Long Chain Perfluorinated Alkyl Acids Derivatisation and Identification in Biota and Abiota Matrices Using Gas Chromatography
An analytical method involving derivatisation of perfluorocarboxylic acids for their analysis in abiotic and biotic matrices is presented. Derivatisation of the acid group to form a suitable alkyl ester provided a suitable compound for mass spectrometric detection in gas chromatography/mass spectros...
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Published in | Bulletin of environmental contamination and toxicology Vol. 83; no. 5; pp. 630 - 635 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
Published |
New York
New York : Springer-Verlag
01.11.2009
Springer-Verlag Springer Nature B.V |
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Abstract | An analytical method involving derivatisation of perfluorocarboxylic acids for their analysis in abiotic and biotic matrices is presented. Derivatisation of the acid group to form a suitable alkyl ester provided a suitable compound for mass spectrometric detection in gas chromatography/mass spectroscopy (GC/MS) instrumental analysis. The acid is esterified by an alkyl halide i.e. benzyl bromide as the alkylating agent for perfluorocarboxylic acids quantification in fish and water by GC/MS. The gas chromatography method can be applied in the analysis perfluoro alkyl acids in water and biological matrices, especially where high levels of these compounds are expected. Typical values for precision obtained were 0.1%-10.0% with concentrations ranging from 0.2 to 1 μg/mL). Results demonstrate that GC/MS can supplement liquid chromatographic/mass spectroscopy method for quantification of fluorocarboxylic acid surfactants. The result indicates that there is need for more research on method analysis of perfluorinated acids in environmental matrices. |
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AbstractList | An analytical method involving derivatisation of perfluorocarboxylic acids for their analysis in abiotic and biotic matrices is presented. Derivatisation of the acid group to form a suitable alkyl ester provided a suitable compound for mass spectrometric detection in gas chromatography/mass spectroscopy (GC/MS) instrumental analysis. The acid is esterified by an alkyl halide i.e. benzyl bromide as the alkylating agent for perfluorocarboxylic acids quantification in fish and water by GC/MS. The gas chromatography method can be applied in the analysis perfluoro alkyl acids in water and biological matrices, especially where high levels of these compounds are expected. Typical values for precision obtained were 0.1%-10.0% with concentrations ranging from 0.2 to 1 μg/mL). Results demonstrate that GC/MS can supplement liquid chromatographic/mass spectroscopy method for quantification of fluorocarboxylic acid surfactants. The result indicates that there is need for more research on method analysis of perfluorinated acids in environmental matrices. [PUBLICATION ABSTRACT] An analytical method involving derivatisation of perfluorocarboxylic acids for their analysis in abiotic and biotic matrices is presented. Derivatisation of the acid group to form a suitable alkyl ester provided a suitable compound for mass spectrometric detection in gas chromatography/mass spectroscopy (GC/MS) instrumental analysis. The acid is esterified by an alkyl halide i.e. benzyl bromide as the alkylating agent for perfluorocarboxylic acids quantification in fish and water by GC/MS. The gas chromatography method can be applied in the analysis perfluoro alkyl acids in water and biological matrices, especially where high levels of these compounds are expected. Typical values for precision obtained were 0.1%-10.0% with concentrations ranging from 0.2 to 1 microg/mL). Results demonstrate that GC/MS can supplement liquid chromatographic/mass spectroscopy method for quantification of fluorocarboxylic acid surfactants. The result indicates that there is need for more research on method analysis of perfluorinated acids in environmental matrices. An analytical method involving derivatisation of perfluorocarboxylic acids for their analysis in abiotic and biotic matrices is presented. Derivatisation of the acid group to form a suitable alkyl ester provided a suitable compound for mass spectrometric detection in gas chromatography/mass spectroscopy (GC/MS) instrumental analysis. The acid is esterified by an alkyl halide i.e. benzyl bromide as the alkylating agent for perfluorocarboxylic acids quantification in fish and water by GC/MS. The gas chromatography method can be applied in the analysis perfluoro alkyl acids in water and biological matrices, especially where high levels of these compounds are expected. Typical values for precision obtained were 0.1%-10.0% with concentrations ranging from 0.2 to 1kg/mL). Results demonstrate that GC/MS can supplement liquid chromatographic/mass spectroscopy method for quantification of fluorocarboxylic acid surfactants. The result indicates that there is need for more research on method analysis of perfluorinated acids in environmental matrices. An analytical method involving derivatisation of perfluorocarboxylic acids for their analysis in abiotic and biotic matrices is presented. Derivatisation of the acid group to form a suitable alkyl ester provided a suitable compound for mass spectrometric detection in gas chromatography/mass spectroscopy (GC/MS) instrumental analysis. The acid is esterified by an alkyl halide i.e. benzyl bromide as the alkylating agent for perfluorocarboxylic acids quantification in fish and water by GC/MS. The gas chromatography method can be applied in the analysis perfluoro alkyl acids in water and biological matrices, especially where high levels of these compounds are expected. Typical values for precision obtained were 0.1%–10.0% with concentrations ranging from 0.2 to 1 μg/mL). Results demonstrate that GC/MS can supplement liquid chromatographic/mass spectroscopy method for quantification of fluorocarboxylic acid surfactants. The result indicates that there is need for more research on method analysis of perfluorinated acids in environmental matrices. An analytical method involving derivatisation of perfluorocarboxylic acids for their analysis in abiotic and biotic matrices is presented. Derivatisation of the acid group to form a suitable alkyl ester provided a suitable compound for mass spectrometric detection in gas chromatography/mass spectroscopy (GC/MS) instrumental analysis. The acid is esterified by an alkyl halide i.e. benzyl bromide as the alkylating agent for perfluorocarboxylic acids quantification in fish and water by GC/MS. The gas chromatography method can be applied in the analysis perfluoro alkyl acids in water and biological matrices, especially where high levels of these compounds are expected. Typical values for precision obtained were 0.1%-10.0% with concentrations ranging from 0.2 to 1 μg/mL). Results demonstrate that GC/MS can supplement liquid chromatographic/mass spectroscopy method for quantification of fluorocarboxylic acid surfactants. The result indicates that there is need for more research on method analysis of perfluorinated acids in environmental matrices. |
Author | Quinete, Natalia Wilken, Rolf-Dieter Orata, Francis |
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CitedBy_id | crossref_primary_10_1007_s00128_012_0685_9 crossref_primary_10_1007_s10337_019_03850_6 crossref_primary_10_1002_ansa_202000089 crossref_primary_10_1007_s11356_018_3483_z crossref_primary_10_1016_j_microc_2023_109667 crossref_primary_10_1007_s00216_012_6492_7 crossref_primary_10_1016_j_chemosphere_2011_12_029 crossref_primary_10_1007_s10661_016_5534_6 crossref_primary_10_1016_j_aca_2016_10_026 crossref_primary_10_1002_ieam_4352 crossref_primary_10_1016_j_chroma_2020_461132 |
Cites_doi | 10.1093/toxsci/kfm128 10.1016/j.chroma.2005.07.053 10.1007/s00216-006-0557-4 10.1093/toxsci/kfm110 10.1016/0003-2697(80)90202-X 10.1007/BF01055778 10.1021/es020955c 10.1021/es981355+ 10.1021/es001489z 10.1039/b108463c 10.1897/1551-5028(2003)022<0196:BATDOP>2.0.CO;2 10.1002/etc.5620220126 |
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Keywords | Water Fish muscles Benzyl esters Perfluorinated alkyl acids GC/MS Derivatisation |
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References | Taniyasu, Kannan, So, Gulkowska, Sinclair, Okazawa, Yamashita (CR11) 2005; 1093 Hebert, Odom, Craig, Dick, Strauss (CR5) 2002; 4 Olsen, Hansen, Stevenson, Burris, Mandel (CR9) 2003; 37 Lau, Thibodeaux, Hanson, Narotsky, Rogers, Lindstrom, Strynar (CR6) 2006; 99 Abbott, Wolf, Schmid, Das, Zehr, Helfant, Nakayama, Lindstrom, Strynar, Lau (CR1) 2007; 98 Moody, Field (CR8) 1999; 33 Hansen, Clemen, Ellefson, Johnson (CR4) 2001; 35 Belisle, Hagen (CR2) 1980; 101 Martin, Mabury, Solomon, Muir (CR7) 2003; 22 Gonza’lez-Barreiro, Martı’nez-Carballo, Sitka, Scharf, Gans (CR3) 2006; 386 Sinclair, Taniyasu, Yamashita, Kannan (CR10) 2004; 66 Ylinen, Hanhijarvi, Peura, Ramo (CR12) 1985; 14 KJ Hansen (9756_CR4) 2001; 35 C Lau (9756_CR6) 2006; 99 J Belisle (9756_CR2) 1980; 101 BD Abbott (9756_CR1) 2007; 98 GN Hebert (9756_CR5) 2002; 4 GW Olsen (9756_CR9) 2003; 37 S Taniyasu (9756_CR11) 2005; 1093 C Gonza’lez-Barreiro (9756_CR3) 2006; 386 JW Martin (9756_CR7) 2003; 22 CA Moody (9756_CR8) 1999; 33 E Sinclair (9756_CR10) 2004; 66 M Ylinen (9756_CR12) 1985; 14 |
References_xml | – volume: 99 start-page: 366 issue: 2 year: 2006 end-page: 394 ident: CR6 article-title: Effects of perfluorooctanoic acid exposure during pregnancy in the mouse publication-title: Toxicol Sci doi: 10.1093/toxsci/kfm128 contributor: fullname: Strynar – volume: 66 start-page: 4069 year: 2004 end-page: 4073 ident: CR10 article-title: Perfluoroocatanoic acid and perfluoroocatane sulfonate in Michigan and New York waters publication-title: Organohalog Compd contributor: fullname: Kannan – volume: 1093 start-page: 89 year: 2005 end-page: 97 ident: CR11 article-title: Analysis of fluorotelomer alcohols, fluortelomer acids and short- and long-chain perfluorinated acids in water and biota publication-title: J Chromatogr A doi: 10.1016/j.chroma.2005.07.053 contributor: fullname: Yamashita – volume: 386 start-page: 7 year: 2006 end-page: 8 ident: CR3 article-title: Method optimization for determination of selected perfluorinated alkylated substances in water samples publication-title: Anal Bioanal Chem doi: 10.1007/s00216-006-0557-4 contributor: fullname: Gans – volume: 98 start-page: 571 issue: 2 year: 2007 end-page: 581 ident: CR1 article-title: Perfluorooctanoic acid induced developmental toxicity in the mouse is dependent on expression of peroxisome proliferators activated receptor-alpha publication-title: Toxicol Sci doi: 10.1093/toxsci/kfm110 contributor: fullname: Lau – volume: 101 start-page: 369 year: 1980 end-page: 376 ident: CR2 article-title: A method for the determination of perfluorooctanoic acid in blood and other biological samples publication-title: Anal Biochem doi: 10.1016/0003-2697(80)90202-X contributor: fullname: Hagen – volume: 14 start-page: 713 year: 1985 end-page: 717 ident: CR12 article-title: Quantitative gas chromatographic determination of perfluorooctanoic acid as the benzyl ester in plasma and urine publication-title: Arch Environ Contam Toxicol doi: 10.1007/BF01055778 contributor: fullname: Ramo – volume: 37 start-page: 888 year: 2003 end-page: 891 ident: CR9 article-title: Human donor liver and serum concentrations of perfluorooctanesulfonate and other perfluorochemicals publication-title: Environ Sci Technol doi: 10.1021/es020955c contributor: fullname: Mandel – volume: 33 start-page: 2800 year: 1999 end-page: 2806 ident: CR8 article-title: Determination of perfluorocarboxylates in groundwater impacted by fire-fighting activity publication-title: Environ Sci Technol doi: 10.1021/es981355+ contributor: fullname: Field – volume: 35 start-page: 766 year: 2001 end-page: 770 ident: CR4 article-title: Compound-specific, quantitative characterization of organic fluorochemicals in biological matrices publication-title: Environ Sci Technol doi: 10.1021/es001489z contributor: fullname: Johnson – volume: 4 start-page: 90 year: 2002 end-page: 95 ident: CR5 article-title: Method for the determination of sub-ppm concentrations of perfluoroalkylsulfonate anions in water publication-title: J Environ Monitor doi: 10.1039/b108463c contributor: fullname: Strauss – volume: 22 start-page: 196 year: 2003 end-page: 204 ident: CR7 article-title: Identification of long-chain perfluorinated acids in biota from the Canadian arctic publication-title: Environ Toxicol Chem doi: 10.1897/1551-5028(2003)022<0196:BATDOP>2.0.CO;2 contributor: fullname: Muir – volume: 99 start-page: 366 issue: 2 year: 2006 ident: 9756_CR6 publication-title: Toxicol Sci doi: 10.1093/toxsci/kfm128 contributor: fullname: C Lau – volume: 14 start-page: 713 year: 1985 ident: 9756_CR12 publication-title: Arch Environ Contam Toxicol doi: 10.1007/BF01055778 contributor: fullname: M Ylinen – volume: 35 start-page: 766 year: 2001 ident: 9756_CR4 publication-title: Environ Sci Technol doi: 10.1021/es001489z contributor: fullname: KJ Hansen – volume: 33 start-page: 2800 year: 1999 ident: 9756_CR8 publication-title: Environ Sci Technol doi: 10.1021/es981355+ contributor: fullname: CA Moody – volume: 386 start-page: 7 year: 2006 ident: 9756_CR3 publication-title: Anal Bioanal Chem doi: 10.1007/s00216-006-0557-4 contributor: fullname: C Gonza’lez-Barreiro – volume: 37 start-page: 888 year: 2003 ident: 9756_CR9 publication-title: Environ Sci Technol doi: 10.1021/es020955c contributor: fullname: GW Olsen – volume: 98 start-page: 571 issue: 2 year: 2007 ident: 9756_CR1 publication-title: Toxicol Sci doi: 10.1093/toxsci/kfm110 contributor: fullname: BD Abbott – volume: 101 start-page: 369 year: 1980 ident: 9756_CR2 publication-title: Anal Biochem doi: 10.1016/0003-2697(80)90202-X contributor: fullname: J Belisle – volume: 4 start-page: 90 year: 2002 ident: 9756_CR5 publication-title: J Environ Monitor doi: 10.1039/b108463c contributor: fullname: GN Hebert – volume: 66 start-page: 4069 year: 2004 ident: 9756_CR10 publication-title: Organohalog Compd contributor: fullname: E Sinclair – volume: 22 start-page: 196 year: 2003 ident: 9756_CR7 publication-title: Environ Toxicol Chem doi: 10.1002/etc.5620220126 contributor: fullname: JW Martin – volume: 1093 start-page: 89 year: 2005 ident: 9756_CR11 publication-title: J Chromatogr A doi: 10.1016/j.chroma.2005.07.053 contributor: fullname: S Taniyasu |
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SubjectTerms | Acids - chemistry Animals Aquatic Pollution Biota Calibration Chemical compounds Chromatography Chromatography, Gas - methods Contamination Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Esterification Fishes Fluorocarbons - analysis Fluorocarbons - chemistry Gas chromatography Gas Chromatography-Mass Spectrometry Mass spectrometry Mass spectroscopy Pollution Soil Science & Conservation Waste Water Technology Water Management Water Pollutants, Chemical - analysis Water Pollution Control |
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Title | Long Chain Perfluorinated Alkyl Acids Derivatisation and Identification in Biota and Abiota Matrices Using Gas Chromatography |
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