Fe-g-C3N4/graphitized mesoporous carbon composite as an effective Fenton-like catalyst in a wide pH range
[Display omitted] •Modified g-C3N4 is used as a Fenton-like catalyst in a wide pH range.•The prepared Fe-g-C3N4/GMC catalyst is adaptable to different organic pollutants.•Fe-N centers as active sites were proved.•The enhancement of electron transfer is responsive for these excellent performances. He...
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| Published in | Applied catalysis. B, Environmental Vol. 201; pp. 232 - 240 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.02.2017
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Modified g-C3N4 is used as a Fenton-like catalyst in a wide pH range.•The prepared Fe-g-C3N4/GMC catalyst is adaptable to different organic pollutants.•Fe-N centers as active sites were proved.•The enhancement of electron transfer is responsive for these excellent performances.
Heterogeneous Fe-N complexes are a kind of promising catalysts for the Fenton-like reaction. The present study selected a stable and inexpensive g-C3N4 as the chelating agent and combined with the graphitized mesoporous carbon (GMC). The fabricated Fe-g-C3N4/GMC composite was characterized by several techniques including FTIR, XRD, XPS, TEM and STXM. Results showed clear sheets of g-C3N4 and graphite with Fe evenly distributed mostly in the Fe-N coordination form. The catalyst expressed high activity in the Fenton-like reaction in a wide pH range of 4–10. 99.2% removal of Acid Red 73 was obtained in 40min, and the degradation data well fitted with the pseudo-first-order kinetics model. By correlating the constant of reaction rates calculated from the model and the Fe speciation contents of the samples prepared at different conditions, we deduced that Fe-N species are the most important active sites for the Fenton-like reaction. More importantly, hydroxyl radicals played a great role in the whole reaction yet their generation was independent of visible light. Cyclic voltammetry results confirmed that the GMC can accelerate the Fe(III)/Fe(II) redox cycle by enhancing electron transfer, and thus enable this Fenton-like catalyst to perform well in a wide pH range. |
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| AbstractList | [Display omitted]
•Modified g-C3N4 is used as a Fenton-like catalyst in a wide pH range.•The prepared Fe-g-C3N4/GMC catalyst is adaptable to different organic pollutants.•Fe-N centers as active sites were proved.•The enhancement of electron transfer is responsive for these excellent performances.
Heterogeneous Fe-N complexes are a kind of promising catalysts for the Fenton-like reaction. The present study selected a stable and inexpensive g-C3N4 as the chelating agent and combined with the graphitized mesoporous carbon (GMC). The fabricated Fe-g-C3N4/GMC composite was characterized by several techniques including FTIR, XRD, XPS, TEM and STXM. Results showed clear sheets of g-C3N4 and graphite with Fe evenly distributed mostly in the Fe-N coordination form. The catalyst expressed high activity in the Fenton-like reaction in a wide pH range of 4–10. 99.2% removal of Acid Red 73 was obtained in 40min, and the degradation data well fitted with the pseudo-first-order kinetics model. By correlating the constant of reaction rates calculated from the model and the Fe speciation contents of the samples prepared at different conditions, we deduced that Fe-N species are the most important active sites for the Fenton-like reaction. More importantly, hydroxyl radicals played a great role in the whole reaction yet their generation was independent of visible light. Cyclic voltammetry results confirmed that the GMC can accelerate the Fe(III)/Fe(II) redox cycle by enhancing electron transfer, and thus enable this Fenton-like catalyst to perform well in a wide pH range. |
| Author | Yang, Qunfeng Liu, Weiping Ma, Jianqing Wen, Yuezhong |
| Author_xml | – sequence: 1 givenname: Jianqing surname: Ma fullname: Ma, Jianqing organization: Institute of Environmental Science, College of Environmental and Resource Sciences, Zhejiang University, Hangzhou 310058, China – sequence: 2 givenname: Qunfeng surname: Yang fullname: Yang, Qunfeng organization: Institute of Environmental Science, College of Environmental and Resource Sciences, Zhejiang University, Hangzhou 310058, China – sequence: 3 givenname: Yuezhong surname: Wen fullname: Wen, Yuezhong email: wenyuezhong@zju.edu.cn organization: Institute of Environmental Science, College of Environmental and Resource Sciences, Zhejiang University, Hangzhou 310058, China – sequence: 4 givenname: Weiping surname: Liu fullname: Liu, Weiping organization: Institute of Environmental Science, College of Environmental and Resource Sciences, Zhejiang University, Hangzhou 310058, China |
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•Modified g-C3N4 is used as a Fenton-like catalyst in a wide pH range.•The prepared Fe-g-C3N4/GMC catalyst is adaptable to different organic... |
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| Title | Fe-g-C3N4/graphitized mesoporous carbon composite as an effective Fenton-like catalyst in a wide pH range |
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