A Proton Conductive Porous Framework of an 18‐Crown‐6‐Ether Derivative Networked by Rigid Hydrogen Bonding Modules
A rigid hydrogen‐bonded organic framework (HOF) was constructed from a C3‐symmetric hexatopic carboxylic acid with a hydrophilic 18‐crown‐6‐ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4’‐dicarboxy‐o‐terphenyl moieties in the...
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| Published in | Angewandte Chemie International Edition Vol. 61; no. 45; pp. e202211686 - n/a |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
WEINHEIM
Wiley
07.11.2022
Wiley Subscription Services, Inc |
| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A rigid hydrogen‐bonded organic framework (HOF) was constructed from a C3‐symmetric hexatopic carboxylic acid with a hydrophilic 18‐crown‐6‐ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4’‐dicarboxy‐o‐terphenyl moieties in the periphery yielded a rigid layered porous framework through directional intermolecular hydrogen bonding. Interestingly, the HOF possesses 1D channels with bottleneck composed of 18C6 rings. The HOF shows proton conductivity (1.12×10−7 S cm−1) through Grotthuss mechanism (Ea=0.27 eV) under 98 %RH. The present unique water channel structure provides an inspiration to create molecular porous materials.
A porous hydrogen‐bonded framework (HOF) was constructed from a 18‐crown‐6‐ether (18C6) derivative. Although a 18C6 macrocycle is flexible and has many possible conformations, directional intermolecular hydrogen bonds of 4,4′‐dicarboxy‐o‐terphenyl modules in the periphery of the 18C6 allowed to form a rigid HOF with 1D channels with a bottleneck composed of 18C6 rings. The wet HOF shows proton conductivity (1.12×10−7 S cm−1) through a Grotthuss mechanism (Ea=0.27 eV) under 98 %RH. |
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| AbstractList | A rigid hydrogen‐bonded organic framework (HOF) was constructed from a C3‐symmetric hexatopic carboxylic acid with a hydrophilic 18‐crown‐6‐ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4’‐dicarboxy‐o‐terphenyl moieties in the periphery yielded a rigid layered porous framework through directional intermolecular hydrogen bonding. Interestingly, the HOF possesses 1D channels with bottleneck composed of 18C6 rings. The HOF shows proton conductivity (1.12×10−7 S cm−1) through Grotthuss mechanism (Ea=0.27 eV) under 98 %RH. The present unique water channel structure provides an inspiration to create molecular porous materials.
A porous hydrogen‐bonded framework (HOF) was constructed from a 18‐crown‐6‐ether (18C6) derivative. Although a 18C6 macrocycle is flexible and has many possible conformations, directional intermolecular hydrogen bonds of 4,4′‐dicarboxy‐o‐terphenyl modules in the periphery of the 18C6 allowed to form a rigid HOF with 1D channels with a bottleneck composed of 18C6 rings. The wet HOF shows proton conductivity (1.12×10−7 S cm−1) through a Grotthuss mechanism (Ea=0.27 eV) under 98 %RH. A rigid hydrogen-bonded organic framework (HOF) was constructed from a C3 -symmetric hexatopic carboxylic acid with a hydrophilic 18-crown-6-ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4'-dicarboxy-o-terphenyl moieties in the periphery yielded a rigid layered porous framework through directional intermolecular hydrogen bonding. Interestingly, the HOF possesses 1D channels with bottleneck composed of 18C6 rings. The HOF shows proton conductivity (1.12×10-7 S cm-1 ) through Grotthuss mechanism (Ea =0.27 eV) under 98 %RH. The present unique water channel structure provides an inspiration to create molecular porous materials.A rigid hydrogen-bonded organic framework (HOF) was constructed from a C3 -symmetric hexatopic carboxylic acid with a hydrophilic 18-crown-6-ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4'-dicarboxy-o-terphenyl moieties in the periphery yielded a rigid layered porous framework through directional intermolecular hydrogen bonding. Interestingly, the HOF possesses 1D channels with bottleneck composed of 18C6 rings. The HOF shows proton conductivity (1.12×10-7 S cm-1 ) through Grotthuss mechanism (Ea =0.27 eV) under 98 %RH. The present unique water channel structure provides an inspiration to create molecular porous materials. A rigid hydrogen‐bonded organic framework (HOF) was constructed from a C 3 ‐symmetric hexatopic carboxylic acid with a hydrophilic 18‐crown‐6‐ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4’‐dicarboxy‐ o ‐terphenyl moieties in the periphery yielded a rigid layered porous framework through directional intermolecular hydrogen bonding. Interestingly, the HOF possesses 1D channels with bottleneck composed of 18C6 rings. The HOF shows proton conductivity (1.12×10 −7 S cm −1 ) through Grotthuss mechanism ( E a =0.27 eV) under 98 %RH. The present unique water channel structure provides an inspiration to create molecular porous materials. A rigid hydrogen‐bonded organic framework (HOF) was constructed from a C3‐symmetric hexatopic carboxylic acid with a hydrophilic 18‐crown‐6‐ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4’‐dicarboxy‐o‐terphenyl moieties in the periphery yielded a rigid layered porous framework through directional intermolecular hydrogen bonding. Interestingly, the HOF possesses 1D channels with bottleneck composed of 18C6 rings. The HOF shows proton conductivity (1.12×10−7 S cm−1) through Grotthuss mechanism (Ea=0.27 eV) under 98 %RH. The present unique water channel structure provides an inspiration to create molecular porous materials. A rigid hydrogen-bonded organic framework (HOF) was constructed from a C-3-symmetric hexatopic carboxylic acid with a hydrophilic 18-crown-6-ether (18C6) component. Despite the flexible macrocyclic structure with many conformations, the derivative with three 4,4'-dicarboxy-o-terphenyl moieties in the periphery yielded a rigid layered porous framework through directional intermolecular hydrogen bonding. Interestingly, the HOF possesses 1D channels with bottleneck composed of 18C6 rings. The HOF shows proton conductivity (1.12x10(-7) S cm(-1)) through Grotthuss mechanism (E-a=0.27 eV) under 98 %RH. The present unique water channel structure provides an inspiration to create molecular porous materials. |
| Author | Huang, Rui‐Kang Hisaki, Ichiro Noro, Shin‐ichiro Chen, Xin Takahashi, Kiyonori Nakamura, Takayoshi |
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| Keywords | DESIGN Proton Conduction BONDED ORGANIC FRAMEWORKS COMPLEXES Crystal Engineering CROWN-ETHERS MOTIF Hydrogen Bond Crown Ether Porous Framework |
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| Snippet | A rigid hydrogen‐bonded organic framework (HOF) was constructed from a C3‐symmetric hexatopic carboxylic acid with a hydrophilic 18‐crown‐6‐ether (18C6)... A rigid hydrogen‐bonded organic framework (HOF) was constructed from a C 3 ‐symmetric hexatopic carboxylic acid with a hydrophilic 18‐crown‐6‐ether (18C6)... A rigid hydrogen-bonded organic framework (HOF) was constructed from a C-3-symmetric hexatopic carboxylic acid with a hydrophilic 18-crown-6-ether (18C6)... A rigid hydrogen-bonded organic framework (HOF) was constructed from a C3 -symmetric hexatopic carboxylic acid with a hydrophilic 18-crown-6-ether (18C6)... |
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| SubjectTerms | Carboxylic acids Chemistry Chemistry, Multidisciplinary Crown Ether Crystal Engineering Hydrogen Hydrogen Bond Hydrogen bonding Molecular structure Physical Sciences Porous Framework Porous materials Proton Conduction Protons Science & Technology |
| Title | A Proton Conductive Porous Framework of an 18‐Crown‐6‐Ether Derivative Networked by Rigid Hydrogen Bonding Modules |
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