Visible‐Light‐Promoted Cascade Radical Cyclization: Synthesis of 1,4‐Diketones Containing Chroman‐4‐One Skeletons
A visible‐light‐induced cascade radical cyclization of aroyl chlorides with 2‐(allyloxy)‐benzaldehyde derivatives has been developed. The method takes advantages of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4‐diketones bearing bio...
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| Published in | Chemistry, an Asian journal Vol. 14; no. 19; pp. 3269 - 3273 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Germany
Wiley Subscription Services, Inc
01.10.2019
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| Abstract | A visible‐light‐induced cascade radical cyclization of aroyl chlorides with 2‐(allyloxy)‐benzaldehyde derivatives has been developed. The method takes advantages of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4‐diketones bearing biologically important chroman‐4‐one skeletons with moderate to good yields.
A visible‐light‐induced cascade radical cyclization of aroyl chlorides with 2‐(allyloxy)‐benzaldehyde derivatives has been developed. The method takes advantage of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4‐diketones bearing biologically important chroman‐4‐one skeletons in moderate to good yields. |
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| AbstractList | A visible‐light‐induced cascade radical cyclization of aroyl chlorides with 2‐(allyloxy)‐benzaldehyde derivatives has been developed. The method takes advantages of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4‐diketones bearing biologically important chroman‐4‐one skeletons with moderate to good yields. A visible-light-induced cascade radical cyclization of aroyl chlorides with 2-(allyloxy)-benzaldehyde derivatives has been developed. The method takes advantages of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4-diketones bearing biologically important chroman-4-one skeletons with moderate to good yields.A visible-light-induced cascade radical cyclization of aroyl chlorides with 2-(allyloxy)-benzaldehyde derivatives has been developed. The method takes advantages of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4-diketones bearing biologically important chroman-4-one skeletons with moderate to good yields. A visible‐light‐induced cascade radical cyclization of aroyl chlorides with 2‐(allyloxy)‐benzaldehyde derivatives has been developed. The method takes advantages of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4‐diketones bearing biologically important chroman‐4‐one skeletons with moderate to good yields. A visible‐light‐induced cascade radical cyclization of aroyl chlorides with 2‐(allyloxy)‐benzaldehyde derivatives has been developed. The method takes advantage of unactivated C=C bonds as the acyl radical acceptors and offers a mild and green approach for the synthesis of 1,4‐diketones bearing biologically important chroman‐4‐one skeletons in moderate to good yields. |
| Author | Wang, Long He, Xiang‐Kui Xuan, Jun Cai, Bao‐Gui Yang, Qing‐Qing |
| Author_xml | – sequence: 1 givenname: Xiang‐Kui surname: He fullname: He, Xiang‐Kui organization: Anhui University – sequence: 2 givenname: Bao‐Gui surname: Cai fullname: Cai, Bao‐Gui organization: Anhui University – sequence: 3 givenname: Qing‐Qing surname: Yang fullname: Yang, Qing‐Qing organization: China Three Gorges University – sequence: 4 givenname: Long surname: Wang fullname: Wang, Long email: wanglongchem@ctgu.edu.cn organization: China Three Gorges University – sequence: 5 givenname: Jun orcidid: 0000-0003-0578-9330 surname: Xuan fullname: Xuan, Jun email: xuanjun@ahu.edu.cn organization: Ministry of Education |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31464012$$D View this record in MEDLINE/PubMed |
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| Keywords | Photoredox catalysis Radical cyclization Visible light Acyl radical 1,4-Diketones |
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| Snippet | A visible‐light‐induced cascade radical cyclization of aroyl chlorides with 2‐(allyloxy)‐benzaldehyde derivatives has been developed. The method takes... A visible-light-induced cascade radical cyclization of aroyl chlorides with 2-(allyloxy)-benzaldehyde derivatives has been developed. The method takes... |
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| SubjectTerms | 1,4-Diketones Acyl radical Benzaldehyde Chemistry Diketones Photoredox catalysis Radical cyclization Synthesis Visible light |
| Title | Visible‐Light‐Promoted Cascade Radical Cyclization: Synthesis of 1,4‐Diketones Containing Chroman‐4‐One Skeletons |
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