Tailoring a facile electronic and ionic pathway to boost the storage performance of Fe3O4 nanowires as negative electrode for supercapacitor application

Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe 3 O 4 -based active materials display a promising theoretical storage performance as a negati...

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Published inScientific reports Vol. 14; no. 1; pp. 16807 - 14
Main Authors Abdelrahim, Ahmed M., El-Moghny, Muhammad G. Abd, Abdelhady, Hosam H., Wali, Hager S., Gamil, Mariam M., Fahmy, Samanta R., Abdel-Hamid, Toka M., Mohammed, Gehad K., Ahmed, Yasmeen A., El-Deab, Mohamed S.
Format Journal Article
LanguageEnglish
Published London Nature Publishing Group UK 22.07.2024
Nature Publishing Group
Nature Portfolio
Subjects
639/638/161
639/638/675
Conductivity
Electrodes
Energy loss
Fe3O4
Graphite felt
Humanities and Social Sciences
Iron oxides
multidisciplinary
Nanotechnology
Nanowires
Negative electrode
Science
Science (multidisciplinary)
Specific capacity
Supercapacitor
Surface fluctuations
Graphite felt
Supercapacitor
Negative electrode
Surface fluctuations
Fe
O
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Abstract Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe 3 O 4 -based active materials display a promising theoretical storage performance as a negative electrode. Thus, to get a high storage performance of Fe 3 O 4 , it must be tailored to have a higher ionic and electronic conductivity and outstanding stability. Functionalized graphite felt (GF) is an excellent candidate for tailoring Fe 3 O 4 with a facile ionic and electronic pathway. However, the steps of the functionalization of GF are complex and time-consuming as well as the energy loss during this step. Thus, the in-situ functionalization of the GF surface throughout the synthesis of Fe 3 O 4 active materials is proposed herein. Fe 3 O 4 is electrodeposited at the in-situ functionalized GF surface with the crystalline nanowires-like structure as revealed from the various analyses; SEM, TEM, Mapping EDX, XPS, XRD, wettability test, and Raman analysis. Advantageously, the synthetic approach introduces full homogeneous and uniform coverage of the large surface area of the GF. Thus, Fe 3 O 4 nanowires with high ionic and electronic conductivity are characterized by a higher storage performance. Interestingly, Fe 3 O 4 /GF possesses a high specific capacity of 1418 mC cm −2 at a potential scan rate of 10 mV s −1 and this value retained to 54% at a potential scan rate of 50 mV s −1 at an extended potential window of 1.45 V. Remarkably, the diffusion-controlled reaction is the main contributor of the storage of Fe 3 O 4 /GF electrode as revealed by the mechanistic studies.
AbstractList Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe3O4-based active materials display a promising theoretical storage performance as a negative electrode. Thus, to get a high storage performance of Fe3O4, it must be tailored to have a higher ionic and electronic conductivity and outstanding stability. Functionalized graphite felt (GF) is an excellent candidate for tailoring Fe3O4 with a facile ionic and electronic pathway. However, the steps of the functionalization of GF are complex and time-consuming as well as the energy loss during this step. Thus, the in-situ functionalization of the GF surface throughout the synthesis of Fe3O4 active materials is proposed herein. Fe3O4 is electrodeposited at the in-situ functionalized GF surface with the crystalline nanowires-like structure as revealed from the various analyses; SEM, TEM, Mapping EDX, XPS, XRD, wettability test, and Raman analysis. Advantageously, the synthetic approach introduces full homogeneous and uniform coverage of the large surface area of the GF. Thus, Fe3O4 nanowires with high ionic and electronic conductivity are characterized by a higher storage performance. Interestingly, Fe3O4/GF possesses a high specific capacity of 1418 mC cm-2 at a potential scan rate of 10 mV s-1 and this value retained to 54% at a potential scan rate of 50 mV s-1 at an extended potential window of 1.45 V. Remarkably, the diffusion-controlled reaction is the main contributor of the storage of Fe3O4/GF electrode as revealed by the mechanistic studies.Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe3O4-based active materials display a promising theoretical storage performance as a negative electrode. Thus, to get a high storage performance of Fe3O4, it must be tailored to have a higher ionic and electronic conductivity and outstanding stability. Functionalized graphite felt (GF) is an excellent candidate for tailoring Fe3O4 with a facile ionic and electronic pathway. However, the steps of the functionalization of GF are complex and time-consuming as well as the energy loss during this step. Thus, the in-situ functionalization of the GF surface throughout the synthesis of Fe3O4 active materials is proposed herein. Fe3O4 is electrodeposited at the in-situ functionalized GF surface with the crystalline nanowires-like structure as revealed from the various analyses; SEM, TEM, Mapping EDX, XPS, XRD, wettability test, and Raman analysis. Advantageously, the synthetic approach introduces full homogeneous and uniform coverage of the large surface area of the GF. Thus, Fe3O4 nanowires with high ionic and electronic conductivity are characterized by a higher storage performance. Interestingly, Fe3O4/GF possesses a high specific capacity of 1418 mC cm-2 at a potential scan rate of 10 mV s-1 and this value retained to 54% at a potential scan rate of 50 mV s-1 at an extended potential window of 1.45 V. Remarkably, the diffusion-controlled reaction is the main contributor of the storage of Fe3O4/GF electrode as revealed by the mechanistic studies.
Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe 3 O 4 -based active materials display a promising theoretical storage performance as a negative electrode. Thus, to get a high storage performance of Fe 3 O 4 , it must be tailored to have a higher ionic and electronic conductivity and outstanding stability. Functionalized graphite felt (GF) is an excellent candidate for tailoring Fe 3 O 4 with a facile ionic and electronic pathway. However, the steps of the functionalization of GF are complex and time-consuming as well as the energy loss during this step. Thus, the in-situ functionalization of the GF surface throughout the synthesis of Fe 3 O 4 active materials is proposed herein. Fe 3 O 4 is electrodeposited at the in-situ functionalized GF surface with the crystalline nanowires-like structure as revealed from the various analyses; SEM, TEM, Mapping EDX, XPS, XRD, wettability test, and Raman analysis. Advantageously, the synthetic approach introduces full homogeneous and uniform coverage of the large surface area of the GF. Thus, Fe 3 O 4 nanowires with high ionic and electronic conductivity are characterized by a higher storage performance. Interestingly, Fe 3 O 4 /GF possesses a high specific capacity of 1418 mC cm −2 at a potential scan rate of 10 mV s −1 and this value retained to 54% at a potential scan rate of 50 mV s −1 at an extended potential window of 1.45 V. Remarkably, the diffusion-controlled reaction is the main contributor of the storage of Fe 3 O 4 /GF electrode as revealed by the mechanistic studies.
Abstract Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe3O4-based active materials display a promising theoretical storage performance as a negative electrode. Thus, to get a high storage performance of Fe3O4, it must be tailored to have a higher ionic and electronic conductivity and outstanding stability. Functionalized graphite felt (GF) is an excellent candidate for tailoring Fe3O4 with a facile ionic and electronic pathway. However, the steps of the functionalization of GF are complex and time-consuming as well as the energy loss during this step. Thus, the in-situ functionalization of the GF surface throughout the synthesis of Fe3O4 active materials is proposed herein. Fe3O4 is electrodeposited at the in-situ functionalized GF surface with the crystalline nanowires-like structure as revealed from the various analyses; SEM, TEM, Mapping EDX, XPS, XRD, wettability test, and Raman analysis. Advantageously, the synthetic approach introduces full homogeneous and uniform coverage of the large surface area of the GF. Thus, Fe3O4 nanowires with high ionic and electronic conductivity are characterized by a higher storage performance. Interestingly, Fe3O4/GF possesses a high specific capacity of 1418 mC cm−2 at a potential scan rate of 10 mV s−1 and this value retained to 54% at a potential scan rate of 50 mV s−1 at an extended potential window of 1.45 V. Remarkably, the diffusion-controlled reaction is the main contributor of the storage of Fe3O4/GF electrode as revealed by the mechanistic studies.
Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe3O4-based active materials display a promising theoretical storage performance as a negative electrode. Thus, to get a high storage performance of Fe3O4, it must be tailored to have a higher ionic and electronic conductivity and outstanding stability. Functionalized graphite felt (GF) is an excellent candidate for tailoring Fe3O4 with a facile ionic and electronic pathway. However, the steps of the functionalization of GF are complex and time-consuming as well as the energy loss during this step. Thus, the in-situ functionalization of the GF surface throughout the synthesis of Fe3O4 active materials is proposed herein. Fe3O4 is electrodeposited at the in-situ functionalized GF surface with the crystalline nanowires-like structure as revealed from the various analyses; SEM, TEM, Mapping EDX, XPS, XRD, wettability test, and Raman analysis. Advantageously, the synthetic approach introduces full homogeneous and uniform coverage of the large surface area of the GF. Thus, Fe3O4 nanowires with high ionic and electronic conductivity are characterized by a higher storage performance. Interestingly, Fe3O4/GF possesses a high specific capacity of 1418 mC cm−2 at a potential scan rate of 10 mV s−1 and this value retained to 54% at a potential scan rate of 50 mV s−1 at an extended potential window of 1.45 V. Remarkably, the diffusion-controlled reaction is the main contributor of the storage of Fe3O4/GF electrode as revealed by the mechanistic studies.
Abstract Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of the negative electrodes is a crucial topic. Fe 3 O 4 -based active materials display a promising theoretical storage performance as a negative electrode. Thus, to get a high storage performance of Fe 3 O 4 , it must be tailored to have a higher ionic and electronic conductivity and outstanding stability. Functionalized graphite felt (GF) is an excellent candidate for tailoring Fe 3 O 4 with a facile ionic and electronic pathway. However, the steps of the functionalization of GF are complex and time-consuming as well as the energy loss during this step. Thus, the in-situ functionalization of the GF surface throughout the synthesis of Fe 3 O 4 active materials is proposed herein. Fe 3 O 4 is electrodeposited at the in-situ functionalized GF surface with the crystalline nanowires-like structure as revealed from the various analyses; SEM, TEM, Mapping EDX, XPS, XRD, wettability test, and Raman analysis. Advantageously, the synthetic approach introduces full homogeneous and uniform coverage of the large surface area of the GF. Thus, Fe 3 O 4 nanowires with high ionic and electronic conductivity are characterized by a higher storage performance. Interestingly, Fe 3 O 4 /GF possesses a high specific capacity of 1418 mC cm −2 at a potential scan rate of 10 mV s −1 and this value retained to 54% at a potential scan rate of 50 mV s −1 at an extended potential window of 1.45 V. Remarkably, the diffusion-controlled reaction is the main contributor of the storage of Fe 3 O 4 /GF electrode as revealed by the mechanistic studies.
ArticleNumber 16807
Author Abdelhady, Hosam H.
Mohammed, Gehad K.
Wali, Hager S.
Abdel-Hamid, Toka M.
Abdelrahim, Ahmed M.
Fahmy, Samanta R.
Gamil, Mariam M.
El-Moghny, Muhammad G. Abd
Ahmed, Yasmeen A.
El-Deab, Mohamed S.
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  givenname: Muhammad G. Abd
  surname: El-Moghny
  fullname: El-Moghny, Muhammad G. Abd
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  organization: Department of Chemistry, Faculty of Science, Cairo University
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  givenname: Hosam H.
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  givenname: Yasmeen A.
  surname: Ahmed
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Issue 1
Keywords Graphite felt
Supercapacitor
Negative electrode
Surface fluctuations
Fe
O
Language English
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SSID ssj0000529419
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Snippet Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage performance of...
Abstract Today, high-energy applications are devoted to boosting the storage performance of asymmetric supercapacitors. Importantly, boosting the storage...
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SubjectTerms 639/638/161
639/638/675
Conductivity
Electrodes
Energy loss
Fe3O4
Graphite felt
Humanities and Social Sciences
Iron oxides
multidisciplinary
Nanotechnology
Nanowires
Negative electrode
Science
Science (multidisciplinary)
Specific capacity
Supercapacitor
Surface fluctuations
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Title Tailoring a facile electronic and ionic pathway to boost the storage performance of Fe3O4 nanowires as negative electrode for supercapacitor application
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https://pubmed.ncbi.nlm.nih.gov/PMC11263369
https://doaj.org/article/7e0c5c304e704821a3e4edd67e3938fc
Volume 14
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