Comparative studies on effects of silica and titania nanoparticles on crystallization and complex segmental dynamics in poly(dimethylsiloxane)

Effects of in situ synthesized silica and titania nanoparticles, 5 and 20–40 nm in diameter, respectively, on glass transition and segmental dynamics of poly(dimethylsiloxane) networks were studied by employing differential scanning calorimetry, thermally stimulated depolarization currents and broad...

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Published inPolymer (Guilford) Vol. 51; no. 23; pp. 5490 - 5499
Main Authors Klonos, P., Panagopoulou, A., Bokobza, L., Kyritsis, A., Peoglos, V., Pissis, P.
Format Journal Article
LanguageEnglish
Published Kidlington Elsevier Ltd 29.10.2010
Elsevier
Subjects
Applied sciences
Broadband
Composites
Dynamic tests
Dynamics
Exact sciences and technology
Forms of application and semi-finished materials
Glass transition
Nanocomposites
Nanoparticles
Poly(dimethylsiloxane) nanocomposites
Polymer crystallization
Polymer industry, paints, wood
Segmental dynamics
Silicon dioxide
Technology of polymers
Titanium dioxide
Poly(dimethylsiloxane) nanocomposites
Polymer crystallization
Segmental dynamics
Dimethylsiloxane polymer
Crystallinity
Experimental study
Titania
Silica
Dielectric relaxation
Transformation temperature
Thermostimulated depolarization
Heat of transformation
Melt crystallization
Concentration effect
Nanocomposite
Titanium oxide
Filler
Comparative study
Silicone elastomer
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Abstract Effects of in situ synthesized silica and titania nanoparticles, 5 and 20–40 nm in diameter, respectively, on glass transition and segmental dynamics of poly(dimethylsiloxane) networks were studied by employing differential scanning calorimetry, thermally stimulated depolarization currents and broadband dielectric relaxation spectroscopy techniques. Strong interactions between the well dispersed fillers and the polymer suppress crystallinity and affect significantly the evolution of the glass transition in the nanocomposites. Next to the α relaxation associated with the glass transition of the bulk amorphous polymer fraction, two more segmental relaxations were recorded, originating from polymer chains restricted between condensed crystal regions (αc-relaxation) and the semi-bound polymer in an interfacial layer with strongly reduced mobility due to interactions with hydroxyls on the nanoparticle surface (α′ relaxation), respectively. Interactions with the polymer were found to be stronger in the case of titania than silica, leading to an estimated interaction length of around 2 nm for silica and at least double for titania nanocomposites. [Display omitted]
AbstractList Effects of in situ synthesized silica and titania nanoparticles, 5 and 20–40 nm in diameter, respectively, on glass transition and segmental dynamics of poly(dimethylsiloxane) networks were studied by employing differential scanning calorimetry, thermally stimulated depolarization currents and broadband dielectric relaxation spectroscopy techniques. Strong interactions between the well dispersed fillers and the polymer suppress crystallinity and affect significantly the evolution of the glass transition in the nanocomposites. Next to the α relaxation associated with the glass transition of the bulk amorphous polymer fraction, two more segmental relaxations were recorded, originating from polymer chains restricted between condensed crystal regions (αc-relaxation) and the semi-bound polymer in an interfacial layer with strongly reduced mobility due to interactions with hydroxyls on the nanoparticle surface (α′ relaxation), respectively. Interactions with the polymer were found to be stronger in the case of titania than silica, leading to an estimated interaction length of around 2 nm for silica and at least double for titania nanocomposites. [Display omitted]
Effects of in situ synthesized silica and titania nanoparticles, 5 and 20-40aanm in diameter, respectively, on glass transition and segmental dynamics of poly(dimethylsiloxane) networks were studied by employing differential scanning calorimetry, thermally stimulated depolarization currents and broadband dielectric relaxation spectroscopy techniques. Strong interactions between the well dispersed fillers and the polymer suppress crystallinity and affect significantly the evolution of the glass transition in the nanocomposites. Next to the a relaxation associated with the glass transition of the bulk amorphous polymer fraction, two more segmental relaxations were recorded, originating from polymer chains restricted between condensed crystal regions (ac -relaxation) and the semi-bound polymer in an interfacial layer with strongly reduced mobility due to interactions with hydroxyls on the nanoparticle surface (aa super(2) relaxation), respectively. Interactions with the polymer were found to be stronger in the case of titania than silica, leading to an estimated interaction length of around 2aanm for silica and at least double for titania nanocomposites. Display Omitted
Author Klonos, P.
Kyritsis, A.
Pissis, P.
Panagopoulou, A.
Peoglos, V.
Bokobza, L.
Author_xml – sequence: 1
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– sequence: 2
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  surname: Panagopoulou
  fullname: Panagopoulou, A.
  organization: Department of Physics, National Technical University of Athens, Zografou Campus, 15780, Athens, Greece
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  givenname: L.
  surname: Bokobza
  fullname: Bokobza, L.
  organization: Laboratoire PPMD, E.S.P.C.I., 10 rue Vauquelin, 75231 Paris Cedex, France
– sequence: 4
  givenname: A.
  surname: Kyritsis
  fullname: Kyritsis, A.
  organization: Department of Physics, National Technical University of Athens, Zografou Campus, 15780, Athens, Greece
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  surname: Peoglos
  fullname: Peoglos, V.
  organization: Department of Physics, National Technical University of Athens, Zografou Campus, 15780, Athens, Greece
– sequence: 6
  givenname: P.
  surname: Pissis
  fullname: Pissis, P.
  organization: Department of Physics, National Technical University of Athens, Zografou Campus, 15780, Athens, Greece
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Issue 23
Keywords Poly(dimethylsiloxane) nanocomposites
Polymer crystallization
Segmental dynamics
Dimethylsiloxane polymer
Crystallinity
Experimental study
Titania
Silica
Dielectric relaxation
Transformation temperature
Thermostimulated depolarization
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Nanocomposite
Titanium oxide
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Comparative study
Silicone elastomer
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Snippet Effects of in situ synthesized silica and titania nanoparticles, 5 and 20–40 nm in diameter, respectively, on glass transition and segmental dynamics of...
Effects of in situ synthesized silica and titania nanoparticles, 5 and 20-40aanm in diameter, respectively, on glass transition and segmental dynamics of...
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SubjectTerms Applied sciences
Broadband
Composites
Dynamic tests
Dynamics
Exact sciences and technology
Forms of application and semi-finished materials
Glass transition
Nanocomposites
Nanoparticles
Poly(dimethylsiloxane) nanocomposites
Polymer crystallization
Polymer industry, paints, wood
Segmental dynamics
Silicon dioxide
Technology of polymers
Titanium dioxide
Title Comparative studies on effects of silica and titania nanoparticles on crystallization and complex segmental dynamics in poly(dimethylsiloxane)
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