An in situ cell for small-angle scattering experiments on nano-structured catalysts
The design, construction and operation of an in situ cell covering the temperature range from room temperature to 870 K with the sample in a controlled gas flow is demonstrated. The setup is designed specifically for acquiring small angle X‐ray scattering data at the JUSIFA beam line at the Hamburge...
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Published in | Journal of applied crystallography Vol. 36; no. 3-1; pp. 812 - 813 |
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Main Authors | , , , , , , |
Format | Journal Article Conference Proceeding |
Language | English |
Published |
5 Abbey Square, Chester, Cheshire CH1 2HU, England
Munksgaard International Publishers
01.06.2003
Blackwell |
Subjects | |
Online Access | Get full text |
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Summary: | The design, construction and operation of an in situ cell covering the temperature range from room temperature to 870 K with the sample in a controlled gas flow is demonstrated. The setup is designed specifically for acquiring small angle X‐ray scattering data at the JUSIFA beam line at the Hamburger Synchrotronstrahlungslabor although it can be employed at other beam lines with only slight modifications. The cell is used for studying dynamic changes in size and morphology of nano structured catalyst particles. |
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Bibliography: | istex:9D2CAA70BBC9F1AE0B7BF5AF22DF86EAC69A5341 ark:/67375/WNG-J1XM8CF2-P ArticleID:JCRKS7503 |
ISSN: | 1600-5767 0021-8898 1600-5767 |
DOI: | 10.1107/S002188980300061X |