Sample environment issues relevant to the acquisition of inelastic neutron scattering measurements of heterogeneous catalyst samples

Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laborat...

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Published inJournal of physics. Conference series Vol. 554; no. 1; pp. 12005 - 12
Main Authors Warringham, R, Bellaire, D, Parker, S F, Taylor, J, Ewings, R A, Goodway, C M, Kibble, M, Wakefield, S R, Jura, M, Dudman, M P, Tooze, R P, Webb, P B, Lennon, D
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LanguageEnglish
Published Bristol IOP Publishing 01.01.2014
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Abstract Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laboratory space and ventilation facilities that are suited to the increasingly wide range of catalytic samples being examined. INS measurements for CO hydrogenation over an iron-based Fischer-Tropsch catalyst recorded using the MARI spectrometer are presented to illustrate the applicability of the new arrangements.
AbstractList Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laboratory space and ventilation facilities that are suited to the increasingly wide range of catalytic samples being examined. INS measurements for CO hydrogenation over an iron-based Fischer-Tropsch catalyst recorded using the MARI spectrometer are presented to illustrate the applicability of the new arrangements.
Author Webb, P B
Lennon, D
Kibble, M
Taylor, J
Ewings, R A
Goodway, C M
Parker, S F
Wakefield, S R
Jura, M
Bellaire, D
Warringham, R
Dudman, M P
Tooze, R P
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Cites_doi 10.1016/S0360-0564(06)51003-X
10.1039/b505974g
10.1142/5628
10.1016/j.jcat.2010.09.001
10.1016/j.cattod.2006.02.041
10.1021/j100462a011
10.1016/j.cattod.2010.07.009
10.1021/ja0381398
10.1016/0021-9517(89)90342-4
10.1002/anie.201210179
10.1021/jp0405963
10.1016/j.jcat.2006.07.012
10.1039/c3ra42435a
10.1016/j.jcat.2014.02.004
10.1006/jcat.1995.1247
10.1021/cs4006088
10.1016/0021-9517(81)90025-7
10.1016/0021-9517(85)90379-3
10.1016/0021-9517(86)90043-6
10.1366/11-06456
10.1002/1521-3773(20020104)41:1<144::AID-ANIE144>3.0.CO;2-J
10.1039/c2cp42745a
10.1016/j.chemphys.2013.10.012
10.1063/1.3553295
10.1016/S0920-5861(01)00334-0
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References 22
23
26
27
Silverwood I P (12) 2011; 82
Arai M (25) 1992
10
11
Mitchell P C H (15) 2005
13
14
16
17
Dry M E (24) 1982; 12
18
19
1
2
3
4
5
6
7
8
9
20
21
References_xml – ident: 1
  doi: 10.1016/S0360-0564(06)51003-X
– ident: 2
  doi: 10.1039/b505974g
– year: 2005
  ident: 15
  publication-title: Vibrational spectroscopy using neutrons.
  doi: 10.1142/5628
  contributor:
    fullname: Mitchell P C H
– ident: 21
  doi: 10.1016/j.jcat.2010.09.001
– ident: 7
  doi: 10.1016/j.cattod.2006.02.041
– ident: 19
  doi: 10.1021/j100462a011
– ident: 8
  doi: 10.1016/j.cattod.2010.07.009
– ident: 14
  doi: 10.1021/ja0381398
– ident: 23
  doi: 10.1016/0021-9517(89)90342-4
– ident: 20
  doi: 10.1002/anie.201210179
– ident: 3
  doi: 10.1021/jp0405963
– ident: 26
  doi: 10.1016/j.jcat.2006.07.012
– ident: 10
  doi: 10.1039/c3ra42435a
– ident: 16
  doi: 10.1016/j.jcat.2014.02.004
– ident: 17
  doi: 10.1006/jcat.1995.1247
– volume: 12
  start-page: 744
  year: 1982
  ident: 24
  publication-title: Chem. Tech.
  contributor:
    fullname: Dry M E
– ident: 6
  doi: 10.1021/cs4006088
– ident: 18
  doi: 10.1016/0021-9517(81)90025-7
– start-page: F321
  year: 1992
  ident: 25
  publication-title: Recent developments in the physics of fluids
  contributor:
    fullname: Arai M
– ident: 22
  doi: 10.1016/0021-9517(85)90379-3
– ident: 27
  doi: 10.1016/0021-9517(86)90043-6
– ident: 4
  doi: 10.1366/11-06456
– ident: 13
  doi: 10.1002/1521-3773(20020104)41:1<144::AID-ANIE144>3.0.CO;2-J
– ident: 9
  doi: 10.1039/c2cp42745a
– ident: 11
  doi: 10.1016/j.chemphys.2013.10.012
– volume: 82
  year: 2011
  ident: 12
  publication-title: Rev. Sci. Instrum.
  doi: 10.1063/1.3553295
  contributor:
    fullname: Silverwood I P
– ident: 5
  doi: 10.1016/S0920-5861(01)00334-0
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Snippet Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst...
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SubjectTerms Acquisitions
Carbon monoxide
Catalysts
Fischer-Tropsch process
Handling
Hydrogenation
Inelastic scattering
Marketing
Neutron scattering
Neutrons
Physics
Spectra
Title Sample environment issues relevant to the acquisition of inelastic neutron scattering measurements of heterogeneous catalyst samples
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