MOF-Derived Cu@N-C Catalyst for 1,3-Dipolar Cycloaddition Reaction

Cu(im)2-derived Cu@N-C composites were used for the first time as efficient heterogeneous catalysts for one-pot 1,3-dipolar cycloaddition of terminal alkynes, aryl halides, and sodium azide to preparation of 1,4-disubstituted 1,2,3-triazoles with broad substrate scope and high yields. The catalyst c...

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Published inNanomaterials (Basel, Switzerland) Vol. 12; no. 7; p. 1070
Main Authors Wang, Zhuangzhuang, Zhou, Xuehao, Gong, Shaofeng, Xie, Jianwei
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 24.03.2022
MDPI
Subjects
1,2,3-triazole
Alkynes
Catalysts
Chemistry
Chromatography
click chemistry
Copper
Cycloaddition
Halides
Heterogeneity
heterogeneous copper catalysts
High temperature
Leaching
Ligands
MOF-derived materials
Porous materials
Recyclability
Sodium azide
Sodium azides
Substrates
United States > US
China
click chemistry
heterogeneous copper catalysts
MOF-derived materials
1,2,3-triazole
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Summary:Cu(im)2-derived Cu@N-C composites were used for the first time as efficient heterogeneous catalysts for one-pot 1,3-dipolar cycloaddition of terminal alkynes, aryl halides, and sodium azide to preparation of 1,4-disubstituted 1,2,3-triazoles with broad substrate scope and high yields. The catalyst can be easily reused without the changes of structure and morphology, and the heterogeneity nature was confirmed from the catalyst recyclability and metal leaching test.
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ISSN:2079-4991
2079-4991
DOI:10.3390/nano12071070