Sample environment issues relevant to the acquisition of inelastic neutron scattering measurements of heterogeneous catalyst samples
Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laborat...
Saved in:
Published in | Journal of physics. Conference series Vol. 554; no. 1; pp. 12005 - 12 |
---|---|
Main Authors | , , , , , , , , , , , , |
Format | Journal Article |
Language | English |
Published |
Bristol
IOP Publishing
01.01.2014
|
Subjects | |
Online Access | Get full text |
Cover
Loading…
Abstract | Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laboratory space and ventilation facilities that are suited to the increasingly wide range of catalytic samples being examined. INS measurements for CO hydrogenation over an iron-based Fischer-Tropsch catalyst recorded using the MARI spectrometer are presented to illustrate the applicability of the new arrangements. |
---|---|
AbstractList | Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laboratory space and ventilation facilities that are suited to the increasingly wide range of catalytic samples being examined. INS measurements for CO hydrogenation over an iron-based Fischer-Tropsch catalyst recorded using the MARI spectrometer are presented to illustrate the applicability of the new arrangements. |
Author | Webb, P B Lennon, D Kibble, M Taylor, J Ewings, R A Goodway, C M Parker, S F Wakefield, S R Jura, M Bellaire, D Warringham, R Dudman, M P Tooze, R P |
Author_xml | – sequence: 1 givenname: R surname: Warringham fullname: Warringham, R – sequence: 2 givenname: D surname: Bellaire fullname: Bellaire, D – sequence: 3 givenname: S surname: Parker middlename: F fullname: Parker, S F – sequence: 4 givenname: J surname: Taylor fullname: Taylor, J – sequence: 5 givenname: R surname: Ewings middlename: A fullname: Ewings, R A – sequence: 6 givenname: C surname: Goodway middlename: M fullname: Goodway, C M – sequence: 7 givenname: M surname: Kibble fullname: Kibble, M – sequence: 8 givenname: S surname: Wakefield middlename: R fullname: Wakefield, S R – sequence: 9 givenname: M surname: Jura fullname: Jura, M – sequence: 10 givenname: M surname: Dudman middlename: P fullname: Dudman, M P – sequence: 11 givenname: R surname: Tooze middlename: P fullname: Tooze, R P – sequence: 12 givenname: P surname: Webb middlename: B fullname: Webb, P B – sequence: 13 givenname: D surname: Lennon fullname: Lennon, D |
BookMark | eNpdkUtLxDAQx4Mo-PwKEvDiZd2keTQ9iviCBQ_qOWTbqUbaZM2kgnc_uKkrHpzLTJjfPDL_Q7IbYgBCTjm74MyYJa9ltdCq0Uul5JIvGa8YUzvk4C-x-xcbs08OEd8YE8XqA_L16MbNABTCh08xjBAy9YgTIE0wwIcr7xxpfgXq2vfJo88-Bhp76gMMDrNvaYApl1qKrcsZkg8vdASHU4K5Hc7wK5REfIEAcUJaODd8Yqb4MxyPyV7vBoSTX39Enm-un67uFquH2_ury9WilYznRWWkEpqpDnjDe6krJ6tGifXamN4wzeR63dXQdqyTmhdrhNCyqXrgXc9EL8QROd_23aT4Xr6Y7eixhWFwP3tZXnPTKNVwXdCzf-hbnFIo29lK1brWouGmUHpLtSkiJujtJvnRpU_LmZ3FsfPd7ayBLeJYbrfiiG9nBYak |
CitedBy_id | crossref_primary_10_1007_s11244_020_01258_3 crossref_primary_10_1007_s11244_020_01259_2 crossref_primary_10_1016_j_apcata_2018_10_010 crossref_primary_10_3390_catal10111255 crossref_primary_10_1021_acs_chemrev_3c00101 crossref_primary_10_1021_acs_iecr_9b04636 crossref_primary_10_1021_acs_jpcc_8b08420 crossref_primary_10_1016_j_ces_2018_04_051 crossref_primary_10_1016_j_cattod_2020_05_030 crossref_primary_10_1063_1_4935054 crossref_primary_10_1002_cctc_202100286 crossref_primary_10_1021_acsomega_9b03503 crossref_primary_10_1021_acsphyschemau_2c00040 crossref_primary_10_1007_s10562_016_1742_5 crossref_primary_10_1063_5_0123434 crossref_primary_10_1016_j_apcata_2023_119442 crossref_primary_10_1016_j_jcat_2020_09_025 crossref_primary_10_1021_acs_jpcc_9b01890 crossref_primary_10_1098_rspa_2016_0126 crossref_primary_10_3390_catal10040433 |
Cites_doi | 10.1016/S0360-0564(06)51003-X 10.1039/b505974g 10.1142/5628 10.1016/j.jcat.2010.09.001 10.1016/j.cattod.2006.02.041 10.1021/j100462a011 10.1016/j.cattod.2010.07.009 10.1021/ja0381398 10.1016/0021-9517(89)90342-4 10.1002/anie.201210179 10.1021/jp0405963 10.1016/j.jcat.2006.07.012 10.1039/c3ra42435a 10.1016/j.jcat.2014.02.004 10.1006/jcat.1995.1247 10.1021/cs4006088 10.1016/0021-9517(81)90025-7 10.1016/0021-9517(85)90379-3 10.1016/0021-9517(86)90043-6 10.1366/11-06456 10.1002/1521-3773(20020104)41:1<144::AID-ANIE144>3.0.CO;2-J 10.1039/c2cp42745a 10.1016/j.chemphys.2013.10.012 10.1063/1.3553295 10.1016/S0920-5861(01)00334-0 |
ContentType | Journal Article |
Copyright | 2014. This work is published under http://creativecommons.org/licenses/by/3.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License. |
Copyright_xml | – notice: 2014. This work is published under http://creativecommons.org/licenses/by/3.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License. |
DBID | AAYXX CITATION 8FD 8FE 8FG ABUWG AFKRA ARAPS AZQEC BENPR BGLVJ CCPQU DWQXO H8D HCIFZ L7M P5Z P62 PIMPY PQEST PQQKQ PQUKI PRINS 7U5 8BQ JG9 |
DOI | 10.1088/1742-6596/554/1/012005 |
DatabaseName | CrossRef Technology Research Database ProQuest SciTech Collection ProQuest Technology Collection ProQuest Central (Alumni Edition) ProQuest Central Advanced Technologies & Aerospace Database (1962 - current) ProQuest Central Essentials ProQuest Central Technology Collection ProQuest One Community College ProQuest Central Aerospace Database SciTech Premium Collection (Proquest) (PQ_SDU_P3) Advanced Technologies Database with Aerospace Advanced Technologies & Aerospace Database ProQuest Advanced Technologies & Aerospace Collection ProQuest - Publicly Available Content Database ProQuest One Academic Eastern Edition (DO NOT USE) ProQuest One Academic ProQuest One Academic UKI Edition ProQuest Central China Solid State and Superconductivity Abstracts METADEX Materials Research Database |
DatabaseTitle | CrossRef Publicly Available Content Database Advanced Technologies & Aerospace Collection Technology Collection Technology Research Database ProQuest Advanced Technologies & Aerospace Collection ProQuest Central Essentials ProQuest One Academic Eastern Edition ProQuest Central (Alumni Edition) SciTech Premium Collection ProQuest One Community College ProQuest Technology Collection ProQuest SciTech Collection ProQuest Central China ProQuest Central Advanced Technologies & Aerospace Database Aerospace Database ProQuest One Academic UKI Edition ProQuest Central Korea ProQuest One Academic Advanced Technologies Database with Aerospace Materials Research Database Solid State and Superconductivity Abstracts METADEX |
DatabaseTitleList | Publicly Available Content Database Materials Research Database |
Database_xml | – sequence: 1 dbid: 8FG name: ProQuest Technology Collection url: https://search.proquest.com/technologycollection1 sourceTypes: Aggregation Database |
DeliveryMethod | fulltext_linktorsrc |
Discipline | Physics |
EISSN | 1742-6596 |
EndPage | 12 |
ExternalDocumentID | 10_1088_1742_6596_554_1_012005 |
GroupedDBID | 1JI 29L 2WC 4.4 5B3 5GY 5PX 5VS 7.Q AAJIO AAJKP AALHV AAYXX ABHWH ACAFW ACHIP AEFHF AEJGL AERVB AFKRA AFYNE AIYBF AKPSB ALMA_UNASSIGNED_HOLDINGS ARAPS ASPBG ATQHT AVWKF AZFZN BENPR BGLVJ CCPQU CEBXE CITATION CJUJL CRLBU CS3 DU5 E3Z EBS EDWGO EJD EQZZN F5P FRP GROUPED_DOAJ GX1 HCIFZ HH5 IJHAN IOP IZVLO J9A JCGBZ KNG KQ8 LAP N5L N9A O3W OK1 P2P PIMPY PJBAE RIN RNS RO9 ROL SY9 T37 TR2 UCJ W28 XSB ~02 8FD 8FE 8FG ABUWG AZQEC DWQXO H8D L7M P62 PQEST PQQKQ PQUKI PRINS 7U5 8BQ JG9 |
ID | FETCH-LOGICAL-c401t-28453605de191f462a42953bb88f80604bbd7ecd0d4611119336492fe1df03f33 |
IEDL.DBID | 8FG |
ISSN | 1742-6588 |
IngestDate | Fri Apr 12 02:44:18 EDT 2024 Fri Sep 13 06:17:24 EDT 2024 Thu Sep 26 18:38:02 EDT 2024 |
IsDoiOpenAccess | true |
IsOpenAccess | true |
IsPeerReviewed | true |
IsScholarly | true |
Issue | 1 |
Language | English |
LinkModel | DirectLink |
MergedId | FETCHMERGED-LOGICAL-c401t-28453605de191f462a42953bb88f80604bbd7ecd0d4611119336492fe1df03f33 |
Notes | ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 |
OpenAccessLink | https://www.proquest.com/docview/2576763918/abstract/?pq-origsite=%requestingapplication% |
PQID | 2576763918 |
PQPubID | 4998668 |
PageCount | 12 |
ParticipantIDs | proquest_miscellaneous_1718955916 proquest_journals_2576763918 crossref_primary_10_1088_1742_6596_554_1_012005 |
PublicationCentury | 2000 |
PublicationDate | 2014-01-01 |
PublicationDateYYYYMMDD | 2014-01-01 |
PublicationDate_xml | – month: 01 year: 2014 text: 2014-01-01 day: 01 |
PublicationDecade | 2010 |
PublicationPlace | Bristol |
PublicationPlace_xml | – name: Bristol |
PublicationTitle | Journal of physics. Conference series |
PublicationYear | 2014 |
Publisher | IOP Publishing |
Publisher_xml | – name: IOP Publishing |
References | 22 23 26 27 Silverwood I P (12) 2011; 82 Arai M (25) 1992 10 11 Mitchell P C H (15) 2005 13 14 16 17 Dry M E (24) 1982; 12 18 19 1 2 3 4 5 6 7 8 9 20 21 |
References_xml | – ident: 1 doi: 10.1016/S0360-0564(06)51003-X – ident: 2 doi: 10.1039/b505974g – year: 2005 ident: 15 publication-title: Vibrational spectroscopy using neutrons. doi: 10.1142/5628 contributor: fullname: Mitchell P C H – ident: 21 doi: 10.1016/j.jcat.2010.09.001 – ident: 7 doi: 10.1016/j.cattod.2006.02.041 – ident: 19 doi: 10.1021/j100462a011 – ident: 8 doi: 10.1016/j.cattod.2010.07.009 – ident: 14 doi: 10.1021/ja0381398 – ident: 23 doi: 10.1016/0021-9517(89)90342-4 – ident: 20 doi: 10.1002/anie.201210179 – ident: 3 doi: 10.1021/jp0405963 – ident: 26 doi: 10.1016/j.jcat.2006.07.012 – ident: 10 doi: 10.1039/c3ra42435a – ident: 16 doi: 10.1016/j.jcat.2014.02.004 – ident: 17 doi: 10.1006/jcat.1995.1247 – volume: 12 start-page: 744 year: 1982 ident: 24 publication-title: Chem. Tech. contributor: fullname: Dry M E – ident: 6 doi: 10.1021/cs4006088 – ident: 18 doi: 10.1016/0021-9517(81)90025-7 – start-page: F321 year: 1992 ident: 25 publication-title: Recent developments in the physics of fluids contributor: fullname: Arai M – ident: 22 doi: 10.1016/0021-9517(85)90379-3 – ident: 27 doi: 10.1016/0021-9517(86)90043-6 – ident: 4 doi: 10.1366/11-06456 – ident: 13 doi: 10.1002/1521-3773(20020104)41:1<144::AID-ANIE144>3.0.CO;2-J – ident: 9 doi: 10.1039/c2cp42745a – ident: 11 doi: 10.1016/j.chemphys.2013.10.012 – volume: 82 year: 2011 ident: 12 publication-title: Rev. Sci. Instrum. doi: 10.1063/1.3553295 contributor: fullname: Silverwood I P – ident: 5 doi: 10.1016/S0920-5861(01)00334-0 |
SSID | ssj0033337 |
Score | 2.232253 |
Snippet | Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst... |
SourceID | proquest crossref |
SourceType | Aggregation Database |
StartPage | 12005 |
SubjectTerms | Acquisitions Carbon monoxide Catalysts Fischer-Tropsch process Handling Hydrogenation Inelastic scattering Marketing Neutron scattering Neutrons Physics Spectra |
Title | Sample environment issues relevant to the acquisition of inelastic neutron scattering measurements of heterogeneous catalyst samples |
URI | https://www.proquest.com/docview/2576763918/abstract/ https://search.proquest.com/docview/1718955916 |
Volume | 554 |
hasFullText | 1 |
inHoldings | 1 |
isFullTextHit | |
isPrint | |
link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV1Lb9QwEB6VVkhcEOUhFtrKSFytrOMka58QoC6rSlQIqNSb5afgwKatswfu_HBmnISWS3NMIkcZ2zPfjOebAXgrbRKt1zX3wVretMlyZeuOBwQHy9pqoT0RhT-fd5uL5uyyvdyDzcyFobTKWScWRR16TzHyioAx7gUtVGUdRQH8UL27uubUP4rOWadmGg_gQFBNPOKMrz_NOlnitRqpkTVHm6tmrjC6f9M93VVoWStREZuUmtndNVP_a-lietZP4PGEGdn7cZIPYS9un8LDkrvp8zP4881SiV92h7PGijgzo44oCJUHNvQMkR6z_nr3c8zSYn1iiDARPOOobBt3FBNn2Zd6m2jP2K_b6GGml39Q4kyP6y32u8xK2Od3HlguH8_P4WJ9-v3jhk_NFbhHl2rgaJZaib5MiOixpaarLVqmVjqnVFJUUce5sIo-LEPTkVrVUnaNrlMUIS1lkvIF7G_7bXwJjEq6JG3lCl2_xrqVU9YFrxv07BDeRbGAapaluRpraJhy9q2UIekbkr5B6RthRukv4GgWuZn2VDa3K2ABb_49xt1ARxy2_DwOJxTV1BPdq_uHeA2PEPo0YzDlCPaHm108RngxuJOyck7g4MPp-ZevfwGhm9BU |
link.rule.ids | 315,786,790,12792,21416,27957,27958,33408,33779,33780,43635,43840 |
linkProvider | ProQuest |
linkToHtml | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwfV1LT9wwELbaRVW5VIVSsUCpkXq1so6drH1CVdXt0i5cChI3y_FD9NAN4Oyhd344M05S6KU5JpGjjO35vhnPg5BPwkZeOV0y561lsoqWKVvWzAM5mJVWc-0wUfj8ol5eye_X1fXgcEtDWOWoE7Oi9q1DH3mBxBj2gubq9PaOYdcoPF0dWmi8JFtSAHRipvji26iJBVzzPiGyZIC0aswQBqNvuKfrAvC04AXmkGILu-fg9K9uzoCzeEveDEyRfu6ndoe8COtd8ipHbLr0jjz8tFjYlz7LVKNZiIliHxQgyB3tWgr8jlp3t_nVx2bRNlLglUCZYVS6Dhv0hNPkcpVNQDH6-8lnmPDlGwyXaWGVhXaTaHb2_EkdTfnjaY9cLb5eflmyoaUCc2BIdQzAqBJgwfgAdlqUdWkBjyrRNEpFhXV0msbPg_MzL2tUplqIWuoyBu7jTEQh3pPJul2HfUKxkEvUVszB4JO2mTfKNt5pCfYckLrAp6QYZWlu-8oZJp94K2VQ-galb0D6hpte-lNyNIrcDDspmad5n5KTv49hD-DBhs0_D8NxhZX0eH3w_yE-ktfLy_OVWZ1d_Dgk20B-ZO9OOSKT7n4TPgDB6JrjvIoeAdTbzeg |
openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=Sample+environment+issues+relevant+to+the+acquisition+of+inelastic+neutron+scattering+measurements+of+heterogeneous+catalyst+samples&rft.jtitle=Journal+of+physics.+Conference+series&rft.au=Warringham%2C+R&rft.au=Bellaire%2C+D&rft.au=Parker%2C+S+F&rft.au=Taylor%2C+J&rft.date=2014-01-01&rft.issn=1742-6588&rft.eissn=1742-6596&rft.volume=554&rft.spage=1&rft.epage=12&rft_id=info:doi/10.1088%2F1742-6596%2F554%2F1%2F012005&rft.externalDBID=NO_FULL_TEXT |
thumbnail_l | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=1742-6588&client=summon |
thumbnail_m | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=1742-6588&client=summon |
thumbnail_s | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=1742-6588&client=summon |