High-resolution neutron powder diffractometer SPODI at research reactor FRM II

• Published in: Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment Vol. 667; pp. 32 - 37
• Main Authors: Hoelzel, M., Senyshyn, A., Juenke, N., Boysen, H., Schmahl, W., Fuess, H.
• Format: Journal Article
• Language: English
• Published: Elsevier B.V 01.03.2012
• Subjects: Arrays; Detectors; Devices; Diffractometers; Electric fields; Monochromators; Multidetector; Neutron diffraction; Neutron instrumentation; Nuclear research reactors; Powder diffraction; Powder diffractometer; Neutron instrumentation; Powder diffraction; Neutron diffraction; Multidetector; Powder diffractometer
• ISSN: 0168-9002; 1872-9576
• DOI: 10.1016/j.nima.2011.11.070

SPODI is a high-resolution thermal neutron diffractometer at the research reactor Heinz Maier-Leibnitz (FRM II) especially dedicated to structural studies of complex systems. Unique features like a very large monochromator take-off angle of 155° and a 5 m monochromator–sample distance in its standard configuration achieve both high-resolution and a good profile shape for a broad scattering angle range. Two dimensional data are collected by an array of 80 vertical position sensitive 3He detectors. SPODI is well suited for studies of complex structural and magnetic order and disorder phenomena at non-ambient conditions. In addition to standard sample environment facilities (cryostats, furnaces, magnet) specific devices (rotatable load frame, cell for electric fields, multichannel potentiostat) were developed. Thus the characterisation of functional materials at in-operando conditions can be achieved. In this contribution the details of the design and present performance of the instrument are reported along with its specifications. A new concept for data reduction using a 2 θ dependent variable height for the intensity integration along the Debye–Scherrer lines is introduced.