Comparison of specific interactions in P4VP/PSCA and PS4VP/PSCA blends and complexes
The compatibilization of an immiscible polymer system polystyrene/poly(4-vinylpyridine) has been induced by the introduction of carboxylic acid groups within the polystyrene chains. Poly(styrene-co-cinnamic acid), PSCA, copolymers were used to prepare blends and complexes with poly(4-vinylpyridine),...
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Published in | Journal of applied polymer science Vol. 108; no. 5; pp. 3256 - 3261 |
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Abstract | The compatibilization of an immiscible polymer system polystyrene/poly(4-vinylpyridine) has been induced by the introduction of carboxylic acid groups within the polystyrene chains. Poly(styrene-co-cinnamic acid), PSCA, copolymers were used to prepare blends and complexes with poly(4-vinylpyridine), P4VP, and in a second time with poly(styrene-co-4-vinylpyridine), PS4VP, copolymer in order to reduce the density of the interacting groups. The miscibility of the systems has been ascertained by DSC, which revealed that both blends and complexes exhibit a single glass transition temperature indicating their single phase nature. The Tgs of the complexes of PS4VP with PSCA15, containing 15 mol % of cinnamic acid content, were higher than those of the corresponding blends indicating that stronger interpolymer interactions were developed in the complexes. Furthermore, the application of the Kwei equation suggested that P4VP interacts more strongly with PSCA15 than does PS4VP. FTIR spectra revealed the development of hydrogen bonding within the PS4VP/PSCA system and both hydrogen bonding and ionic interaction in the P4VP/PSCA blends whereas the same interactions were expected in both systems. This observation confirmed the stronger ability of P4VP to interact with PSCA copolymer. The viscosimetric study showed both positive and negative deviations of the reduced viscosity of the blends from the additivity law confirming the presence of specific interactions within the blend solutions. |
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AbstractList | The compatibilization of an immiscible polymer system polystyrene/poly(4‐vinylpyridine) has been induced by the introduction of carboxylic acid groups within the polystyrene chains. Poly(styrene‐co‐cinnamic acid), PSCA, copolymers were used to prepare blends and complexes with poly(4‐vinylpyridine), P4VP, and in a second time with poly(styrene‐co‐4‐vinylpyridine), PS4VP, copolymer in order to reduce the density of the interacting groups. The miscibility of the systems has been ascertained by DSC, which revealed that both blends and complexes exhibit a single glass transition temperature indicating their single phase nature. The Tgs of the complexes of PS4VP with PSCA15, containing 15 mol % of cinnamic acid content, were higher than those of the corresponding blends indicating that stronger interpolymer interactions were developed in the complexes. Furthermore, the application of the Kwei equation suggested that P4VP interacts more strongly with PSCA15 than does PS4VP. FTIR spectra revealed the development of hydrogen bonding within the PS4VP/PSCA system and both hydrogen bonding and ionic interaction in the P4VP/PSCA blends whereas the same interactions were expected in both systems. This observation confirmed the stronger ability of P4VP to interact with PSCA copolymer. The viscosimetric study showed both positive and negative deviations of the reduced viscosity of the blends from the additivity law confirming the presence of specific interactions within the blend solutions. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 The compatibilization of an immiscible polymer system polystyrene/poly(4-vinylpyridine) has been induced by the introduction of carboxylic acid groups within the polystyrene chains. Poly(styrene-co-cinnamic acid), PSCA, copolymers were used to prepare blends and complexes with poly(4-vinylpyridine), P4VP, and in a second time with poly(styrene-co-4-vinylpyridine), PS4VP, copolymer in order to reduce the density of the interacting groups. The miscibility of the systems has been ascertained by DSC, which revealed that both blends and complexes exhibit a single glass transition temperature indicating their single phase nature. The Tgs of the complexes of PS4VP with PSCA15, containing 15 mol % of cinnamic acid content, were higher than those of the corresponding blends indicating that stronger interpolymer interactions were developed in the complexes. Furthermore, the application of the Kwei equation suggested that P4VP interacts more strongly with PSCA15 than does PS4VP. FTIR spectra revealed the development of hydrogen bonding within the PS4VP/PSCA system and both hydrogen bonding and ionic interaction in the P4VP/PSCA blends whereas the same interactions were expected in both systems. This observation confirmed the stronger ability of P4VP to interact with PSCA copolymer. The viscosimetric study showed both positive and negative deviations of the reduced viscosity of the blends from the additivity law confirming the presence of specific interactions within the blend solutions. Abstract The compatibilization of an immiscible polymer system polystyrene/poly(4‐vinylpyridine) has been induced by the introduction of carboxylic acid groups within the polystyrene chains. Poly(styrene‐ co ‐cinnamic acid), PSCA, copolymers were used to prepare blends and complexes with poly(4‐vinylpyridine), P4VP, and in a second time with poly(styrene‐ co ‐4‐vinylpyridine), PS4VP, copolymer in order to reduce the density of the interacting groups. The miscibility of the systems has been ascertained by DSC, which revealed that both blends and complexes exhibit a single glass transition temperature indicating their single phase nature. The T g s of the complexes of PS4VP with PSCA15, containing 15 mol % of cinnamic acid content, were higher than those of the corresponding blends indicating that stronger interpolymer interactions were developed in the complexes. Furthermore, the application of the Kwei equation suggested that P4VP interacts more strongly with PSCA15 than does PS4VP. FTIR spectra revealed the development of hydrogen bonding within the PS4VP/PSCA system and both hydrogen bonding and ionic interaction in the P4VP/PSCA blends whereas the same interactions were expected in both systems. This observation confirmed the stronger ability of P4VP to interact with PSCA copolymer. The viscosimetric study showed both positive and negative deviations of the reduced viscosity of the blends from the additivity law confirming the presence of specific interactions within the blend solutions. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 |
Author | Amrani, Farouk Bouslah, Naima Haddadine, Nabila Hammachin, Rabah |
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Cites_doi | 10.1016/S0032-3861(02)00928-X 10.1016/0032-3861(95)93655-6 10.1016/S0032-3861(01)00462-1 10.1016/j.progpolymsci.2004.07.002 10.1016/S0032-3861(97)00096-7 10.1016/S0032-3861(03)00578-0 10.1016/S0032-3861(00)00332-3 10.1021/ma9614611 10.1016/S0032-3861(02)00291-4 10.1081/MB-100100380 10.1016/S0032-3861(01)00641-3 10.1016/S0032-3861(97)10271-3 10.1080/00222349808212418 10.1021/ma00200a052 10.1016/S0032-3861(02)00878-9 10.1016/j.eurpolymj.2003.11.016 10.1016/0032-3861(95)97882-G 10.1016/S0032-3861(03)00188-5 10.1002/polb.1989.090270508 |
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Keywords | Polymer blends Property composition relationship Experimental study viscosimetry Thermal properties hydrogen bonding viscosity DSC FTIR Miscibility Pyridine(4-vinyl) copolymer Interpolymer Acid copolymer Thermodynamic properties Pyridine(4-vinyl) polymer glass transition Cinnamic derivative copolymer Hydrogen bond Styrene copolymer |
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Snippet | The compatibilization of an immiscible polymer system polystyrene/poly(4-vinylpyridine) has been induced by the introduction of carboxylic acid groups within... The compatibilization of an immiscible polymer system polystyrene/poly(4‐vinylpyridine) has been induced by the introduction of carboxylic acid groups within... Abstract The compatibilization of an immiscible polymer system polystyrene/poly(4‐vinylpyridine) has been induced by the introduction of carboxylic acid groups... |
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SubjectTerms | Applied sciences DSC Exact sciences and technology FTIR glass transition hydrogen bonding Organic polymers Physicochemistry of polymers polymer blends Properties and characterization Thermal and thermodynamic properties viscosimetry viscosity |
Title | Comparison of specific interactions in P4VP/PSCA and PS4VP/PSCA blends and complexes |
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