Local shrinkage and stress induced by thermo-oxidation in composite materials at high temperatures

• Published in: Journal of the mechanics and physics of solids Vol. 59; no. 3; pp. 696 - 712
• Main Authors: Gigliotti, Marco, Olivier, Loic, Vu, Dinh Quy, Grandidier, Jean-Claude, Christine Lafarie-Frenot, Marie
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.03.2011
• Subjects: Assessments; Carbon; Composite materials; Computer simulation; Confocal interferometric microscopy; Damage onset; High temperature; Irreversible processes; Mathematical models; Matrix shrinkage; Multiphysical modelling; Shrinkage; Stresses; Thermo-oxidation; Multiphysical modelling; Confocal interferometric microscopy; Matrix shrinkage; Damage onset; Thermo-oxidation
• ISSN: 0022-5096
• DOI: 10.1016/j.jmps.2010.12.001

The paper is concerned with the modelling, simulation and experimental characterisation of local shrinkage strains and stresses induced by thermo-oxidation phenomena in the IM7/977-2 carbon/epoxy composite material at elevated temperatures. The oxygen concentration and mechanical fields were established through a coupled model constructed from a unified multiphysical approach and the thermodynamics of irreversible processes. The model was implemented in the ABAQUS ® finite element commercial code. Simulations of thermo-oxidation-induced matrix shrinkage were run at a local scale, i.e., the scale of the elementary constituents of the composite, the fibre and the matrix. The experimental assessment was done at the same scale, and the local matrix shrinkage profiles were measured by confocal interferometric microscopy. A good agreement was found between the simulated and measured profiles, validating the unified model. The thermo-oxidation induced stress field was analysed to understand the influence of the environment on the onset of damage in composite materials at elevated temperature.