Studies on the Reactions of Heterocyclic Compounds. II. Syntheses and Some Reactions of 1, 6-Phenanthroline N-Oxides

1, 6-Phenanthroline was synthesized from 4-aminoquinoline by the Skraup reaction using sulfo-mix, and N-oxidation was carried out in various ways to obtain 6-oxide and 1, 6-dioxide. Reactions of 6-oxide with acetic anhydride and with phosphoryl chloride and the Reissert reaction were carreid out and...

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Published inChemical & pharmaceutical bulletin Vol. 17; no. 7; pp. 1511 - 1514
Main Authors KOBAYASHI, YOSHIRO, KUMADAKI, ITSUMARO, MORINAGA, KUNIO
Format Journal Article
LanguageEnglish
Published Tokyo The Pharmaceutical Society of Japan 1969
Japan Science and Technology Agency
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Summary:1, 6-Phenanthroline was synthesized from 4-aminoquinoline by the Skraup reaction using sulfo-mix, and N-oxidation was carried out in various ways to obtain 6-oxide and 1, 6-dioxide. Reactions of 6-oxide with acetic anhydride and with phosphoryl chloride and the Reissert reaction were carreid out and the results were compared with those in the case of 1, 6-naphthyridine.
ISSN:0009-2363
1347-5223
DOI:10.1248/cpb.17.1511