Surface Finishing and Coating Parameters Impact on Additively Manufactured Binder-Jetted Steel-Bronze Composites

• Published in: Materials Vol. 17; no. 3; p. 598
• Main Authors: Grizzle, Andrew C, Elliott, Amy, Klein, Kate L, Tyagi, Pawan
• Format: Journal Article
• Language: English
• Published: Switzerland MDPI AG 26.01.2024; MDPI
• Subjects: Additive manufacturing; Analysis; binder jetting; Bronzes; Cleaning; Coating; Coatings; Composite materials; Contact angle; Corrosion; Design of experiments; Electroless nickel plating; Electronics industry; MATERIALS SCIENCE; Morphology; nickel plating; Phosphorus; Plasma etching; post-processing; Process parameters; rapid prototyping; Stainless steel; Stainless steels; Statistical analysis; Steel industry; Steel, Stainless; Surface finishing; Surface preparation; Surface properties; Surface roughness; Temperature; Thickness; Time factors; Japan; United States > US; post-processing; nickel plating; additive manufacturing; rapid prototyping; binder jetting; surface roughness
• ISSN: 1996-1944; 1996-1944
• DOI: 10.3390/ma17030598

In this paper, electroless nickel plating is explored for the protection of binder-jetting-based additively manufactured (AM) composite materials. Electroless nickel plating was attempted on binder-jetted composites composed of stainless steel and bronze, resulting in differences in the physicochemical properties. We investigated the impact of surface finishing, plating solution chemistry, and plating parameters to attain a wide range of surface morphologies and roughness levels. We employed the Keyence microscope to quantitatively evaluate dramatically different surface properties before and after the coating of AM composites. Scanning electron microscopy revealed a wide range of microstructural properties in relation to each combination of surface finishing and coating parameters. We studied chempolishing, plasma cleaning, and organic cleaning as the surface preparation methods prior to coating. We found that surface preparation dictated the surface roughness. Taguchi statistical analysis was performed to investigate the relative strength of experimental factors and interconnectedness among process parameters to attain optimum coating qualities. The quantitative impacts of phosphorous level, temperature, surface preparation, and time factor on the roughness of the nickel-plated surface were 17.95%, 8.2%, 50.02%, and 13.21%, respectively. On the other hand, the quantitative impacts of phosphorous level, temperature, surface preparation, and time factor on the thickness of nickel plating were 35.12%, 41.40%, 3.87%, and 18.24%, respectively. The optimum combination of the factors' level projected the lowest roughness of Ra at 7.76 µm. The optimum combination of the factors' level projected the maximum achievable thickness of ~149 µm. This paper provides insights into coating process for overcoming the sensitivity of AM composites in hazardous application spaces via robust coating.