Influence of Factors in the Photopolymerization Process on Dental Composites Microhardness

• Published in: Materials Vol. 15; no. 18; p. 6459
• Main Authors: Maximov, Jordan, Dikova, Tsanka, Duncheva, Galya, Georgiev, Georgi
• Format: Journal Article
• Language: English
• Published: Basel MDPI AG 17.09.2022; MDPI
• Subjects: Adaptation; Composite materials; Curing; Dental cement; Dental materials; Dental matrices; Design of experiments; Diamond pyramid hardness; Hardness; irradiation time; layer thickness; Light; light intensity; light-cured dental composites; Luminous intensity; Measurement; Mechanical properties; microhardness; Photopolymerization; Photopolymers; Polymerization; Regression analysis; Testing; Thickness; Variance analysis; Viscosity; Bulgaria
• ISSN: 1996-1944; 1996-1944
• DOI: 10.3390/ma15186459

The aim of the present paper is to investigate the influence of factors in photopolymerization process that govern microhardness of three types of dental composites—universal (UC), bulk-fill (BC), and flowable (FC). Cylindrical specimens with different thicknesses are made and light cured. The significance of light intensity, irradiation time, and layer thickness on Vickers microhardness is evaluated by experimental design, analysis of variance, and regression analysis. It is found that the main factor influencing the microhardness on the top surface of the three composites is light intensity. The second factor is layer thickness for the UC and FC, while for BC, it is curing time. The third factor is curing time for the first two composites and layer thickness for bulk-fill. The significance of factors’ influence on the microhardness of the bottom surface is the same for the UC and FC, but different for BC. The main factor for the first two composites is layer thickness, followed by curing time and light intensity. For bulk-fill, curing time is main factor, light intensity is second, and layer thickness is last. Different significance of factors influencing the microhardness on top and bottom surfaces of investigated composites is revealed for the first time in the present study.