: 248 year: 2011 ident: 2023082312443790900_c1 article-title: Neutron imaging in materials science publication-title: Mater. Today doi: 10.1016/S1369-7021(11)70139-0 – volume: 9 start-page: 671 year: 2012 ident: 2023082312443790900_c9 article-title: NIH image to ImageJ: 25 years of image analysis publication-title: Nat. Methods doi: 10.1038/nmeth.2089 – volume: 91 start-page: 043302 year: 2020 ident: 2023082312443790900_c7 article-title: The energy-resolved neutron imaging system, RADEN publication-title: Rev. Sci. Instrum. doi: 10.1063/1.5136034 – volume: 63 start-page: 46 year: 2012 ident: 2023082312443790900_c5 article-title: Neutron radiography on tubular flow reactor for hydrothermal synthesis: In situ monitoring of mixing behavior of supercritical water and room-temperature water publication-title: J. Supercrit. Fluids doi: 10.1016/j.supflu.2011.11.010 – volume: 43 start-page: 490 year: 2008 ident: 2023082312443790900_c2 article-title: In situ visualization of the performance of a supercritical-water salt separator using neutron radiography publication-title: J. Supercrit. Fluids doi: 10.1016/j.supflu.2007.08.003 – volume: 10 start-page: 4114 year: 2019 ident: 2023082312443790900_c4 article-title: Visualization of supercritical water pseudo-boiling at Widom line crossover publication-title: Nat. Commun. doi: 10.1038/s41467-019-12117-5 – volume: 49 start-page: 71 year: 2009 ident: 2023082312443790900_c3 article-title: Normal-phase dynamic imaging of supercritical-water salt precipitation using neutron radiography publication-title: J. Supercrit. Fluids doi: 10.1016/j.supflu.2008.11.019 – volume: 7 start-page: 3749 year: 2019 ident: 2023082312443790900_c10 article-title: Use of supercritical water for the liquefaction of polypropylene into oil publication-title: ACS Sustainable Chem. Eng. doi: 10.1021/acssuschemeng.8b03841 – ident: 2023082312443790900_c6 – volume: 600 start-page: 1 year: 2009 ident: 2023082312443790900_c8 article-title: J-PARC status update publication-title: Nucl. Instrum. Methods Phys. Res., Sect. A doi: 10.1016/j.nima.2008.11.019 |
| SSID | ssib026261105 ssib045031068 ssib006542853 ssib000302842 ssib002505594 ssib004908367 ssib017603183 ssib003115832 ssj0000511 ssib000332244 ssib002557691 |
| Score | 2.4156299 |
| Snippet | This study developed a high-temperature and high-pressure (HTHP) cell for in situ neutron imaging of hydrothermal reactions. The cell’s maximum temperature and... This study developed a high-temperature and high-pressure (HTHP) cell for in situ neutron imaging of hydrothermal reactions. The cell's maximum temperature and... |
| SourceID | proquest pubmed crossref scitation nii |
| SourceType | Aggregation Database Index Database Enrichment Source Publisher |
| SubjectTerms | Decomposition reactions High pressure High temperature Hydrothermal reactions Image transmission Pressure cells Reforming Scientific apparatus & instruments |
| Title | A high-temperature and high-pressure cell for in situ visualization of reaction processes by neutron imaging |
| URI | https://cir.nii.ac.jp/crid/1873961342663738368 http://dx.doi.org/10.1063/5.0159685 https://www.ncbi.nlm.nih.gov/pubmed/38065167 https://www.proquest.com/docview/2855722259 https://www.proquest.com/docview/2902970383 |
| Volume | 94 |
| hasFullText | 1 |
| inHoldings | 1 |
| isFullTextHit | |
| isPrint | |
| link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwnV1bb5RAFJ7Y7YP6YKxXtDXj5aGGoMBcgMeNl1TjNkbbpG-bgRlSbIVGWJPur_ccGFhW13h5IbuzhLBzPs58ZzjnO4Q8k9hEJIqYp2M_8nga554SLPOk4BqePa3TFN_ozg7lwTF_fyJO-n73trqkSV9ky411Jf9jVRgDu2KV7D9YdrgoDMBnsC8cwcJw_CsbT11UG_ZQXspqI7fvAtrBNsEVR3Brvk0mLEq3LpqF-72osZJyOZBF4I1dw_CLrmrA1EhKS7PAbXK3-No2Mhqz2E-repe2nhLTjdq0A1RisNpQbVrOonSnqVl5lvq0OC2-Ve5MNTBPVVMNGwf14kzVyp0Vl2oJpHa1oXCG3Z7cw8quH3aDImRDepyF1LuPoy21sS9m3MNWJ91K1LlfP048gAgb--euCfIvrh64FdgHRVdFImOxRbZDiBTCCdmevp59-DyO-WAJHmsUgg8bcxrggGIc4woIwZKx0wtEPCq-xTelTK4V54YjzhNEbd_u4XsIESNQrMFpcoFirHIlaQ9esWvraKejl7-S7OXw59ZI01ZZFJvioevkKrCmLoFjxJGObpIbNrih0w6pO-TKF3WL7Njlo6b7VuP8-W1yPqU_Q5cCdOkadClClwJ0aVFShC5dgy6tctpDlw7QpekltdClFrp3yPHbN0evDjzb-MPLOGeNFwZGh1zFhmmdMJkZMEruG26UTAOhWKL8LFI6T3Ops1RzjnGPirQyOoH4PGR3yaSsSnOf0DwJEq55EPsauXKmUNBOGZRpTFUghUP2-5md95OHzVnO5212hmRzMbdGcMiT4dSLTgpm00l7YB64FB6DOGIJ8GVkwaggxmTskN3ecHPrSeo54EdEuPGSOOTx8DP4eZxmVZpqAeck2GbOh4s45F5n8OEuGGZHBDJyyNMBAb-_xQd_uMWH5NrqMd4lE_AdZg-Yd5M-ss_WD3s8x7c |
| linkProvider | EBSCOhost |
| openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=A+high-temperature+and+high-pressure+cell+for+in+situ+visualization+of+reaction+processes+by+neutron+imaging&rft.jtitle=Review+of+Scientific+Instruments&rft.au=Jun+Abe&rft.au=Yoshihiro+Matsumoto&rft.au=Tsukasa+Miyazaki&rft.au=Takashi+Noma&rft.date=2023-08-01&rft.pub=AIP+Publishing&rft.issn=0034-6748&rft.eissn=1089-7623&rft.volume=94&rft_id=info:doi/10.1063%2F5.0159685 |
| thumbnail_l | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=0034-6748&client=summon |
| thumbnail_m | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=0034-6748&client=summon |
| thumbnail_s | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=0034-6748&client=summon |