On Shear Testing of Single Crystal Ni-Base Superalloys

• Published in: Metallurgical and materials transactions. A, Physical metallurgy and materials science Vol. 49; no. 9; pp. 3951 - 3962
• Main Authors: Eggeler, G., Wieczorek, N., Fox, F., Berglund, S., Bürger, D., Dlouhy, A., Wollgramm, P., Neuking, K., Schreuer, J., Agudo Jácome, L., Gao, S., Hartmaier, A., Laplanche, G.
• Format: Journal Article
• Language: English
• Published: New York Springer US 01.09.2018; Springer Nature B.V
• Subjects: Characterization and Evaluation of Materials; Chemistry and Materials Science; Creep strength; Creep tests; Crystallography; Dislocations; Materials Science; Metallic Materials; Microstructure; Nanotechnology; Nickel base alloys; Plastic deformation; Shear creep; Shear stress; Shear tests; Single crystals; Specimen geometry; Structural Materials; Substructures (crystalline); Superalloys; Surfaces and Interfaces; Thin Films; Third European Symposium on Superalloys and their Applications; Topical Collection: Superalloys and Their Applications
• ISSN: 1073-5623; 1543-1940
• DOI: 10.1007/s11661-018-4726-9

Shear testing can contribute to a better understanding of the plastic deformation of Ni-base superalloy single crystals. In the present study, shear testing is discussed with special emphasis placed on its strengths and weaknesses. Key mechanical and microstructural results which were obtained for the high-temperature ( T  ≈ 1000 °C) and low-stress ( τ  ≈ 200 MPa) creep regime are briefly reviewed. New 3D stereo STEM images of dislocation substructures which form during shear creep deformation in this regime are presented. It is then shown which new aspects need to be considered when performing double shear creep testing at lower temperatures ( T  < 800 °C) and higher stresses ( τ  > 600 MPa). In this creep regime, the macroscopic crystallographic [11−2](111) shear system deforms significantly faster than the [01−1](111) system. This represents direct mechanical evidence for a new planar fault nucleation scenario, which was recently suggested (Wu et al . in Acta Mater 144:642–655, 2018 ). The double shear creep specimen geometry inspired a micro-mechanical in-situ shear test specimen. Moreover, the in-situ SEM shear specimen can be FIB micro-machined from prior dendritic and interdendritic regions. Dendritic regions, which have a lower γ ′ volume fraction, show a lower critical resolved shear stress.