Gram-scale free radical polymerization of an azaborine vinyl monomer

The gram-scale polymerization of a novel azaborine vinyl monomer is reported. We describe an efficient and high-yielding synthesis of B-vinyl-2,1-borazanaphthalene. Homopolymers and co-polymers with 2-vinylnaphthalene are characterized by heteronuclear NMR and absorbance spectroscopy.

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Bibliographic Details
Published inChemical communications (Cambridge, England) Vol. 53; no. 53; pp. 7262 - 7265
Main Authors van de Wouw, Heidi L, Lee, Jae Young, Klausen, Rebekka S
Format Journal Article
LanguageEnglish
Published England 2017
Subjects
Absorbance
Copolymers
Free radical polymerization
Monomers
Nuclear magnetic resonance
Polymerization
Spectroscopy
Synthesis
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Summary:The gram-scale polymerization of a novel azaborine vinyl monomer is reported. We describe an efficient and high-yielding synthesis of B-vinyl-2,1-borazanaphthalene. Homopolymers and co-polymers with 2-vinylnaphthalene are characterized by heteronuclear NMR and absorbance spectroscopy.
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ISSN:1359-7345
1364-548X
DOI:10.1039/c7cc02300f