Sample environment issues relevant to the acquisition of inelastic neutron scattering measurements of heterogeneous catalyst samples

Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laborat...

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Published inJournal of physics. Conference series Vol. 554; no. 1; pp. 12005 - 12
Main Authors Warringham, R, Bellaire, D, Parker, S F, Taylor, J, Ewings, R A, Goodway, C M, Kibble, M, Wakefield, S R, Jura, M, Dudman, M P, Tooze, R P, Webb, P B, Lennon, D
Format Journal Article
LanguageEnglish
Published Bristol IOP Publishing 01.01.2014
Subjects
Acquisitions
Carbon monoxide
Catalysts
Fischer-Tropsch process
Handling
Hydrogenation
Inelastic scattering
Marketing
Neutron scattering
Neutrons
Physics
Spectra
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Summary:Refinements to established sample handling issues connected with the acquisition of inelastic neutron scattering (INS) spectra of heterogeneous catalyst samples are described. This involves modification of a reactor and improvements to gas handling apparatus. The latter includes provision of laboratory space and ventilation facilities that are suited to the increasingly wide range of catalytic samples being examined. INS measurements for CO hydrogenation over an iron-based Fischer-Tropsch catalyst recorded using the MARI spectrometer are presented to illustrate the applicability of the new arrangements.
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ISSN:1742-6588
1742-6596
DOI:10.1088/1742-6596/554/1/012005