Flexural test as an alternative to tensile test for bond strength of resin cement to zirconia

• Published in: Journal of the mechanical behavior of biomedical materials Vol. 119; p. 104525
• Main Authors: Shin, Yoojin, Kim, Youngmin, Cho, Byeong-Hoon
• Format: Journal Article
• Language: English
• Published: Netherlands Elsevier Ltd 01.07.2021
• Subjects: Dental bonding; Flexural strength; Statistical data analysis; Tensile strength; Zirconia ceramic; Statistical data analysis; Dental bonding; Zirconia ceramic; Tensile strength; Flexural strength
• ISSN: 1751-6161; 1878-0180
• DOI: 10.1016/j.jmbbm.2021.104525

There has been a great many technical difficulties in measuring the bond strengths between brittle dental substrates and materials, especially in preparing specimens. This study evaluated the validity of the relatively easy flexural bond strength (FBS) test in measuring bond strength of resin cement to zirconia as an alternative to the cumbersome tensile bond strength (TBS) and micro-tensile bond strength (MTBS) tests. The FBS and TBS of resin cement to zirconia were measured experimentally after three surface treatments on a zirconia ceramic: air abrasion only (A), conditioning with Single Bond Universal (U) after air abrasion, and conditioning with Z-Prime Plus (Z) after air abrasion. The data were investigated using two-way analysis of variance (ANOVA), Weibull statistics, and a theoretical simulation. In both the FBS and TBS tests, the experimental data were consistent and quantitatively similar. First, according to ANOVA, the U group showed the highest bond strengths in both tests, followed by the Z group and the A group. In each surface treatment group, the FBS was always higher than the TBS. Second, the Weibull fitting showed the same order of strength in both tests (A < Z < U) and in all surface treatment groups (FBS > TBS). Third, the theoretical ratios calculated from the Weibull moduli agreed well with the experimental ratios of the FBS to the TBS. The FBS test can be an alternative to the TBS and MTBS tests in measuring the bond strength of brittle resin cement to zirconia.