A Novel Study on the Effect of Tool Offset in Friction Stir Processing for Mg-NiTi Composite

• Published in: Crystals (Basel) Vol. 12; no. 11; p. 1651
• Main Authors: Lone, Nadeem, Bajaj, Dhruv, Gangil, Namrata, Mohammed, Sohail, Chen, Daolun, Siddiquee, Arshad
• Format: Journal Article
• Language: English
• Published: Basel MDPI AG 01.11.2022
• Subjects: Alloys; Base metal; Biocompatibility; defect morphology; Defects; Friction stir processing; Friction stir welding; Heat; Homogenization; Intermetallic compounds; Magnesium; Metal matrix composites; Mg-NiTi; Morphology; Nickel base alloys; Nickel compounds; Nickel titanides; offset; Process parameters; Shape memory alloys; Temperature; Titanium compounds
• ISSN: 2073-4352; 2073-4352
• DOI: 10.3390/cryst12111651

Mg-NiTi-based metal matrix composites are appropriate solutions for the two most important goals of material engineers in the present day, i.e., imparting functional behaviour and the light weighting of metallic structures. In recent years, due to its solid-state nature, the development of Mg-based metal matrix composites has largely benefited from friction stir processing. Despite the great effort of researchers in the domain of friction stir welding and processing, finding optimum process parameters for efficient material mixing and consolidation remains a rigorous and exhaustive challenge. Tool offset variation has been seen to aid the integrity and strength of friction stir welds; however, its effect upon the stir zone structure, material flow, particle distribution, and defect formation has not been investigated for friction stir processing. Therefore, the authors employed Mg as the base metal and NiTi shape memory alloy as the reinforcement to the targeted metal matrix composite. The tool offset was linearly varied by tilting the slotted length with respect to the traverse direction. Friction stir processing performed at a rotational speed of 560 rpm and traverse speed of 80 mm/min revealed crucial changes in defect morphology and area, which has been explicated with the quantified variation in tool offset from the advancing side to the retreating side. For the positive offset conditions, i.e., tool offset towards the advancing side, the shape of the tunnelling defect was chiefly convex from the outward direction. Meanwhile, for the negative offset conditions, i.e., tool offset towards the retreating side, the tunnelling defect exhibited a concave outward shape. A transition from rectangular to triangular morphology was also observed as the tool moved from an offset of 1.75 mm in the advancing side to 1.75 mm in the retreating side.