Rapid In Situ Synthesis of Spherical Microflower Pt/C Catalyst Via Spray-drying for High Performance Fuel Cell Application

A facile route for the rapid in situ synthesis of platinum nanoparticles on spherical microflower carbon has been developed. An aqueous precursor slurry containing carbon black, polystyrene latex (PSL), polyvinyl alcohol, and platinum salt was spray‐dried, followed by calcination to simultaneously r...

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Published inFuel cells (Weinheim an der Bergstrasse, Germany) Vol. 12; no. 4; pp. 665 - 669
Main Authors Balgis, R., Anilkumar, G. M., Sago, S., Ogi, T., Okuyama, K.
Format Journal Article
LanguageEnglish
Published Weinheim WILEY-VCH Verlag 01.08.2012
WILEY‐VCH Verlag
Wiley Subscription Services, Inc
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Summary:A facile route for the rapid in situ synthesis of platinum nanoparticles on spherical microflower carbon has been developed. An aqueous precursor slurry containing carbon black, polystyrene latex (PSL), polyvinyl alcohol, and platinum salt was spray‐dried, followed by calcination to simultaneously reduce platinum salt and to decompose PSL particles. Prepared Pt/C catalyst showed high‐performance electrocatalytic activity with excellent durability. The mass activity and specific activity values were 132.26 mA mg–1 Pt and 207.62 μA cm–2 Pt, respectively. This work presents a future direction for the production of high‐performance Pt/C catalyst in an industrial scale.
Bibliography:ark:/67375/WNG-W309BRN1-T
Ministry of Education, Culture, Sports, Science, and Technology (MEXT) - No. 22246099
ArticleID:FUCE201200070
istex:9C594495FEFF0A1B549DA464A3C508D729169E51
ISSN:1615-6846
1615-6854
DOI:10.1002/fuce.201200070