NMR and conformational studies of new 5-phenylpyrrole-carboxamide derivatives
The 1H and 13C NMR resonances of 22 5‐(5‐substituted‐2‐nitrophenyl)‐1H‐pyrrole‐2‐carboxamides, 22 5‐(5‐substituted‐2‐aminophenyl)‐1H‐pyrrole‐2‐carboxamides, and 9 5‐phenyl‐1H‐pyrrole‐2‐carboxamides were assigned completely using the concerted application of one‐ and two‐dimensional experiments (DEPT...
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Published in | Magnetic resonance in chemistry Vol. 47; no. 12; pp. 1101 - 1109 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
Published |
Chichester, UK
John Wiley & Sons, Ltd
01.12.2009
Wiley |
Subjects | |
Online Access | Get full text |
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Summary: | The 1H and 13C NMR resonances of 22 5‐(5‐substituted‐2‐nitrophenyl)‐1H‐pyrrole‐2‐carboxamides, 22 5‐(5‐substituted‐2‐aminophenyl)‐1H‐pyrrole‐2‐carboxamides, and 9 5‐phenyl‐1H‐pyrrole‐2‐carboxamides were assigned completely using the concerted application of one‐ and two‐dimensional experiments (DEPT, gs‐HMQC and gs‐HMBC). NOE studies and conformational analysis confirm the preferred conformations of such compounds. Copyright © 2009 John Wiley & Sons, Ltd.
The 1H and 13C NMR resonances of 53 5‐(2,5‐disubstitutedphenyl)‐1H‐pyrrole‐2‐carboxamides were assigned completely. NOE studies and conformational analysis confirm the preferred conformation of such compounds. |
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Bibliography: | istex:7FE0D443898DBBC9B500DF4338FC8DCD37680AC4 Junta de Andalucia - No. P06-CTS-01941 ArticleID:MRC2524 Ministerio de Ciencia y Tecnología - No. SAF2005-07991-C02-02 ark:/67375/WNG-DXLH8DNF-2 ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 ObjectType-Article-2 ObjectType-Feature-1 |
ISSN: | 0749-1581 1097-458X 1097-458X |
DOI: | 10.1002/mrc.2524 |